data_mm241_5 _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C48 H64 Er2 K2 O4' _chemical_formula_weight 1117.71 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'K' 'K' 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Er' 'Er' -0.2586 4.9576 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting Triclinic _symmetry_space_group_name_H-M P-1 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.4865(10) _cell_length_b 12.8999(10) _cell_length_c 16.7853(15) _cell_angle_alpha 107.250(2) _cell_angle_beta 98.705(2) _cell_angle_gamma 111.302(2) _cell_volume 2301.4(3) _cell_formula_units_Z 2 _cell_measurement_temperature 200(2) _cell_measurement_reflns_used 3205 _cell_measurement_theta_min 2.45 _cell_measurement_theta_max 30.01 _exptl_crystal_description plate _exptl_crystal_colour orange _exptl_crystal_size_max 0.30 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.03 _exptl_crystal_density_meas n/a _exptl_crystal_density_diffrn 1.613 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 1116 _exptl_absorpt_coefficient_mu 3.843 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.3918 _exptl_absorpt_correction_T_max 0.8804 _exptl_absorpt_process_details 'SADABS, Bruker (2003)' _exptl_special_details ; Data collection is performed with four batch runs at phi = 0.00 deg (600 frames), at phi = 90.00 deg (600 frames), at phi = 180.00 deg (600 frames), and at phi = 270.00 deg (600 frames). A fifth batch run is collected at phi = 0.00 deg (50 frames) to monitor crystal and diffractometer stability. Frame width = 0.30 deg in omega. Data is merged, corrected for decay (if any), and treated with multi-scan absorption corrections (if required). All symmetry-equivalent reflections are merged for centrosymmetric data. Friedel pairs are not merged for noncentrosymmetric data. ; _diffrn_ambient_temperature 200(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 19618 _diffrn_reflns_av_R_equivalents 0.0000 _diffrn_reflns_av_sigmaI/netI 0.1445 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_theta_min 1.81 _diffrn_reflns_theta_max 30.55 _reflns_number_total 12703 _reflns_number_gt 7065 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'APEX II, Bruker (2009)' _computing_cell_refinement 'APEX II, Bruker (2009)' _computing_data_reduction 'XPREP, Bruker (2009)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 2008)' _computing_molecular_graphics 'SHELXTL, Bruker (2004)' _computing_publication_material 'SHELXTL, Bruker (2004)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0819P)^2^]' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 12703 _refine_ls_number_parameters 578 _refine_ls_number_restraints 1246 _refine_ls_R_factor_all 0.1665 _refine_ls_R_factor_gt 0.0837 _refine_ls_wR_factor_ref 0.1864 _refine_ls_wR_factor_gt 0.1559 _refine_ls_goodness_of_fit_ref 1.046 _refine_ls_restrained_S_all 1.005 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Er1 Er 0.80006(4) 0.99441(4) 0.76808(3) 0.02634(13) Uani 1 1 d U A . Er2 Er 1.17401(4) 0.52533(4) 0.71019(3) 0.03023(14) Uani 1 1 d U . . K1 K 0.5930(2) 1.2174(2) 0.77336(15) 0.0353(5) Uani 1 1 d U . . K2 K 1.0017(2) 0.7742(2) 0.76522(18) 0.0477(7) Uani 1 1 d U A . O1 O 0.3760(8) 1.1032(8) 0.6521(7) 0.057(2) Uani 1 1 d U . . O2 O 0.7003(10) 1.4365(9) 0.9064(8) 0.067(3) Uani 1 1 d U . . O3 O 0.6288(10) 1.3323(8) 0.6618(7) 0.058(2) Uani 1 1 d U . . O4 O 0.4558(9) 1.1994(9) 0.8822(7) 0.054(2) Uani 1 1 d U . . C1 C 0.5743(11) 0.9491(11) 0.7173(11) 0.051(2) Uani 1 1 d U . . H1A H 0.5008 0.8786 0.6884 0.061 Uiso 1 1 calc R . . C2 C 0.6276(13) 0.9924(12) 0.6577(8) 0.052(2) Uani 1 1 d U . . H2A H 0.5842 0.9436 0.5982 0.062 Uiso 1 1 calc R . . C3 C 0.7295(14) 1.0908(13) 0.6695(10) 0.051(2) Uani 1 1 d U . . H3A H 0.7398 1.0931 0.6151 0.061 Uiso 1 1 calc R . . C4 C 0.8204(13) 1.1863(12) 0.7367(11) 0.050(2) Uani 1 1 d U . . H4A H 0.8755 1.2394 0.7175 0.061 Uiso 1 1 calc R . . C5 C 0.8518(12) 1.2250(11) 0.8293(11) 0.053(2) Uani 1 1 d U . . H5A H 0.9233 1.2976 0.8583 0.063 Uiso 1 1 calc R . . C6 C 0.7995(13) 1.1787(12) 0.8860(9) 0.053(2) Uani 1 1 d U . . H6A H 0.8444 1.2263 0.9454 0.064 Uiso 1 1 calc R . . C7 C 0.6953(14) 1.0775(14) 0.8761(9) 0.052(2) Uani 1 1 d U . . H7A H 0.6873 1.0730 0.9305 0.062 Uiso 1 1 calc R . . C8 C 0.6029(12) 0.9841(13) 0.8070(12) 0.052(2) Uani 1 1 d U . . H8A H 0.5452 0.9314 0.8249 0.062 Uiso 1 1 calc R . . C9 C 0.7467(11) 0.7639(10) 0.7063(10) 0.057(2) Uani 1 1 d DU . . H9A H 0.6732 0.6940 0.6752 0.069 Uiso 1 1 calc R A . C10 C 0.8069(12) 0.8099(11) 0.6511(7) 0.056(2) Uani 1 1 d DU A . H10A H 0.7678 0.7611 0.5910 0.068 Uiso 1 1 calc R . . C11 C 0.9098(13) 0.9098(13) 0.6650(8) 0.051(2) Uani 1 1 d DU . . H11A H 0.9200 0.9166 0.6115 0.061 Uiso 1 1 calc R A . C12 C 1.0020(11) 1.0028(11) 0.7352(10) 0.048(2) Uani 1 1 d DU A . H12A H 1.0645 1.0523 0.7187 0.057 Uiso 1 1 calc R . . C13 C 1.0230(11) 1.0396(10) 0.8255(9) 0.047(2) Uani 1 1 d DU . . H13A H 1.0920 1.1142 0.8561 0.056 Uiso 1 1 calc R A . C14 C 0.9675(12) 0.9938(11) 0.8826(7) 0.050(2) Uani 1 1 d DU A . H14A H 1.0092 1.0415 0.9425 0.060 Uiso 1 1 calc R . . C15 C 0.8629(12) 0.8918(12) 0.8684(8) 0.050(2) Uani 1 1 d DU A . H15A H 0.8519 0.8847 0.9217 0.060 Uiso 1 1 calc R . . C16 C 0.7717(12) 0.7989(11) 0.7973(11) 0.055(2) Uani 1 1 d DU A . H16A H 0.7116 0.7463 0.8137 0.066 Uiso 1 1 calc R . . C17 C 0.959(2) 0.518(2) 0.658(2) 0.043(4) Uani 0.50 1 d PDU A 1 H17A H 0.8871 0.4550 0.6165 0.052 Uiso 0.50 1 calc PR A 1 C18 C 1.032(3) 0.592(3) 0.6219(11) 0.042(4) Uani 0.50 1 d PDU A 1 H18A H 0.9946 0.5718 0.5624 0.050 Uiso 0.50 1 calc PR A 1 C19 C 1.145(3) 0.686(3) 0.6520(19) 0.038(4) Uani 0.50 1 d PDU A 1 H19A H 1.1699 0.7085 0.6066 0.045 Uiso 0.50 1 calc PR A 1 C20 C 1.232(2) 0.755(2) 0.732(3) 0.036(4) Uani 0.50 1 d PDU A 1 H20A H 1.2988 0.8182 0.7288 0.044 Uiso 0.50 1 calc PR A 1 C21 C 1.2446(19) 0.753(2) 0.815(2) 0.035(5) Uani 0.50 1 d PDU A 1 H21A H 1.3187 0.8140 0.8557 0.041 Uiso 0.50 1 calc PR A 1 C22 C 1.173(3) 0.681(3) 0.8538(11) 0.034(5) Uani 0.50 1 d PDU A 1 H22A H 1.2114 0.7029 0.9135 0.041 Uiso 0.50 1 calc PR A 1 C23 C 1.058(3) 0.585(3) 0.8226(19) 0.035(4) Uani 0.50 1 d PDU A 1 H23A H 1.0339 0.5600 0.8674 0.042 Uiso 0.50 1 calc PR A 1 C24 C 0.970(2) 0.518(2) 0.743(3) 0.040(4) Uani 0.50 1 d PDU A 1 H24A H 0.9002 0.4585 0.7463 0.048 Uiso 0.50 1 calc PR A 1 C17' C 0.9489(18) 0.503(2) 0.691(3) 0.043(5) Uani 0.50 1 d PDU A 2 H17B H 0.8707 0.4385 0.6673 0.051 Uiso 0.50 1 calc PR A 2 C18' C 0.992(3) 0.546(3) 0.6281(14) 0.043(4) Uani 0.50 1 d PDU A 2 H18B H 0.9394 0.4972 0.5708 0.051 Uiso 0.50 1 calc PR A 2 C19' C 1.090(4) 0.640(3) 0.6290(15) 0.040(4) Uani 0.50 1 d PDU A 2 H19B H 1.0821 0.6482 0.5741 0.048 Uiso 0.50 1 calc PR A 2 C20' C 1.196(3) 0.727(3) 0.690(3) 0.038(4) Uani 0.50 1 d PDU A 2 H20B H 1.2502 0.7725 0.6662 0.046 Uiso 0.50 1 calc PR A 2 C21' C 1.2433(18) 0.7624(19) 0.781(2) 0.035(4) Uani 0.50 1 d PDU A 2 H21B H 1.3167 0.8336 0.8045 0.042 Uiso 0.50 1 calc PR A 2 C22' C 1.208(3) 0.718(3) 0.8445(14) 0.033(5) Uani 0.50 1 d PDU A 2 H22B H 1.2671 0.7602 0.8999 0.040 Uiso 0.50 1 calc PR A 2 C23' C 1.103(3) 0.625(3) 0.8430(14) 0.033(5) Uani 0.50 1 d PDU A 2 H23B H 1.1060 0.6222 0.8991 0.040 Uiso 0.50 1 calc PR A 2 C24' C 0.998(3) 0.537(2) 0.781(2) 0.039(5) Uani 0.50 1 d PDU A 2 H24B H 0.9469 0.4872 0.8042 0.047 Uiso 0.50 1 calc PR A 2 C25 C 1.1044(14) 0.2957(11) 0.6540(12) 0.059(3) Uani 1 1 d U A . H25A H 1.0287 0.2282 0.6364 0.071 Uiso 1 1 calc R . . C26 C 1.1330(14) 0.3300(12) 0.5867(10) 0.057(3) Uani 1 1 d U A . H26A H 1.0717 0.2784 0.5332 0.068 Uiso 1 1 calc R . . C27 C 1.2248(14) 0.4175(13) 0.5750(9) 0.057(2) Uani 1 1 d U A . H27A H 1.2115 0.4122 0.5164 0.069 Uiso 1 1 calc R . . C28 C 1.3313(15) 0.5106(14) 0.6297(12) 0.062(3) Uani 1 1 d U A . H28A H 1.3753 0.5549 0.5999 0.074 Uiso 1 1 calc R . . C29 C 1.3919(12) 0.5572(13) 0.7194(13) 0.063(3) Uani 1 1 d U A . H29A H 1.4650 0.6276 0.7369 0.075 Uiso 1 1 calc R . . C30 C 1.3667(14) 0.5210(15) 0.7894(11) 0.066(3) Uani 1 1 d U A . H30A H 1.4295 0.5696 0.8425 0.080 Uiso 1 1 calc R . . C31 C 1.2726(16) 0.4321(15) 0.7981(10) 0.064(3) Uani 1 1 d U A . H31A H 1.2858 0.4350 0.8561 0.077 Uiso 1 1 calc R . . C32 C 1.1647(16) 0.3404(13) 0.7441(12) 0.061(3) Uani 1 1 d U A . H32A H 1.1200 0.2966 0.7738 0.073 Uiso 1 1 calc R . . C33 C 0.2939(13) 1.1507(13) 0.6363(11) 0.062(4) Uani 1 1 d U . . H33A H 0.3322 1.2232 0.6232 0.074 Uiso 1 1 calc R . . H33B H 0.2661 1.1737 0.6882 0.074 Uiso 1 1 calc R . . C34 C 0.1893(14) 1.0543(14) 0.5594(11) 0.063(4) Uani 1 1 d U . . H34A H 0.1124 1.0561 0.5659 0.076 Uiso 1 1 calc R . . H34B H 0.1998 1.0627 0.5040 0.076 Uiso 1 1 calc R . . C35 C 0.1946(12) 0.9430(13) 0.5635(11) 0.057(3) Uani 1 1 d U . . H35A H 0.1499 0.9152 0.6027 0.069 Uiso 1 1 calc R . . H35B H 0.1612 0.8778 0.5049 0.069 Uiso 1 1 calc R . . C36 C 0.3240(12) 0.9805(12) 0.5984(10) 0.051(3) Uani 1 1 d U . . H36A H 0.3371 0.9330 0.6324 0.062 Uiso 1 1 calc R . . H36B H 0.3606 0.9674 0.5501 0.062 Uiso 1 1 calc R . . C37 C 0.8222(14) 1.5107(13) 0.9586(14) 0.076(5) Uani 1 1 d U . . H37A H 0.8780 1.4877 0.9295 0.091 Uiso 1 1 calc R . . H37B H 0.8350 1.5046 1.0164 0.091 Uiso 1 1 calc R . . C38 C 0.8395(19) 1.6313(15) 0.9671(17) 0.102(6) Uani 1 1 d U . . H38A H 0.8668 1.6500 0.9185 0.123 Uiso 1 1 calc R . . H38B H 0.9001 1.6915 1.0229 0.123 Uiso 1 1 calc R . . C39 C 0.7209(18) 1.6319(15) 0.9646(15) 0.095(5) Uani 1 1 d U . . H39A H 0.7155 1.6651 1.0243 0.114 Uiso 1 1 calc R . . H39B H 0.7065 1.6806 0.9321 0.114 Uiso 1 1 calc R . . C40 C 0.6348(16) 1.5061(14) 0.9200(13) 0.083(5) Uani 1 1 d U . . H40A H 0.5819 1.4821 0.9560 0.100 Uiso 1 1 calc R . . H40B H 0.5842 1.4936 0.8635 0.100 Uiso 1 1 calc R . . C41 C 0.6049(19) 1.2591(13) 0.5728(10) 0.075(5) Uani 1 1 d U . . H41A H 0.5414 1.1773 0.5576 0.090 Uiso 1 1 calc R . . H41B H 0.6783 1.2527 0.5617 0.090 Uiso 1 1 calc R . . C44 C 0.6202(15) 1.4397(12) 0.6679(10) 0.061(4) Uani 1 1 d U . . H44A H 0.6975 1.5099 0.7038 0.073 Uiso 1 1 calc R . . H44B H 0.5569 1.4464 0.6953 0.073 Uiso 1 1 calc R . . C43 C 0.589(2) 1.4361(15) 0.5771(12) 0.090(6) Uani 1 1 d U . . H43A H 0.5180 1.4520 0.5652 0.108 Uiso 1 1 calc R . . H43B H 0.6574 1.4969 0.5684 0.108 Uiso 1 1 calc R . . C42 C 0.565(3) 1.3195(16) 0.5224(13) 0.132(8) Uani 1 1 d U . . H42A H 0.6078 1.3238 0.4773 0.159 Uiso 1 1 calc R . . H42B H 0.4782 1.2730 0.4926 0.159 Uiso 1 1 calc R . . C45 C 0.5134(14) 1.2408(14) 0.9731(10) 0.062(4) Uani 1 1 d U . . H45A H 0.5087 1.3160 1.0057 0.075 Uiso 1 1 calc R . . H45B H 0.5990 1.2564 0.9835 0.075 Uiso 1 1 calc R . . C47 C 0.3248(15) 1.0756(14) 0.9384(11) 0.067(4) Uani 1 1 d U . . H47A H 0.2690 1.1072 0.9600 0.080 Uiso 1 1 calc R . . H47B H 0.2919 0.9884 0.9265 0.080 Uiso 1 1 calc R . . C48 C 0.3470(14) 1.0997(17) 0.8588(11) 0.084(6) Uani 1 1 d U . . H48A H 0.3485 1.0287 0.8162 0.101 Uiso 1 1 calc R . . H48B H 0.2812 1.1146 0.8310 0.101 Uiso 1 1 calc R . . C46 C 0.4469(17) 1.1418(16) 1.0012(12) 0.082(5) Uani 1 1 d U . . H46A H 0.4871 1.0879 0.9993 0.098 Uiso 1 1 calc R . . H46B H 0.4429 1.1754 1.0614 0.098 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Er1 0.0279(3) 0.0258(3) 0.0296(3) 0.0122(2) 0.0055(2) 0.0159(2) Er2 0.0317(3) 0.0298(3) 0.0342(3) 0.0124(2) 0.0086(2) 0.0189(2) K1 0.0360(13) 0.0341(12) 0.0377(12) 0.0132(10) 0.0079(11) 0.0185(11) K2 0.0500(17) 0.0471(15) 0.0626(17) 0.0229(14) 0.0147(15) 0.0377(14) O1 0.040(4) 0.055(5) 0.059(5) 0.009(4) -0.006(4) 0.022(3) O2 0.060(5) 0.044(4) 0.073(6) -0.004(4) 0.005(5) 0.023(4) O3 0.083(6) 0.044(5) 0.053(5) 0.026(4) 0.015(5) 0.030(5) O4 0.047(5) 0.068(6) 0.047(5) 0.023(5) 0.013(4) 0.024(4) C1 0.027(4) 0.029(4) 0.081(6) 0.011(4) -0.002(4) 0.010(3) C2 0.060(5) 0.054(5) 0.035(4) 0.001(4) -0.009(4) 0.040(4) C3 0.076(6) 0.074(6) 0.044(4) 0.040(4) 0.030(4) 0.057(4) C4 0.051(5) 0.041(5) 0.093(6) 0.047(5) 0.042(5) 0.030(4) C5 0.034(4) 0.020(4) 0.086(6) 0.007(4) 0.001(4) 0.011(3) C6 0.059(5) 0.055(5) 0.035(4) -0.003(4) -0.007(4) 0.039(4) C7 0.074(6) 0.081(6) 0.044(4) 0.037(4) 0.035(4) 0.060(4) C8 0.040(4) 0.057(5) 0.091(6) 0.051(5) 0.037(5) 0.029(4) C9 0.033(4) 0.022(4) 0.094(7) 0.006(4) -0.005(5) 0.010(4) C10 0.068(6) 0.054(6) 0.038(4) -0.002(4) -0.013(5) 0.042(4) C11 0.076(6) 0.074(6) 0.041(5) 0.033(5) 0.030(5) 0.059(5) C12 0.044(6) 0.050(5) 0.079(6) 0.041(5) 0.038(5) 0.030(4) C13 0.028(4) 0.030(4) 0.067(6) 0.009(4) -0.001(4) 0.010(3) C14 0.056(5) 0.063(5) 0.031(4) 0.007(4) -0.004(4) 0.041(4) C15 0.062(6) 0.083(6) 0.055(5) 0.053(4) 0.030(4) 0.059(5) C16 0.041(5) 0.047(5) 0.106(7) 0.053(5) 0.037(5) 0.026(3) C17 0.029(6) 0.037(5) 0.052(10) 0.011(6) -0.004(6) 0.013(5) C18 0.042(9) 0.039(8) 0.038(7) 0.010(6) -0.003(6) 0.020(7) C19 0.046(9) 0.037(8) 0.035(9) 0.018(7) 0.010(7) 0.021(7) C20 0.034(6) 0.031(5) 0.042(12) 0.014(6) 0.009(7) 0.013(5) C21 0.026(7) 0.030(6) 0.036(10) 0.008(6) 0.001(8) 0.009(6) C22 0.031(11) 0.037(9) 0.036(8) 0.013(6) 0.007(7) 0.018(8) C23 0.037(11) 0.035(11) 0.046(9) 0.023(8) 0.017(8) 0.021(9) C24 0.022(6) 0.036(6) 0.061(13) 0.020(7) 0.011(7) 0.012(5) C17' 0.020(5) 0.034(5) 0.065(13) 0.016(6) 0.002(6) 0.007(5) C18' 0.033(7) 0.038(7) 0.045(8) 0.009(5) -0.006(6) 0.015(6) C19' 0.049(10) 0.042(9) 0.034(8) 0.018(6) 0.007(7) 0.025(8) C20' 0.040(7) 0.032(6) 0.047(12) 0.021(7) 0.015(8) 0.015(6) C21' 0.025(5) 0.028(5) 0.045(11) 0.012(6) 0.008(6) 0.007(5) C22' 0.027(10) 0.034(8) 0.033(8) 0.010(7) 0.000(7) 0.014(7) C23' 0.035(11) 0.036(11) 0.038(9) 0.020(7) 0.012(8) 0.020(9) C24' 0.032(8) 0.028(9) 0.060(12) 0.018(9) 0.022(9) 0.012(7) C25 0.052(6) 0.030(3) 0.096(7) 0.019(4) 0.026(5) 0.021(4) C26 0.059(6) 0.045(4) 0.051(5) -0.003(4) 0.003(5) 0.030(4) C27 0.087(7) 0.063(6) 0.045(5) 0.020(4) 0.028(5) 0.053(5) C28 0.064(6) 0.066(7) 0.085(7) 0.036(6) 0.050(5) 0.042(5) C29 0.030(4) 0.051(6) 0.102(8) 0.015(6) 0.018(4) 0.023(4) C30 0.054(5) 0.082(7) 0.061(6) 0.007(6) -0.007(5) 0.053(5) C31 0.096(7) 0.087(7) 0.051(6) 0.035(5) 0.021(5) 0.077(6) C32 0.087(7) 0.058(5) 0.088(7) 0.051(6) 0.055(6) 0.057(5) C33 0.052(7) 0.055(7) 0.079(10) 0.021(7) 0.014(6) 0.030(6) C34 0.055(8) 0.090(9) 0.059(9) 0.038(8) 0.004(6) 0.044(7) C35 0.038(6) 0.060(7) 0.055(9) 0.016(7) 0.002(6) 0.013(6) C36 0.039(6) 0.049(6) 0.062(9) 0.019(6) 0.004(6) 0.021(5) C37 0.055(7) 0.055(7) 0.095(13) 0.007(7) 0.003(8) 0.024(6) C38 0.087(9) 0.046(7) 0.143(16) 0.021(10) 0.025(13) 0.011(7) C39 0.116(12) 0.054(6) 0.129(15) 0.037(9) 0.035(12) 0.051(8) C40 0.078(8) 0.064(7) 0.103(13) 0.012(8) 0.014(10) 0.045(7) C41 0.131(14) 0.044(7) 0.043(7) 0.018(6) 0.015(9) 0.036(8) C44 0.088(10) 0.045(7) 0.064(7) 0.023(6) 0.022(8) 0.042(7) C43 0.150(16) 0.071(9) 0.069(10) 0.037(8) 0.017(11) 0.064(11) C42 0.24(2) 0.063(9) 0.054(7) 0.019(7) -0.026(13) 0.053(12) C45 0.056(8) 0.078(9) 0.038(6) 0.019(7) 0.011(5) 0.017(6) C47 0.071(8) 0.056(9) 0.061(9) 0.022(8) 0.018(7) 0.015(7) C48 0.050(8) 0.109(12) 0.052(8) 0.026(9) 0.009(6) -0.002(7) C46 0.087(10) 0.079(10) 0.064(9) 0.039(9) 0.005(8) 0.014(9) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Er1 C3 2.575(12) . ? Er1 C11 2.597(13) . ? Er1 C13 2.588(12) . ? Er1 C7 2.595(13) . ? Er1 C2 2.606(11) . ? Er1 C6 2.607(13) . ? Er1 C1 2.606(13) . ? Er1 C8 2.609(13) . ? Er1 C4 2.614(11) . ? Er1 C9 2.624(12) . ? Er1 C14 2.621(12) . ? Er1 C16 2.620(11) . ? Er2 C26 2.559(14) . ? Er2 C29 2.573(13) . ? Er2 C28 2.576(14) . ? Er2 C25 2.578(13) . ? Er2 C27 2.587(13) . ? Er2 C32 2.579(13) . ? Er2 C31 2.592(14) . ? Er2 C30 2.595(15) . ? Er2 C18' 2.62(2) . ? Er2 C20' 2.64(2) . ? Er2 C19 2.64(2) . ? Er2 C17 2.65(3) . ? K1 O4 2.691(10) . ? K1 O1 2.703(10) . ? K1 O3 2.706(9) . ? K1 O2 2.714(11) . ? K1 C4 3.132(14) . ? K1 C3 3.137(14) . ? K1 C5 3.182(14) . ? K1 C2 3.195(12) . ? K1 C1 3.215(13) . ? K1 C6 3.239(14) . ? K1 C8 3.263(13) . ? K1 C7 3.274(13) . ? K2 C18 3.01(2) . ? K2 C19' 3.03(3) . ? K2 C17 3.05(3) . ? K2 C21' 3.05(3) . ? K2 C24 3.08(3) . ? K2 C19 3.06(3) . ? K2 C20' 3.07(3) . ? K2 C20 3.10(3) . ? K2 C15 3.093(13) . ? K2 C18' 3.10(3) . ? K2 C16 3.110(13) . ? K2 C17' 3.11(3) . ? O1 C36 1.404(16) . ? O1 C33 1.403(16) . ? O2 C40 1.413(18) . ? O2 C37 1.429(19) . ? O3 C44 1.403(15) . ? O3 C41 1.426(17) . ? O4 C48 1.387(17) . ? O4 C45 1.427(17) . ? C1 C8 1.38(2) . ? C1 C2 1.420(19) . ? C2 C3 1.367(19) . ? C3 C4 1.36(2) . ? C4 C5 1.43(2) . ? C5 C6 1.39(2) . ? C6 C7 1.414(19) . ? C7 C8 1.37(2) . ? C9 C16 1.407(18) . ? C9 C10 1.410(18) . ? C10 C11 1.376(17) . ? C11 C12 1.379(17) . ? C12 C13 1.398(17) . ? C13 C14 1.409(16) . ? C14 C15 1.402(16) . ? C15 C16 1.381(17) . ? C17 C24 1.41(2) . ? C17 C18 1.41(2) . ? C18 C19 1.37(2) . ? C19 C20 1.38(2) . ? C20 C21 1.40(2) . ? C21 C22 1.41(2) . ? C22 C23 1.41(2) . ? C23 C24 1.39(2) . ? C17' C24' 1.41(2) . ? C17' C18' 1.41(2) . ? C18' C19' 1.37(2) . ? C19' C20' 1.38(2) . ? C20' C21' 1.40(2) . ? C21' C22' 1.41(2) . ? C22' C23' 1.41(2) . ? C23' C24' 1.38(2) . ? C25 C26 1.38(2) . ? C25 C32 1.42(2) . ? C26 C27 1.374(19) . ? C27 C28 1.37(2) . ? C28 C29 1.41(2) . ? C29 C30 1.42(2) . ? C30 C31 1.37(2) . ? C31 C32 1.37(2) . ? C33 C34 1.51(2) . ? C34 C35 1.48(2) . ? C35 C36 1.471(19) . ? C37 C38 1.45(2) . ? C38 C39 1.48(3) . ? C39 C40 1.46(2) . ? C41 C42 1.45(2) . ? C44 C43 1.50(2) . ? C43 C42 1.40(2) . ? C45 C46 1.499(19) . ? C47 C46 1.48(2) . ? C47 C48 1.50(2) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C3 Er1 C11 93.9(4) . . ? C3 Er1 C13 123.1(4) . . ? C11 Er1 C13 59.0(4) . . ? C3 Er1 C7 88.4(4) . . ? C11 Er1 C7 177.6(4) . . ? C13 Er1 C7 119.1(5) . . ? C3 Er1 C2 30.6(4) . . ? C11 Er1 C2 101.5(4) . . ? C13 Er1 C2 150.9(5) . . ? C7 Er1 C2 80.8(4) . . ? C3 Er1 C6 80.1(5) . . ? C11 Er1 C6 148.4(5) . . ? C13 Er1 C6 98.4(4) . . ? C7 Er1 C6 31.5(4) . . ? C2 Er1 C6 89.1(4) . . ? C3 Er1 C1 59.0(5) . . ? C11 Er1 C1 123.2(5) . . ? C13 Er1 C1 177.3(5) . . ? C7 Er1 C1 58.6(5) . . ? C2 Er1 C1 31.6(4) . . ? C6 Er1 C1 80.2(5) . . ? C3 Er1 C8 80.1(4) . . ? C11 Er1 C8 150.6(5) . . ? C13 Er1 C8 146.6(5) . . ? C7 Er1 C8 30.6(5) . . ? C2 Er1 C8 59.8(5) . . ? C6 Er1 C8 59.3(5) . . ? C1 Er1 C8 30.8(5) . . ? C3 Er1 C4 30.4(5) . . ? C11 Er1 C4 101.0(4) . . ? C13 Er1 C4 101.5(4) . . ? C7 Er1 C4 80.6(4) . . ? C2 Er1 C4 58.5(5) . . ? C6 Er1 C4 59.4(5) . . ? C1 Er1 C4 79.7(4) . . ? C8 Er1 C4 88.3(4) . . ? C3 Er1 C9 120.5(5) . . ? C11 Er1 C9 58.9(4) . . ? C13 Er1 C9 89.0(4) . . ? C7 Er1 C9 120.4(5) . . ? C2 Er1 C9 99.0(4) . . ? C6 Er1 C9 149.2(5) . . ? C1 Er1 C9 91.2(4) . . ? C8 Er1 C9 99.4(4) . . ? C4 Er1 C9 148.2(5) . . ? C3 Er1 C14 151.1(5) . . ? C11 Er1 C14 80.3(4) . . ? C13 Er1 C14 31.4(4) . . ? C7 Er1 C14 97.4(4) . . ? C2 Er1 C14 177.7(4) . . ? C6 Er1 C14 90.1(4) . . ? C1 Er1 C14 146.1(5) . . ? C8 Er1 C14 118.0(4) . . ? C4 Er1 C14 122.7(5) . . ? C9 Er1 C14 80.7(4) . . ? C3 Er1 C16 148.0(5) . . ? C11 Er1 C16 79.8(4) . . ? C13 Er1 C16 80.5(4) . . ? C7 Er1 C16 98.6(4) . . ? C2 Er1 C16 119.6(5) . . ? C6 Er1 C16 120.7(5) . . ? C1 Er1 C16 98.3(4) . . ? C8 Er1 C16 90.2(4) . . ? C4 Er1 C16 178.0(4) . . ? C9 Er1 C16 31.1(4) . . ? C14 Er1 C16 59.1(4) . . ? C26 Er2 C29 80.8(5) . . ? C26 Er2 C28 58.8(5) . . ? C29 Er2 C28 31.8(5) . . ? C26 Er2 C25 31.2(5) . . ? C29 Er2 C25 90.1(5) . . ? C28 Er2 C25 81.0(5) . . ? C26 Er2 C27 31.0(4) . . ? C29 Er2 C27 59.9(5) . . ? C28 Er2 C27 30.7(5) . . ? C25 Er2 C27 59.7(5) . . ? C26 Er2 C32 59.9(5) . . ? C29 Er2 C32 81.5(5) . . ? C28 Er2 C32 89.7(5) . . ? C25 Er2 C32 31.9(5) . . ? C27 Er2 C32 81.6(5) . . ? C26 Er2 C31 80.4(5) . . ? C29 Er2 C31 60.1(6) . . ? C28 Er2 C31 81.3(5) . . ? C25 Er2 C31 59.6(6) . . ? C27 Er2 C31 89.3(5) . . ? C32 Er2 C31 30.7(5) . . ? C26 Er2 C30 88.6(5) . . ? C29 Er2 C30 32.0(5) . . ? C28 Er2 C30 60.5(6) . . ? C25 Er2 C30 80.9(5) . . ? C27 Er2 C30 81.2(5) . . ? C32 Er2 C30 58.9(6) . . ? C31 Er2 C30 30.7(5) . . ? C26 Er2 C18' 93.2(6) . . ? C29 Er2 C18' 143.9(10) . . ? C28 Er2 C18' 116.7(9) . . ? C25 Er2 C18' 103.1(8) . . ? C27 Er2 C18' 98.0(7) . . ? C32 Er2 C18' 126.0(9) . . ? C31 Er2 C18' 154.3(10) . . ? C30 Er2 C18' 175.0(10) . . ? C26 Er2 C20' 124.8(9) . . ? C29 Er2 C20' 96.6(7) . . ? C28 Er2 C20' 91.3(6) . . ? C25 Er2 C20' 153.4(10) . . ? C27 Er2 C20' 101.9(7) . . ? C32 Er2 C20' 174.7(10) . . ? C31 Er2 C20' 144.6(10) . . ? C30 Er2 C20' 117.4(9) . . ? C18' Er2 C20' 57.8(6) . . ? C26 Er2 C19 112.5(8) . . ? C29 Er2 C19 105.6(8) . . ? C28 Er2 C19 92.4(7) . . ? C25 Er2 C19 138.3(9) . . ? C27 Er2 C19 94.9(6) . . ? C32 Er2 C19 169.2(10) . . ? C31 Er2 C19 160.1(10) . . ? C30 Er2 C19 130.9(10) . . ? C18' Er2 C19 44.1(6) . . ? C20' Er2 C19 15.9(6) . . ? C26 Er2 C17 95.7(7) . . ? C29 Er2 C17 161.0(10) . . ? C28 Er2 C17 131.9(10) . . ? C25 Er2 C17 96.6(7) . . ? C27 Er2 C17 108.6(8) . . ? C32 Er2 C17 113.1(8) . . ? C31 Er2 C17 138.2(9) . . ? C30 Er2 C17 167.0(10) . . ? C18' Er2 C17 17.1(6) . . ? C20' Er2 C17 69.8(7) . . ? C19 Er2 C17 58.2(6) . . ? O4 K1 O1 82.1(3) . . ? O4 K1 O3 134.6(3) . . ? O1 K1 O3 77.7(3) . . ? O4 K1 O2 75.5(3) . . ? O1 K1 O2 131.2(3) . . ? O3 K1 O2 88.1(3) . . ? O4 K1 C4 142.4(4) . . ? O1 K1 C4 123.0(4) . . ? O3 K1 C4 81.4(3) . . ? O2 K1 C4 100.0(4) . . ? O4 K1 C3 143.1(3) . . ? O1 K1 C3 98.8(4) . . ? O3 K1 C3 80.4(3) . . ? O2 K1 C3 124.8(4) . . ? C4 K1 C3 25.1(4) . . ? O4 K1 C5 118.9(4) . . ? O1 K1 C5 146.0(4) . . ? O3 K1 C5 99.6(4) . . ? O2 K1 C5 82.0(4) . . ? C4 K1 C5 26.1(4) . . ? C3 K1 C5 48.0(4) . . ? O4 K1 C2 122.1(4) . . ? O1 K1 C2 82.2(3) . . ? O3 K1 C2 94.9(3) . . ? O2 K1 C2 146.0(4) . . ? C4 K1 C2 47.5(4) . . ? C3 K1 C2 24.9(4) . . ? C5 K1 C2 64.1(3) . . ? O4 K1 C1 97.0(4) . . ? O1 K1 C1 82.3(3) . . ? O3 K1 C1 119.6(4) . . ? O2 K1 C1 142.5(4) . . ? C4 K1 C1 63.6(3) . . ? C3 K1 C1 47.3(4) . . ? C5 K1 C1 69.5(3) . . ? C2 K1 C1 25.6(4) . . ? O4 K1 C6 95.0(4) . . ? O1 K1 C6 144.4(3) . . ? O3 K1 C6 124.3(4) . . ? O2 K1 C6 81.1(4) . . ? C4 K1 C6 47.9(4) . . ? C3 K1 C6 63.1(4) . . ? C5 K1 C6 25.0(4) . . ? C2 K1 C6 69.3(3) . . ? C1 K1 C6 62.7(3) . . ? O4 K1 C8 80.5(3) . . ? O1 K1 C8 98.1(4) . . ? O3 K1 C8 142.1(4) . . ? O2 K1 C8 119.6(4) . . ? C4 K1 C8 69.3(3) . . ? C3 K1 C8 62.8(3) . . ? C5 K1 C8 63.1(3) . . ? C2 K1 C8 47.5(4) . . ? C1 K1 C8 24.7(4) . . ? C6 K1 C8 46.7(4) . . ? O4 K1 C7 79.8(3) . . ? O1 K1 C7 121.6(4) . . ? O3 K1 C7 144.9(3) . . ? O2 K1 C7 96.5(4) . . ? C4 K1 C7 63.4(3) . . ? C3 K1 C7 68.3(3) . . ? C5 K1 C7 47.3(4) . . ? C2 K1 C7 62.8(3) . . ? C1 K1 C7 46.2(4) . . ? C6 K1 C7 25.1(3) . . ? C8 K1 C7 24.2(4) . . ? C18 K2 C19' 13.7(5) . . ? C18 K2 C17 26.9(4) . . ? C19' K2 C17 39.4(5) . . ? C18 K2 C21' 59.6(6) . . ? C19' K2 C21' 49.9(5) . . ? C17 K2 C21' 71.0(6) . . ? C18 K2 C24 50.5(5) . . ? C19' K2 C24 60.0(6) . . ? C17 K2 C24 26.6(4) . . ? C21' K2 C24 70.0(6) . . ? C18 K2 C19 26.2(4) . . ? C19' K2 C19 12.8(4) . . ? C17 K2 C19 49.8(5) . . ? C21' K2 C19 39.1(5) . . ? C24 K2 C19 66.5(6) . . ? C18 K2 C20' 38.7(5) . . ? C19' K2 C20' 26.2(4) . . ? C17 K2 C20' 59.3(6) . . ? C21' K2 C20' 26.5(4) . . ? C24 K2 C20' 70.8(6) . . ? C19 K2 C20' 13.7(5) . . ? C18 K2 C20 49.5(5) . . ? C19' K2 C20 37.9(5) . . ? C17 K2 C20 66.5(5) . . ? C21' K2 C20 14.6(5) . . ? C24 K2 C20 72.6(5) . . ? C19 K2 C20 25.9(4) . . ? C20' K2 C20 12.5(4) . . ? C18 K2 C15 156.5(7) . . ? C19' K2 C15 167.0(7) . . ? C17 K2 C15 136.1(7) . . ? C21' K2 C15 142.9(7) . . ? C24 K2 C15 121.3(6) . . ? C19 K2 C15 171.8(5) . . ? C20' K2 C15 164.2(7) . . ? C20 K2 C15 154.0(7) . . ? C18 K2 C18' 12.5(4) . . ? C19' K2 C18' 25.7(4) . . ? C17 K2 C18' 14.6(5) . . ? C21' K2 C18' 65.8(5) . . ? C24 K2 C18' 39.8(6) . . ? C19 K2 C18' 37.4(5) . . ? C20' K2 C18' 48.7(5) . . ? C20 K2 C18' 58.1(6) . . ? C15 K2 C18' 147.1(7) . . ? C18 K2 C16 130.8(7) . . ? C19' K2 C16 142.2(8) . . ? C17 K2 C16 114.4(6) . . ? C21' K2 C16 166.2(8) . . ? C24 K2 C16 108.7(5) . . ? C19 K2 C16 153.9(8) . . ? C20' K2 C16 167.1(8) . . ? C20 K2 C16 178.6(5) . . ? C15 K2 C16 25.7(3) . . ? C18' K2 C16 122.5(6) . . ? C18 K2 C17' 38.1(6) . . ? C19' K2 C17' 49.7(5) . . ? C17 K2 C17' 12.0(4) . . ? C21' K2 C17' 72.7(5) . . ? C24 K2 C17' 15.1(5) . . ? C19 K2 C17' 58.7(6) . . ? C20' K2 C17' 66.2(5) . . ? C20 K2 C17' 71.3(6) . . ? C15 K2 C17' 128.2(6) . . ? C18' K2 C17' 26.3(4) . . ? C16 K2 C17' 109.8(5) . . ? C36 O1 C33 108.9(10) . . ? C36 O1 K1 123.7(8) . . ? C33 O1 K1 127.3(9) . . ? C40 O2 C37 108.5(12) . . ? C40 O2 K1 118.0(10) . . ? C37 O2 K1 132.3(10) . . ? C44 O3 C41 110.3(11) . . ? C44 O3 K1 127.9(9) . . ? C41 O3 K1 116.6(7) . . ? C48 O4 C45 109.6(10) . . ? C48 O4 K1 121.3(9) . . ? C45 O4 K1 118.6(8) . . ? C8 C1 C2 135.9(12) . . ? C8 C1 Er1 74.7(8) . . ? C2 C1 Er1 74.2(7) . . ? C8 C1 K1 79.6(8) . . ? C2 C1 K1 76.4(7) . . ? Er1 C1 K1 100.9(4) . . ? C3 C2 C1 132.3(14) . . ? C3 C2 Er1 73.5(8) . . ? C1 C2 Er1 74.2(7) . . ? C3 C2 K1 75.2(9) . . ? C1 C2 K1 78.0(7) . . ? Er1 C2 K1 101.4(4) . . ? C4 C3 C2 138.5(14) . . ? C4 C3 Er1 76.4(8) . . ? C2 C3 Er1 75.9(7) . . ? C4 C3 K1 77.3(8) . . ? C2 C3 K1 79.9(9) . . ? Er1 C3 K1 103.7(4) . . ? C3 C4 C5 134.6(12) . . ? C3 C4 Er1 73.2(7) . . ? C5 C4 Er1 74.8(7) . . ? C3 C4 K1 77.7(8) . . ? C5 C4 K1 78.9(8) . . ? Er1 C4 K1 102.9(4) . . ? C6 C5 C4 133.4(12) . . ? C6 C5 Er1 73.7(7) . . ? C4 C5 Er1 73.6(7) . . ? C6 C5 K1 79.8(8) . . ? C4 C5 K1 75.0(8) . . ? Er1 C5 K1 101.2(4) . . ? C5 C6 C7 135.0(15) . . ? C5 C6 Er1 75.5(8) . . ? C7 C6 Er1 73.8(9) . . ? C5 C6 K1 75.2(8) . . ? C7 C6 K1 78.9(9) . . ? Er1 C6 K1 100.2(4) . . ? C8 C7 C6 135.5(14) . . ? C8 C7 Er1 75.3(8) . . ? C6 C7 Er1 74.7(9) . . ? C8 C7 K1 77.4(8) . . ? C6 C7 K1 76.1(9) . . ? Er1 C7 K1 99.6(4) . . ? C7 C8 C1 134.8(12) . . ? C7 C8 Er1 74.1(8) . . ? C1 C8 Er1 74.5(8) . . ? C7 C8 K1 78.3(8) . . ? C1 C8 K1 75.7(8) . . ? Er1 C8 K1 99.6(4) . . ? C16 C9 C10 134.0(11) . . ? C16 C9 Er1 74.3(7) . . ? C10 C9 Er1 75.0(7) . . ? C16 C9 K2 76.2(8) . . ? C10 C9 K2 76.5(7) . . ? Er1 C9 K2 100.1(4) . . ? C11 C10 C9 134.2(12) . . ? C11 C10 Er1 73.2(8) . . ? C9 C10 Er1 73.9(7) . . ? C11 C10 K2 78.0(8) . . ? C9 C10 K2 77.4(7) . . ? Er1 C10 K2 100.1(3) . . ? C12 C11 C10 137.4(12) . . ? C12 C11 Er1 76.1(7) . . ? C10 C11 Er1 76.4(8) . . ? C12 C11 K2 77.2(7) . . ? C10 C11 K2 76.6(8) . . ? Er1 C11 K2 100.6(4) . . ? C11 C12 C13 133.6(10) . . ? C11 C12 Er1 73.3(7) . . ? C13 C12 Er1 72.7(7) . . ? C11 C12 K2 77.3(7) . . ? C13 C12 K2 78.4(7) . . ? Er1 C12 K2 99.8(3) . . ? C12 C13 C14 135.9(11) . . ? C12 C13 Er1 76.3(7) . . ? C14 C13 Er1 75.6(7) . . ? C12 C13 K2 75.9(7) . . ? C14 C13 K2 76.4(7) . . ? Er1 C13 K2 100.0(3) . . ? C15 C14 C13 132.7(12) . . ? C15 C14 Er1 74.6(8) . . ? C13 C14 Er1 73.0(7) . . ? C15 C14 K2 74.8(8) . . ? C13 C14 K2 77.8(7) . . ? Er1 C14 K2 99.7(4) . . ? C16 C15 C14 136.6(11) . . ? C16 C15 Er1 74.6(7) . . ? C14 C15 Er1 74.4(7) . . ? C16 C15 K2 77.8(8) . . ? C14 C15 K2 79.2(8) . . ? Er1 C15 K2 101.1(4) . . ? C15 C16 C9 135.1(11) . . ? C15 C16 Er1 74.9(6) . . ? C9 C16 Er1 74.6(7) . . ? C15 C16 K2 76.4(7) . . ? C9 C16 K2 77.7(8) . . ? Er1 C16 K2 100.7(3) . . ? C24 C17 C18 133.9(15) . . ? C24 C17 Er2 75.2(14) . . ? C18 C17 Er2 75.3(13) . . ? C24 C17 K2 77.6(15) . . ? C18 C17 K2 74.7(14) . . ? Er2 C17 K2 101.7(5) . . ? C19 C18 C17 135.2(15) . . ? C19 C18 Er2 73.9(13) . . ? C17 C18 Er2 74.0(13) . . ? C19 C18 K2 79.1(15) . . ? C17 C18 K2 78.4(14) . . ? Er2 C18 K2 102.5(5) . . ? C20 C19 C18 136.2(16) . . ? C20 C19 Er2 76.2(13) . . ? C18 C19 Er2 76.1(12) . . ? C20 C19 K2 78.6(14) . . ? C18 C19 K2 74.8(14) . . ? Er2 C19 K2 101.8(5) . . ? C21 C20 C19 134.6(15) . . ? C21 C20 Er2 74.3(13) . . ? C19 C20 Er2 73.7(13) . . ? C21 C20 K2 79.4(14) . . ? C19 C20 K2 75.5(14) . . ? Er2 C20 K2 100.1(5) . . ? C20 C21 C22 135.3(15) . . ? C20 C21 Er2 75.3(13) . . ? C22 C21 Er2 74.1(12) . . ? C20 C21 K2 74.8(14) . . ? C22 C21 K2 78.6(14) . . ? Er2 C21 K2 99.0(5) . . ? C21 C22 C23 133.5(14) . . ? C21 C22 Er2 75.1(13) . . ? C23 C22 Er2 74.9(13) . . ? C21 C22 K2 75.7(14) . . ? C23 C22 K2 74.5(13) . . ? Er2 C22 K2 98.3(5) . . ? C24 C23 C22 136.1(15) . . ? C24 C23 Er2 75.4(14) . . ? C22 C23 Er2 74.3(13) . . ? C24 C23 K2 75.1(15) . . ? C22 C23 K2 79.7(13) . . ? Er2 C23 K2 99.8(5) . . ? C23 C24 C17 134.8(15) . . ? C23 C24 Er2 74.4(13) . . ? C17 C24 Er2 74.1(14) . . ? C23 C24 K2 79.1(15) . . ? C17 C24 K2 75.9(15) . . ? Er2 C24 K2 100.8(5) . . ? C24' C17' C18' 133.2(15) . . ? C24' C17' Er2 74.7(13) . . ? C18' C17' Er2 72.2(13) . . ? C24' C17' K2 77.8(14) . . ? C18' C17' K2 76.2(14) . . ? Er2 C17' K2 99.6(5) . . ? C19' C18' C17' 136.3(16) . . ? C19' C18' Er2 76.6(15) . . ? C17' C18' Er2 76.8(13) . . ? C19' C18' K2 74.5(16) . . ? C17' C18' K2 77.5(14) . . ? Er2 C18' K2 101.3(5) . . ? C20' C19' C18' 135.4(16) . . ? C20' C19' Er2 74.0(13) . . ? C18' C19' Er2 73.4(14) . . ? C20' C19' K2 78.2(15) . . ? C18' C19' K2 79.7(16) . . ? Er2 C19' K2 102.1(6) . . ? C19' C20' C21' 134.5(15) . . ? C19' C20' Er2 75.8(13) . . ? C21' C20' Er2 75.9(13) . . ? C19' C20' K2 75.6(15) . . ? C21' C20' K2 76.2(14) . . ? Er2 C20' K2 101.7(5) . . ? C22' C21' C20' 135.6(14) . . ? C22' C21' Er2 74.3(13) . . ? C20' C21' Er2 73.4(13) . . ? C22' C21' K2 80.1(14) . . ? C20' C21' K2 77.3(15) . . ? Er2 C21' K2 101.4(5) . . ? C21' C22' C23' 133.0(15) . . ? C21' C22' Er2 75.0(13) . . ? C23' C22' Er2 74.9(14) . . ? C21' C22' K2 73.6(14) . . ? C23' C22' K2 76.8(15) . . ? Er2 C22' K2 99.5(5) . . ? C24' C23' C22' 136.3(15) . . ? C24' C23' Er2 75.4(14) . . ? C22' C23' Er2 74.4(14) . . ? C24' C23' K2 77.5(15) . . ? C22' C23' K2 77.2(15) . . ? Er2 C23' K2 99.5(5) . . ? C23' C24' C17' 135.0(14) . . ? C23' C24' Er2 74.6(13) . . ? C17' C24' Er2 74.8(13) . . ? C23' C24' K2 77.0(14) . . ? C17' C24' K2 76.2(14) . . ? Er2 C24' K2 99.1(5) . . ? C26 C25 C32 133.2(14) . . ? C26 C25 Er2 73.7(8) . . ? C32 C25 Er2 74.1(8) . . ? C27 C26 C25 138.1(16) . . ? C27 C26 Er2 75.6(9) . . ? C25 C26 Er2 75.2(8) . . ? C26 C27 C28 133.7(16) . . ? C26 C27 Er2 73.4(9) . . ? C28 C27 Er2 74.2(8) . . ? C27 C28 C29 135.8(14) . . ? C27 C28 Er2 75.1(8) . . ? C29 C28 Er2 73.9(8) . . ? C30 C29 C28 133.5(14) . . ? C30 C29 Er2 74.9(8) . . ? C28 C29 Er2 74.2(8) . . ? C31 C30 C29 134.9(18) . . ? C31 C30 Er2 74.5(10) . . ? C29 C30 Er2 73.1(8) . . ? C32 C31 C30 136.0(18) . . ? C32 C31 Er2 74.1(9) . . ? C30 C31 Er2 74.8(10) . . ? C31 C32 C25 134.7(14) . . ? C31 C32 Er2 75.2(8) . . ? C25 C32 Er2 74.0(8) . . ? O1 C33 C34 107.3(12) . . ? C35 C34 C33 101.9(12) . . ? C36 C35 C34 103.3(12) . . ? O1 C36 C35 107.4(12) . . ? O2 C37 C38 104.0(15) . . ? C37 C38 C39 105.6(14) . . ? C40 C39 C38 104.7(14) . . ? O2 C40 C39 107.8(15) . . ? O3 C41 C42 105.4(14) . . ? O3 C44 C43 107.2(13) . . ? C42 C43 C44 105.3(13) . . ? C43 C42 C41 110.2(15) . . ? O4 C45 C46 105.7(12) . . ? C46 C47 C48 102.3(13) . . ? O4 C48 C47 109.6(13) . . ? C47 C46 C45 105.4(14) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O4 K1 O1 C36 -104.0(10) . . . . ? O3 K1 O1 C36 116.9(11) . . . . ? O2 K1 O1 C36 -166.8(10) . . . . ? C4 K1 O1 C36 45.7(11) . . . . ? C3 K1 O1 C36 38.8(11) . . . . ? C5 K1 O1 C36 28.0(13) . . . . ? C2 K1 O1 C36 20.1(10) . . . . ? C1 K1 O1 C36 -5.7(10) . . . . ? C6 K1 O1 C36 -16.4(13) . . . . ? C8 K1 O1 C36 -24.8(11) . . . . ? C7 K1 O1 C36 -31.2(11) . . . . ? O4 K1 O1 C33 70.9(11) . . . . ? O3 K1 O1 C33 -68.2(11) . . . . ? O2 K1 O1 C33 8.1(13) . . . . ? C4 K1 O1 C33 -139.4(11) . . . . ? C3 K1 O1 C33 -146.4(11) . . . . ? C5 K1 O1 C33 -157.1(11) . . . . ? C2 K1 O1 C33 -165.0(12) . . . . ? C1 K1 O1 C33 169.1(12) . . . . ? C6 K1 O1 C33 158.5(10) . . . . ? C8 K1 O1 C33 150.1(11) . . . . ? C7 K1 O1 C33 143.7(11) . . . . ? O4 K1 O2 C40 -63.2(12) . . . . ? O1 K1 O2 C40 2.3(14) . . . . ? O3 K1 O2 C40 74.1(12) . . . . ? C4 K1 O2 C40 155.1(12) . . . . ? C3 K1 O2 C40 151.1(11) . . . . ? C5 K1 O2 C40 174.1(12) . . . . ? C2 K1 O2 C40 170.1(11) . . . . ? C1 K1 O2 C40 -145.7(12) . . . . ? C6 K1 O2 C40 -160.7(12) . . . . ? C8 K1 O2 C40 -133.1(12) . . . . ? C7 K1 O2 C40 -140.8(12) . . . . ? O4 K1 O2 C37 131.0(15) . . . . ? O1 K1 O2 C37 -163.5(13) . . . . ? O3 K1 O2 C37 -91.7(14) . . . . ? C4 K1 O2 C37 -10.7(15) . . . . ? C3 K1 O2 C37 -14.7(16) . . . . ? C5 K1 O2 C37 8.3(14) . . . . ? C2 K1 O2 C37 4.3(18) . . . . ? C1 K1 O2 C37 48.5(16) . . . . ? C6 K1 O2 C37 33.5(14) . . . . ? C8 K1 O2 C37 61.0(15) . . . . ? C7 K1 O2 C37 53.4(15) . . . . ? O4 K1 O3 C44 29.5(14) . . . . ? O1 K1 O3 C44 95.1(12) . . . . ? O2 K1 O3 C44 -37.9(12) . . . . ? C4 K1 O3 C44 -138.3(12) . . . . ? C3 K1 O3 C44 -163.7(13) . . . . ? C5 K1 O3 C44 -119.4(12) . . . . ? C2 K1 O3 C44 176.0(12) . . . . ? C1 K1 O3 C44 168.8(11) . . . . ? C6 K1 O3 C44 -115.8(12) . . . . ? C8 K1 O3 C44 -177.5(11) . . . . ? C7 K1 O3 C44 -136.5(12) . . . . ? O4 K1 O3 C41 -122.2(12) . . . . ? O1 K1 O3 C41 -56.6(12) . . . . ? O2 K1 O3 C41 170.5(12) . . . . ? C4 K1 O3 C41 70.1(12) . . . . ? C3 K1 O3 C41 44.7(12) . . . . ? C5 K1 O3 C41 88.9(12) . . . . ? C2 K1 O3 C41 24.4(12) . . . . ? C1 K1 O3 C41 17.1(13) . . . . ? C6 K1 O3 C41 92.5(12) . . . . ? C8 K1 O3 C41 30.9(14) . . . . ? C7 K1 O3 C41 71.9(14) . . . . ? O1 K1 O4 C48 35.3(12) . . . . ? O3 K1 O4 C48 99.2(12) . . . . ? O2 K1 O4 C48 171.6(13) . . . . ? C4 K1 O4 C48 -100.8(13) . . . . ? C3 K1 O4 C48 -58.9(14) . . . . ? C5 K1 O4 C48 -116.4(12) . . . . ? C2 K1 O4 C48 -40.3(13) . . . . ? C1 K1 O4 C48 -45.9(12) . . . . ? C6 K1 O4 C48 -108.9(12) . . . . ? C8 K1 O4 C48 -64.4(12) . . . . ? C7 K1 O4 C48 -88.9(12) . . . . ? O1 K1 O4 C45 176.5(10) . . . . ? O3 K1 O4 C45 -119.6(10) . . . . ? O2 K1 O4 C45 -47.3(10) . . . . ? C4 K1 O4 C45 40.3(13) . . . . ? C3 K1 O4 C45 82.3(12) . . . . ? C5 K1 O4 C45 24.8(11) . . . . ? C2 K1 O4 C45 100.8(10) . . . . ? C1 K1 O4 C45 95.2(10) . . . . ? C6 K1 O4 C45 32.2(10) . . . . ? C8 K1 O4 C45 76.8(10) . . . . ? C7 K1 O4 C45 52.2(10) . . . . ? C3 Er1 C1 C8 -128.1(9) . . . . ? C11 Er1 C1 C8 159.3(7) . . . . ? C13 Er1 C1 C8 12(8) . . . . ? C7 Er1 C1 C8 -18.9(7) . . . . ? C2 Er1 C1 C8 -148.3(12) . . . . ? C6 Er1 C1 C8 -43.8(8) . . . . ? C4 Er1 C1 C8 -104.2(9) . . . . ? C9 Er1 C1 C8 106.5(8) . . . . ? C14 Er1 C1 C8 31.4(11) . . . . ? C16 Er1 C1 C8 76.1(8) . . . . ? C3 Er1 C1 C2 20.2(8) . . . . ? C11 Er1 C1 C2 -52.4(8) . . . . ? C13 Er1 C1 C2 161(8) . . . . ? C7 Er1 C1 C2 129.4(8) . . . . ? C6 Er1 C1 C2 104.5(8) . . . . ? C8 Er1 C1 C2 148.3(12) . . . . ? C4 Er1 C1 C2 44.1(7) . . . . ? C9 Er1 C1 C2 -105.2(8) . . . . ? C14 Er1 C1 C2 179.7(7) . . . . ? C16 Er1 C1 C2 -135.6(8) . . . . ? C3 Er1 C1 K1 -52.2(5) . . . . ? C11 Er1 C1 K1 -124.7(5) . . . . ? C13 Er1 C1 K1 88(8) . . . . ? C7 Er1 C1 K1 57.0(5) . . . . ? C2 Er1 C1 K1 -72.4(7) . . . . ? C6 Er1 C1 K1 32.2(5) . . . . ? C8 Er1 C1 K1 75.9(8) . . . . ? C4 Er1 C1 K1 -28.2(5) . . . . ? C9 Er1 C1 K1 -177.5(5) . . . . ? C14 Er1 C1 K1 107.3(6) . . . . ? C16 Er1 C1 K1 152.0(5) . . . . ? O4 K1 C1 C8 -48.3(8) . . . . ? O1 K1 C1 C8 -129.4(8) . . . . ? O3 K1 C1 C8 159.5(8) . . . . ? O2 K1 C1 C8 26.9(11) . . . . ? C4 K1 C1 C8 97.7(9) . . . . ? C3 K1 C1 C8 121.1(10) . . . . ? C5 K1 C1 C8 70.0(8) . . . . ? C2 K1 C1 C8 142.6(12) . . . . ? C6 K1 C1 C8 43.7(8) . . . . ? C7 K1 C1 C8 20.2(7) . . . . ? O4 K1 C1 C2 169.0(7) . . . . ? O1 K1 C1 C2 88.0(8) . . . . ? O3 K1 C1 C2 16.9(9) . . . . ? O2 K1 C1 C2 -115.7(9) . . . . ? C4 K1 C1 C2 -44.9(7) . . . . ? C3 K1 C1 C2 -21.5(7) . . . . ? C5 K1 C1 C2 -72.7(8) . . . . ? C6 K1 C1 C2 -99.0(8) . . . . ? C8 K1 C1 C2 -142.6(12) . . . . ? C7 K1 C1 C2 -122.4(9) . . . . ? O4 K1 C1 Er1 -120.4(5) . . . . ? O1 K1 C1 Er1 158.6(5) . . . . ? O3 K1 C1 Er1 87.5(5) . . . . ? O2 K1 C1 Er1 -45.1(8) . . . . ? C4 K1 C1 Er1 25.7(4) . . . . ? C3 K1 C1 Er1 49.1(5) . . . . ? C5 K1 C1 Er1 -2.1(4) . . . . ? C2 K1 C1 Er1 70.6(7) . . . . ? C6 K1 C1 Er1 -28.4(4) . . . . ? C8 K1 C1 Er1 -72.1(8) . . . . ? C7 K1 C1 Er1 -51.8(5) . . . . ? C8 C1 C2 C3 -2(3) . . . . ? Er1 C1 C2 C3 -48.9(15) . . . . ? K1 C1 C2 C3 56.8(15) . . . . ? C8 C1 C2 Er1 46.7(16) . . . . ? K1 C1 C2 Er1 105.7(3) . . . . ? C8 C1 C2 K1 -59.0(17) . . . . ? Er1 C1 C2 K1 -105.7(3) . . . . ? C11 Er1 C2 C3 -78.0(9) . . . . ? C13 Er1 C2 C3 -33.7(13) . . . . ? C7 Er1 C2 C3 102.5(10) . . . . ? C6 Er1 C2 C3 72.0(9) . . . . ? C1 Er1 C2 C3 144.5(13) . . . . ? C8 Er1 C2 C3 126.4(10) . . . . ? C4 Er1 C2 C3 17.9(9) . . . . ? C9 Er1 C2 C3 -137.9(9) . . . . ? C14 Er1 C2 C3 140(9) . . . . ? C16 Er1 C2 C3 -162.8(9) . . . . ? C3 Er1 C2 C1 -144.5(13) . . . . ? C11 Er1 C2 C1 137.5(8) . . . . ? C13 Er1 C2 C1 -178.2(8) . . . . ? C7 Er1 C2 C1 -42.0(8) . . . . ? C6 Er1 C2 C1 -72.5(8) . . . . ? C8 Er1 C2 C1 -18.1(8) . . . . ? C4 Er1 C2 C1 -126.5(8) . . . . ? C9 Er1 C2 C1 77.6(8) . . . . ? C14 Er1 C2 C1 -4(10) . . . . ? C16 Er1 C2 C1 52.7(9) . . . . ? C3 Er1 C2 K1 -70.6(9) . . . . ? C11 Er1 C2 K1 -148.6(4) . . . . ? C13 Er1 C2 K1 -104.3(8) . . . . ? C7 Er1 C2 K1 31.9(4) . . . . ? C6 Er1 C2 K1 1.3(5) . . . . ? C1 Er1 C2 K1 73.9(7) . . . . ? C8 Er1 C2 K1 55.7(5) . . . . ? C4 Er1 C2 K1 -52.7(5) . . . . ? C9 Er1 C2 K1 151.5(5) . . . . ? C14 Er1 C2 K1 70(10) . . . . ? C16 Er1 C2 K1 126.6(4) . . . . ? O4 K1 C2 C3 -153.1(8) . . . . ? O1 K1 C2 C3 131.3(9) . . . . ? O3 K1 C2 C3 54.5(9) . . . . ? O2 K1 C2 C3 -39.4(11) . . . . ? C4 K1 C2 C3 -19.2(8) . . . . ? C5 K1 C2 C3 -43.8(8) . . . . ? C1 K1 C2 C3 -140.2(13) . . . . ? C6 K1 C2 C3 -70.4(9) . . . . ? C8 K1 C2 C3 -120.1(10) . . . . ? C7 K1 C2 C3 -97.0(9) . . . . ? O4 K1 C2 C1 -12.9(9) . . . . ? O1 K1 C2 C1 -88.5(8) . . . . ? O3 K1 C2 C1 -165.3(8) . . . . ? O2 K1 C2 C1 100.8(10) . . . . ? C4 K1 C2 C1 121.0(8) . . . . ? C3 K1 C2 C1 140.2(13) . . . . ? C5 K1 C2 C1 96.4(8) . . . . ? C6 K1 C2 C1 69.8(8) . . . . ? C8 K1 C2 C1 20.1(7) . . . . ? C7 K1 C2 C1 43.2(7) . . . . ? O4 K1 C2 Er1 -83.8(5) . . . . ? O1 K1 C2 Er1 -159.4(5) . . . . ? O3 K1 C2 Er1 123.8(4) . . . . ? O2 K1 C2 Er1 29.8(9) . . . . ? C4 K1 C2 Er1 50.1(5) . . . . ? C3 K1 C2 Er1 69.3(8) . . . . ? C5 K1 C2 Er1 25.5(4) . . . . ? C1 K1 C2 Er1 -70.9(7) . . . . ? C6 K1 C2 Er1 -1.2(4) . . . . ? C8 K1 C2 Er1 -50.8(4) . . . . ? C7 K1 C2 Er1 -27.7(4) . . . . ? C1 C2 C3 C4 0(3) . . . . ? Er1 C2 C3 C4 -49.6(19) . . . . ? K1 C2 C3 C4 57.4(19) . . . . ? C1 C2 C3 Er1 49.1(14) . . . . ? K1 C2 C3 Er1 107.0(3) . . . . ? C1 C2 C3 K1 -57.9(14) . . . . ? Er1 C2 C3 K1 -107.0(3) . . . . ? C11 Er1 C3 C4 -105.2(9) . . . . ? C13 Er1 C3 C4 -50.1(10) . . . . ? C7 Er1 C3 C4 74.1(9) . . . . ? C2 Er1 C3 C4 148.7(14) . . . . ? C6 Er1 C3 C4 43.5(9) . . . . ? C1 Er1 C3 C4 127.9(9) . . . . ? C8 Er1 C3 C4 103.7(9) . . . . ? C9 Er1 C3 C4 -161.1(8) . . . . ? C14 Er1 C3 C4 -28.3(14) . . . . ? C16 Er1 C3 C4 177.8(8) . . . . ? C11 Er1 C3 C2 106.1(9) . . . . ? C13 Er1 C3 C2 161.2(8) . . . . ? C7 Er1 C3 C2 -74.6(9) . . . . ? C6 Er1 C3 C2 -105.2(9) . . . . ? C1 Er1 C3 C2 -20.8(8) . . . . ? C8 Er1 C3 C2 -45.0(9) . . . . ? C4 Er1 C3 C2 -148.7(14) . . . . ? C9 Er1 C3 C2 50.2(10) . . . . ? C14 Er1 C3 C2 -177.0(7) . . . . ? C16 Er1 C3 C2 29.1(14) . . . . ? C11 Er1 C3 K1 -178.2(5) . . . . ? C13 Er1 C3 K1 -123.1(5) . . . . ? C7 Er1 C3 K1 1.1(5) . . . . ? C2 Er1 C3 K1 75.7(8) . . . . ? C6 Er1 C3 K1 -29.5(5) . . . . ? C1 Er1 C3 K1 54.9(5) . . . . ? C8 Er1 C3 K1 30.7(5) . . . . ? C4 Er1 C3 K1 -73.0(8) . . . . ? C9 Er1 C3 K1 125.9(5) . . . . ? C14 Er1 C3 K1 -101.3(8) . . . . ? C16 Er1 C3 K1 104.8(8) . . . . ? O4 K1 C3 C4 -105.4(9) . . . . ? O1 K1 C3 C4 166.1(8) . . . . ? O3 K1 C3 C4 90.3(8) . . . . ? O2 K1 C3 C4 9.4(9) . . . . ? C5 K1 C3 C4 -22.0(7) . . . . ? C2 K1 C3 C4 -145.0(13) . . . . ? C1 K1 C3 C4 -122.9(9) . . . . ? C6 K1 C3 C4 -46.4(8) . . . . ? C8 K1 C3 C4 -99.3(8) . . . . ? C7 K1 C3 C4 -73.3(8) . . . . ? O4 K1 C3 C2 39.7(12) . . . . ? O1 K1 C3 C2 -48.9(8) . . . . ? O3 K1 C3 C2 -124.7(9) . . . . ? O2 K1 C3 C2 154.4(8) . . . . ? C4 K1 C3 C2 145.0(13) . . . . ? C5 K1 C3 C2 123.1(9) . . . . ? C1 K1 C3 C2 22.1(7) . . . . ? C6 K1 C3 C2 98.7(8) . . . . ? C8 K1 C3 C2 45.8(8) . . . . ? C7 K1 C3 C2 71.8(8) . . . . ? O4 K1 C3 Er1 -33.0(9) . . . . ? O1 K1 C3 Er1 -121.6(5) . . . . ? O3 K1 C3 Er1 162.6(5) . . . . ? O2 K1 C3 Er1 81.7(6) . . . . ? C4 K1 C3 Er1 72.3(8) . . . . ? C5 K1 C3 Er1 50.3(5) . . . . ? C2 K1 C3 Er1 -72.7(7) . . . . ? C1 K1 C3 Er1 -50.6(5) . . . . ? C6 K1 C3 Er1 26.0(4) . . . . ? C8 K1 C3 Er1 -26.9(4) . . . . ? C7 K1 C3 Er1 -1.0(4) . . . . ? C2 C3 C4 C5 2(3) . . . . ? Er1 C3 C4 C5 -47.1(16) . . . . ? K1 C3 C4 C5 60.6(16) . . . . ? C2 C3 C4 Er1 49.4(19) . . . . ? K1 C3 C4 Er1 107.7(3) . . . . ? C2 C3 C4 K1 -58.2(19) . . . . ? Er1 C3 C4 K1 -107.7(3) . . . . ? C11 Er1 C4 C3 78.7(9) . . . . ? C13 Er1 C4 C3 139.0(9) . . . . ? C7 Er1 C4 C3 -103.0(9) . . . . ? C2 Er1 C4 C3 -18.1(8) . . . . ? C6 Er1 C4 C3 -128.0(10) . . . . ? C1 Er1 C4 C3 -43.4(8) . . . . ? C8 Er1 C4 C3 -73.2(9) . . . . ? C9 Er1 C4 C3 32.0(13) . . . . ? C14 Er1 C4 C3 164.2(8) . . . . ? C16 Er1 C4 C3 -36(14) . . . . ? C3 Er1 C4 C5 147.2(13) . . . . ? C11 Er1 C4 C5 -134.0(8) . . . . ? C13 Er1 C4 C5 -73.8(8) . . . . ? C7 Er1 C4 C5 44.3(9) . . . . ? C2 Er1 C4 C5 129.2(9) . . . . ? C6 Er1 C4 C5 19.2(7) . . . . ? C1 Er1 C4 C5 103.8(9) . . . . ? C8 Er1 C4 C5 74.0(9) . . . . ? C9 Er1 C4 C5 179.2(8) . . . . ? C14 Er1 C4 C5 -48.5(9) . . . . ? C16 Er1 C4 C5 111(14) . . . . ? C3 Er1 C4 K1 72.7(8) . . . . ? C11 Er1 C4 K1 151.4(5) . . . . ? C13 Er1 C4 K1 -148.3(5) . . . . ? C7 Er1 C4 K1 -30.3(5) . . . . ? C2 Er1 C4 K1 54.6(5) . . . . ? C6 Er1 C4 K1 -55.3(5) . . . . ? C1 Er1 C4 K1 29.3(5) . . . . ? C8 Er1 C4 K1 -0.5(6) . . . . ? C9 Er1 C4 K1 104.7(8) . . . . ? C14 Er1 C4 K1 -123.1(5) . . . . ? C16 Er1 C4 K1 36(14) . . . . ? O4 K1 C4 C3 108.6(10) . . . . ? O1 K1 C4 C3 -16.5(9) . . . . ? O3 K1 C4 C3 -85.7(8) . . . . ? O2 K1 C4 C3 -172.2(8) . . . . ? C5 K1 C4 C3 140.8(11) . . . . ? C2 K1 C4 C3 19.1(7) . . . . ? C1 K1 C4 C3 43.5(7) . . . . ? C6 K1 C4 C3 119.5(8) . . . . ? C8 K1 C4 C3 69.8(8) . . . . ? C7 K1 C4 C3 95.5(8) . . . . ? O4 K1 C4 C5 -32.1(10) . . . . ? O1 K1 C4 C5 -157.2(7) . . . . ? O3 K1 C4 C5 133.5(7) . . . . ? O2 K1 C4 C5 47.0(8) . . . . ? C3 K1 C4 C5 -140.8(11) . . . . ? C2 K1 C4 C5 -121.7(8) . . . . ? C1 K1 C4 C5 -97.2(8) . . . . ? C6 K1 C4 C5 -21.2(6) . . . . ? C8 K1 C4 C5 -71.0(7) . . . . ? C7 K1 C4 C5 -45.3(7) . . . . ? O4 K1 C4 Er1 39.3(9) . . . . ? O1 K1 C4 Er1 -85.8(6) . . . . ? O3 K1 C4 Er1 -155.0(6) . . . . ? O2 K1 C4 Er1 118.4(5) . . . . ? C3 K1 C4 Er1 -69.4(7) . . . . ? C5 K1 C4 Er1 71.4(7) . . . . ? C2 K1 C4 Er1 -50.3(4) . . . . ? C1 K1 C4 Er1 -25.8(4) . . . . ? C6 K1 C4 Er1 50.2(5) . . . . ? C8 K1 C4 Er1 0.4(5) . . . . ? C7 K1 C4 Er1 26.1(5) . . . . ? C3 C4 C5 C6 0(3) . . . . ? Er1 C4 C5 C6 -47.1(15) . . . . ? K1 C4 C5 C6 59.6(15) . . . . ? C3 C4 C5 Er1 46.6(16) . . . . ? K1 C4 C5 Er1 106.8(3) . . . . ? C3 C4 C5 K1 -60.1(16) . . . . ? Er1 C4 C5 K1 -106.8(3) . . . . ? C3 Er1 C5 C6 127.7(9) . . . . ? C11 Er1 C5 C6 -158.0(8) . . . . ? C13 Er1 C5 C6 -103.9(8) . . . . ? C7 Er1 C5 C6 19.4(9) . . . . ? C2 Er1 C5 C6 104.3(8) . . . . ? C1 Er1 C5 C6 73.4(9) . . . . ? C8 Er1 C5 C6 43.5(8) . . . . ? C4 Er1 C5 C6 146.3(13) . . . . ? C9 Er1 C5 C6 86(63) . . . . ? C14 Er1 C5 C6 -73.5(8) . . . . ? C16 Er1 C5 C6 -30.1(12) . . . . ? C3 Er1 C5 C4 -18.6(8) . . . . ? C11 Er1 C5 C4 55.7(9) . . . . ? C13 Er1 C5 C4 109.8(8) . . . . ? C7 Er1 C5 C4 -126.9(10) . . . . ? C2 Er1 C5 C4 -42.1(8) . . . . ? C6 Er1 C5 C4 -146.3(13) . . . . ? C1 Er1 C5 C4 -72.9(9) . . . . ? C8 Er1 C5 C4 -102.8(9) . . . . ? C9 Er1 C5 C4 -60(63) . . . . ? C14 Er1 C5 C4 140.2(8) . . . . ? C16 Er1 C5 C4 -176.4(8) . . . . ? C3 Er1 C5 K1 51.9(5) . . . . ? C11 Er1 C5 K1 126.3(5) . . . . ? C13 Er1 C5 K1 -179.7(5) . . . . ? C7 Er1 C5 K1 -56.4(5) . . . . ? C2 Er1 C5 K1 28.5(5) . . . . ? C6 Er1 C5 K1 -75.8(8) . . . . ? C1 Er1 C5 K1 -2.4(5) . . . . ? C8 Er1 C5 K1 -32.3(5) . . . . ? C4 Er1 C5 K1 70.5(8) . . . . ? C9 Er1 C5 K1 10(63) . . . . ? C14 Er1 C5 K1 -149.2(4) . . . . ? C16 Er1 C5 K1 -105.9(8) . . . . ? O4 K1 C5 C6 17.8(9) . . . . ? O1 K1 C5 C6 -104.9(10) . . . . ? O3 K1 C5 C6 172.9(8) . . . . ? O2 K1 C5 C6 86.2(8) . . . . ? C4 K1 C5 C6 -140.5(12) . . . . ? C3 K1 C5 C6 -119.3(9) . . . . ? C2 K1 C5 C6 -96.2(8) . . . . ? C1 K1 C5 C6 -68.9(8) . . . . ? C8 K1 C5 C6 -42.9(7) . . . . ? C7 K1 C5 C6 -20.3(8) . . . . ? O4 K1 C5 C4 158.2(7) . . . . ? O1 K1 C5 C4 35.5(10) . . . . ? O3 K1 C5 C4 -46.6(7) . . . . ? O2 K1 C5 C4 -133.3(8) . . . . ? C3 K1 C5 C4 21.1(6) . . . . ? C2 K1 C5 C4 44.2(7) . . . . ? C1 K1 C5 C4 71.5(7) . . . . ? C6 K1 C5 C4 140.5(12) . . . . ? C8 K1 C5 C4 97.6(8) . . . . ? C7 K1 C5 C4 120.1(8) . . . . ? O4 K1 C5 Er1 88.8(5) . . . . ? O1 K1 C5 Er1 -33.9(9) . . . . ? O3 K1 C5 Er1 -116.1(5) . . . . ? O2 K1 C5 Er1 157.2(5) . . . . ? C4 K1 C5 Er1 -69.5(7) . . . . ? C3 K1 C5 Er1 -48.3(4) . . . . ? C2 K1 C5 Er1 -25.2(4) . . . . ? C1 K1 C5 Er1 2.1(4) . . . . ? C6 K1 C5 Er1 71.0(7) . . . . ? C8 K1 C5 Er1 28.1(4) . . . . ? C7 K1 C5 Er1 50.7(5) . . . . ? C4 C5 C6 C7 -1(3) . . . . ? Er1 C5 C6 C7 -48.1(17) . . . . ? K1 C5 C6 C7 56.8(18) . . . . ? C4 C5 C6 Er1 47.1(15) . . . . ? K1 C5 C6 Er1 104.9(3) . . . . ? C4 C5 C6 K1 -57.8(15) . . . . ? Er1 C5 C6 K1 -104.9(3) . . . . ? C3 Er1 C6 C5 -43.6(8) . . . . ? C11 Er1 C6 C5 37.7(12) . . . . ? C13 Er1 C6 C5 78.7(8) . . . . ? C7 Er1 C6 C5 -146.8(14) . . . . ? C2 Er1 C6 C5 -73.0(9) . . . . ? C1 Er1 C6 C5 -103.5(9) . . . . ? C8 Er1 C6 C5 -127.9(9) . . . . ? C4 Er1 C6 C5 -19.7(8) . . . . ? C9 Er1 C6 C5 -179.1(8) . . . . ? C14 Er1 C6 C5 109.1(8) . . . . ? C16 Er1 C6 C5 162.6(8) . . . . ? C3 Er1 C6 C7 103.2(10) . . . . ? C11 Er1 C6 C7 -175.5(8) . . . . ? C13 Er1 C6 C7 -134.5(9) . . . . ? C2 Er1 C6 C7 73.8(9) . . . . ? C1 Er1 C6 C7 43.3(9) . . . . ? C8 Er1 C6 C7 18.9(9) . . . . ? C4 Er1 C6 C7 127.1(11) . . . . ? C9 Er1 C6 C7 -32.3(14) . . . . ? C14 Er1 C6 C7 -104.1(9) . . . . ? C16 Er1 C6 C7 -50.7(10) . . . . ? C3 Er1 C6 K1 28.1(4) . . . . ? C11 Er1 C6 K1 109.4(7) . . . . ? C13 Er1 C6 K1 150.4(4) . . . . ? C7 Er1 C6 K1 -75.1(9) . . . . ? C2 Er1 C6 K1 -1.3(5) . . . . ? C1 Er1 C6 K1 -31.8(4) . . . . ? C8 Er1 C6 K1 -56.2(4) . . . . ? C4 Er1 C6 K1 52.0(4) . . . . ? C9 Er1 C6 K1 -107.4(8) . . . . ? C14 Er1 C6 K1 -179.2(4) . . . . ? C16 Er1 C6 K1 -125.7(4) . . . . ? O4 K1 C6 C5 -164.5(8) . . . . ? O1 K1 C6 C5 112.1(9) . . . . ? O3 K1 C6 C5 -8.5(9) . . . . ? O2 K1 C6 C5 -90.0(8) . . . . ? C4 K1 C6 C5 22.2(7) . . . . ? C3 K1 C6 C5 46.6(8) . . . . ? C2 K1 C6 C5 73.1(8) . . . . ? C1 K1 C6 C5 100.2(9) . . . . ? C8 K1 C6 C5 123.5(9) . . . . ? C7 K1 C6 C5 142.9(14) . . . . ? O4 K1 C6 C7 52.6(9) . . . . ? O1 K1 C6 C7 -30.8(13) . . . . ? O3 K1 C6 C7 -151.4(8) . . . . ? O2 K1 C6 C7 127.1(10) . . . . ? C4 K1 C6 C7 -120.7(11) . . . . ? C3 K1 C6 C7 -96.3(10) . . . . ? C5 K1 C6 C7 -142.9(14) . . . . ? C2 K1 C6 C7 -69.9(9) . . . . ? C1 K1 C6 C7 -42.7(9) . . . . ? C8 K1 C6 C7 -19.4(8) . . . . ? O4 K1 C6 Er1 123.6(4) . . . . ? O1 K1 C6 Er1 40.2(8) . . . . ? O3 K1 C6 Er1 -80.4(5) . . . . ? O2 K1 C6 Er1 -161.9(5) . . . . ? C4 K1 C6 Er1 -49.7(4) . . . . ? C3 K1 C6 Er1 -25.3(4) . . . . ? C5 K1 C6 Er1 -71.9(8) . . . . ? C2 K1 C6 Er1 1.1(4) . . . . ? C1 K1 C6 Er1 28.3(4) . . . . ? C8 K1 C6 Er1 51.6(5) . . . . ? C7 K1 C6 Er1 71.0(9) . . . . ? C5 C6 C7 C8 -1(3) . . . . ? Er1 C6 C7 C8 -49.2(18) . . . . ? K1 C6 C7 C8 55.1(19) . . . . ? C5 C6 C7 Er1 48.6(17) . . . . ? K1 C6 C7 Er1 104.2(3) . . . . ? C5 C6 C7 K1 -55.6(17) . . . . ? Er1 C6 C7 K1 -104.2(3) . . . . ? C3 Er1 C7 C8 73.1(8) . . . . ? C11 Er1 C7 C8 -123(11) . . . . ? C13 Er1 C7 C8 -159.4(7) . . . . ? C2 Er1 C7 C8 43.3(8) . . . . ? C6 Er1 C7 C8 146.8(14) . . . . ? C1 Er1 C7 C8 19.1(7) . . . . ? C4 Er1 C7 C8 102.7(8) . . . . ? C9 Er1 C7 C8 -51.7(9) . . . . ? C14 Er1 C7 C8 -135.3(8) . . . . ? C16 Er1 C7 C8 -75.5(8) . . . . ? C3 Er1 C7 C6 -73.6(9) . . . . ? C11 Er1 C7 C6 90(11) . . . . ? C13 Er1 C7 C6 53.9(10) . . . . ? C2 Er1 C7 C6 -103.5(9) . . . . ? C1 Er1 C7 C6 -127.7(10) . . . . ? C8 Er1 C7 C6 -146.8(14) . . . . ? C4 Er1 C7 C6 -44.1(9) . . . . ? C9 Er1 C7 C6 161.5(8) . . . . ? C14 Er1 C7 C6 78.0(9) . . . . ? C16 Er1 C7 C6 137.7(9) . . . . ? C3 Er1 C7 K1 -1.1(5) . . . . ? C11 Er1 C7 K1 163(11) . . . . ? C13 Er1 C7 K1 126.5(4) . . . . ? C2 Er1 C7 K1 -30.9(4) . . . . ? C6 Er1 C7 K1 72.6(8) . . . . ? C1 Er1 C7 K1 -55.1(4) . . . . ? C8 Er1 C7 K1 -74.2(8) . . . . ? C4 Er1 C7 K1 28.5(5) . . . . ? C9 Er1 C7 K1 -125.9(5) . . . . ? C14 Er1 C7 K1 150.5(4) . . . . ? C16 Er1 C7 K1 -149.7(5) . . . . ? O4 K1 C7 C8 89.6(8) . . . . ? O1 K1 C7 C8 15.6(9) . . . . ? O3 K1 C7 C8 -100.5(10) . . . . ? O2 K1 C7 C8 163.5(8) . . . . ? C4 K1 C7 C8 -98.5(9) . . . . ? C3 K1 C7 C8 -71.5(8) . . . . ? C5 K1 C7 C8 -123.7(9) . . . . ? C2 K1 C7 C8 -44.8(8) . . . . ? C1 K1 C7 C8 -20.6(8) . . . . ? C6 K1 C7 C8 -143.9(14) . . . . ? O4 K1 C7 C6 -126.5(10) . . . . ? O1 K1 C7 C6 159.5(9) . . . . ? O3 K1 C7 C6 43.4(13) . . . . ? O2 K1 C7 C6 -52.5(9) . . . . ? C4 K1 C7 C6 45.4(9) . . . . ? C3 K1 C7 C6 72.4(9) . . . . ? C5 K1 C7 C6 20.3(8) . . . . ? C2 K1 C7 C6 99.2(10) . . . . ? C1 K1 C7 C6 123.4(11) . . . . ? C8 K1 C7 C6 143.9(14) . . . . ? O4 K1 C7 Er1 162.1(5) . . . . ? O1 K1 C7 Er1 88.0(5) . . . . ? O3 K1 C7 Er1 -28.1(9) . . . . ? O2 K1 C7 Er1 -124.0(5) . . . . ? C4 K1 C7 Er1 -26.0(4) . . . . ? C3 K1 C7 Er1 0.9(4) . . . . ? C5 K1 C7 Er1 -51.2(5) . . . . ? C2 K1 C7 Er1 27.7(4) . . . . ? C1 K1 C7 Er1 51.9(5) . . . . ? C6 K1 C7 Er1 -71.5(8) . . . . ? C8 K1 C7 Er1 72.4(8) . . . . ? C6 C7 C8 C1 1(3) . . . . ? Er1 C7 C8 C1 -47.7(17) . . . . ? K1 C7 C8 C1 56.0(17) . . . . ? C6 C7 C8 Er1 49.0(19) . . . . ? K1 C7 C8 Er1 103.6(3) . . . . ? C6 C7 C8 K1 -54.6(19) . . . . ? Er1 C7 C8 K1 -103.6(3) . . . . ? C2 C1 C8 C7 1(3) . . . . ? Er1 C1 C8 C7 47.5(17) . . . . ? K1 C1 C8 C7 -56.9(17) . . . . ? C2 C1 C8 Er1 -46.5(16) . . . . ? K1 C1 C8 Er1 -104.4(3) . . . . ? C2 C1 C8 K1 57.9(16) . . . . ? Er1 C1 C8 K1 104.4(3) . . . . ? C3 Er1 C8 C7 -103.8(8) . . . . ? C11 Er1 C8 C7 176.0(8) . . . . ? C13 Er1 C8 C7 34.0(11) . . . . ? C2 Er1 C8 C7 -128.4(9) . . . . ? C6 Er1 C8 C7 -19.5(8) . . . . ? C1 Er1 C8 C7 -147.0(12) . . . . ? C4 Er1 C8 C7 -74.4(8) . . . . ? C9 Er1 C8 C7 136.7(8) . . . . ? C14 Er1 C8 C7 52.2(9) . . . . ? C16 Er1 C8 C7 106.8(8) . . . . ? C3 Er1 C8 C1 43.2(8) . . . . ? C11 Er1 C8 C1 -37.0(12) . . . . ? C13 Er1 C8 C1 -179.0(7) . . . . ? C7 Er1 C8 C1 147.0(12) . . . . ? C2 Er1 C8 C1 18.6(7) . . . . ? C6 Er1 C8 C1 127.5(9) . . . . ? C4 Er1 C8 C1 72.6(9) . . . . ? C9 Er1 C8 C1 -76.3(8) . . . . ? C14 Er1 C8 C1 -160.8(7) . . . . ? C16 Er1 C8 C1 -106.2(8) . . . . ? C3 Er1 C8 K1 -29.0(5) . . . . ? C11 Er1 C8 K1 -109.2(7) . . . . ? C13 Er1 C8 K1 108.9(6) . . . . ? C7 Er1 C8 K1 74.9(7) . . . . ? C2 Er1 C8 K1 -53.6(4) . . . . ? C6 Er1 C8 K1 55.4(5) . . . . ? C1 Er1 C8 K1 -72.1(7) . . . . ? C4 Er1 C8 K1 0.5(6) . . . . ? C9 Er1 C8 K1 -148.5(5) . . . . ? C14 Er1 C8 K1 127.1(4) . . . . ? C16 Er1 C8 K1 -178.3(5) . . . . ? O4 K1 C8 C7 -86.1(8) . . . . ? O1 K1 C8 C7 -166.7(8) . . . . ? O3 K1 C8 C7 113.0(9) . . . . ? O2 K1 C8 C7 -18.9(9) . . . . ? C4 K1 C8 C7 71.0(8) . . . . ? C3 K1 C8 C7 97.6(9) . . . . ? C5 K1 C8 C7 43.2(8) . . . . ? C2 K1 C8 C7 121.8(9) . . . . ? C1 K1 C8 C7 142.6(13) . . . . ? C6 K1 C8 C7 20.0(8) . . . . ? O4 K1 C8 C1 131.3(8) . . . . ? O1 K1 C8 C1 50.7(8) . . . . ? O3 K1 C8 C1 -29.7(11) . . . . ? O2 K1 C8 C1 -161.5(8) . . . . ? C4 K1 C8 C1 -71.6(8) . . . . ? C3 K1 C8 C1 -45.0(8) . . . . ? C5 K1 C8 C1 -99.4(9) . . . . ? C2 K1 C8 C1 -20.8(7) . . . . ? C6 K1 C8 C1 -122.6(9) . . . . ? C7 K1 C8 C1 -142.6(13) . . . . ? O4 K1 C8 Er1 -157.6(6) . . . . ? O1 K1 C8 Er1 121.9(5) . . . . ? O3 K1 C8 Er1 41.5(9) . . . . ? O2 K1 C8 Er1 -90.3(6) . . . . ? C4 K1 C8 Er1 -0.4(5) . . . . ? C3 K1 C8 Er1 26.1(5) . . . . ? C5 K1 C8 Er1 -28.2(4) . . . . ? C2 K1 C8 Er1 50.3(5) . . . . ? C1 K1 C8 Er1 71.2(8) . . . . ? C6 K1 C8 Er1 -51.4(5) . . . . ? C7 K1 C8 Er1 -71.5(7) . . . . ? C3 Er1 C9 C16 -158.3(7) . . . . ? C11 Er1 C9 C16 126.9(9) . . . . ? C13 Er1 C9 C16 73.1(8) . . . . ? C7 Er1 C9 C16 -50.5(9) . . . . ? C2 Er1 C9 C16 -135.0(8) . . . . ? C6 Er1 C9 C16 -31.6(12) . . . . ? C1 Er1 C9 C16 -104.2(8) . . . . ? C8 Er1 C9 C16 -74.4(8) . . . . ? C4 Er1 C9 C16 -176.5(8) . . . . ? C14 Er1 C9 C16 42.7(8) . . . . ? C3 Er1 C9 C10 56.3(8) . . . . ? C11 Er1 C9 C10 -18.4(7) . . . . ? C13 Er1 C9 C10 -72.2(8) . . . . ? C7 Er1 C9 C10 164.2(7) . . . . ? C2 Er1 C9 C10 79.6(8) . . . . ? C6 Er1 C9 C10 -176.9(8) . . . . ? C1 Er1 C9 C10 110.4(8) . . . . ? C8 Er1 C9 C10 140.3(8) . . . . ? C4 Er1 C9 C10 38.2(11) . . . . ? C14 Er1 C9 C10 -102.7(7) . . . . ? C16 Er1 C9 C10 -145.4(12) . . . . ? C3 Er1 C9 K2 129.2(5) . . . . ? C11 Er1 C9 K2 54.5(5) . . . . ? C13 Er1 C9 K2 0.7(4) . . . . ? C7 Er1 C9 K2 -122.9(5) . . . . ? C2 Er1 C9 K2 152.6(5) . . . . ? C6 Er1 C9 K2 -104.0(8) . . . . ? C1 Er1 C9 K2 -176.6(5) . . . . ? C8 Er1 C9 K2 -146.8(5) . . . . ? C4 Er1 C9 K2 111.1(7) . . . . ? C14 Er1 C9 K2 -29.7(4) . . . . ? C16 Er1 C9 K2 -72.4(7) . . . . ? C18 K2 C9 C16 149.4(10) . . . . ? C19' K2 C9 C16 160.9(9) . . . . ? C17 K2 C9 C16 122.6(10) . . . . ? C21' K2 C9 C16 174(2) . . . . ? C24 K2 C9 C16 95.9(9) . . . . ? C19 K2 C9 C16 169.9(9) . . . . ? C20' K2 C9 C16 177.4(9) . . . . ? C20 K2 C9 C16 -177.1(10) . . . . ? C15 K2 C9 C16 -20.3(6) . . . . ? C18' K2 C9 C16 137.3(10) . . . . ? C17' K2 C9 C16 110.4(10) . . . . ? C18 K2 C9 C10 -68.0(10) . . . . ? C19' K2 C9 C10 -56.5(10) . . . . ? C17 K2 C9 C10 -94.8(10) . . . . ? C21' K2 C9 C10 -43(3) . . . . ? C24 K2 C9 C10 -121.5(10) . . . . ? C19 K2 C9 C10 -47.5(10) . . . . ? C20' K2 C9 C10 -40.0(11) . . . . ? C20 K2 C9 C10 -34.5(13) . . . . ? C15 K2 C9 C10 122.3(8) . . . . ? C18' K2 C9 C10 -80.1(10) . . . . ? C16 K2 C9 C10 142.6(11) . . . . ? C17' K2 C9 C10 -107.0(10) . . . . ? C18 K2 C9 Er1 -139.7(8) . . . . ? C19' K2 C9 Er1 -128.2(7) . . . . ? C17 K2 C9 Er1 -166.5(8) . . . . ? C21' K2 C9 Er1 -115(2) . . . . ? C24 K2 C9 Er1 166.8(8) . . . . ? C19 K2 C9 Er1 -119.3(8) . . . . ? C20' K2 C9 Er1 -111.7(8) . . . . ? C20 K2 C9 Er1 -106.2(10) . . . . ? C15 K2 C9 Er1 50.6(4) . . . . ? C18' K2 C9 Er1 -151.8(8) . . . . ? C16 K2 C9 Er1 70.9(7) . . . . ? C17' K2 C9 Er1 -178.7(8) . . . . ? C16 C9 C10 C11 -4(3) . . . . ? Er1 C9 C10 C11 45.5(15) . . . . ? K2 C9 C10 C11 -59.0(16) . . . . ? C16 C9 C10 Er1 -49.5(15) . . . . ? K2 C9 C10 Er1 -104.6(3) . . . . ? C16 C9 C10 K2 55.1(16) . . . . ? Er1 C9 C10 K2 104.6(3) . . . . ? C3 Er1 C10 C11 79.2(8) . . . . ? C13 Er1 C10 C11 -42.9(8) . . . . ? C7 Er1 C10 C11 -175.4(8) . . . . ? C2 Er1 C10 C11 108.8(8) . . . . ? C6 Er1 C10 C11 -46(16) . . . . ? C1 Er1 C10 C11 139.4(8) . . . . ? C8 Er1 C10 C11 164.2(8) . . . . ? C4 Er1 C10 C11 54.6(9) . . . . ? C9 Er1 C10 C11 -147.7(12) . . . . ? C14 Er1 C10 C11 -73.3(8) . . . . ? C16 Er1 C10 C11 -127.7(9) . . . . ? C3 Er1 C10 C9 -133.1(8) . . . . ? C11 Er1 C10 C9 147.7(12) . . . . ? C13 Er1 C10 C9 104.8(8) . . . . ? C7 Er1 C10 C9 -27.7(11) . . . . ? C2 Er1 C10 C9 -103.5(8) . . . . ? C6 Er1 C10 C9 102(16) . . . . ? C1 Er1 C10 C9 -72.9(8) . . . . ? C8 Er1 C10 C9 -48.1(9) . . . . ? C4 Er1 C10 C9 -157.7(7) . . . . ? C14 Er1 C10 C9 74.4(8) . . . . ? C16 Er1 C10 C9 20.0(7) . . . . ? C3 Er1 C10 K2 153.2(5) . . . . ? C11 Er1 C10 K2 74.1(8) . . . . ? C13 Er1 C10 K2 31.2(4) . . . . ? C7 Er1 C10 K2 -101.3(8) . . . . ? C2 Er1 C10 K2 -177.1(5) . . . . ? C6 Er1 C10 K2 28(16) . . . . ? C1 Er1 C10 K2 -146.6(4) . . . . ? C8 Er1 C10 K2 -121.8(5) . . . . ? C4 Er1 C10 K2 128.7(5) . . . . ? C9 Er1 C10 K2 -73.6(7) . . . . ? C14 Er1 C10 K2 0.8(4) . . . . ? C16 Er1 C10 K2 -53.6(4) . . . . ? C18 K2 C10 C11 -101.0(10) . . . . ? C19' K2 C10 C11 -87.7(10) . . . . ? C17 K2 C10 C11 -128.1(11) . . . . ? C21' K2 C10 C11 -53.2(12) . . . . ? C24 K2 C10 C11 -149.8(10) . . . . ? C19 K2 C10 C11 -76.6(10) . . . . ? C20' K2 C10 C11 -66.4(10) . . . . ? C20 K2 C10 C11 -58.3(10) . . . . ? C15 K2 C10 C11 96.7(8) . . . . ? C18' K2 C10 C11 -113.7(10) . . . . ? C16 K2 C10 C11 120.4(9) . . . . ? C17' K2 C10 C11 -138.9(10) . . . . ? C18 K2 C10 C9 117.9(10) . . . . ? C19' K2 C10 C9 131.2(10) . . . . ? C17 K2 C10 C9 90.9(10) . . . . ? C21' K2 C10 C9 165.7(9) . . . . ? C24 K2 C10 C9 69.1(10) . . . . ? C19 K2 C10 C9 142.4(9) . . . . ? C20' K2 C10 C9 152.5(9) . . . . ? C20 K2 C10 C9 160.6(8) . . . . ? C15 K2 C10 C9 -44.4(7) . . . . ? C18' K2 C10 C9 105.3(10) . . . . ? C16 K2 C10 C9 -20.6(7) . . . . ? C17' K2 C10 C9 80.0(9) . . . . ? C18 K2 C10 Er1 -171.3(8) . . . . ? C19' K2 C10 Er1 -157.9(8) . . . . ? C17 K2 C10 Er1 161.7(8) . . . . ? C21' K2 C10 Er1 -123.5(7) . . . . ? C24 K2 C10 Er1 139.9(7) . . . . ? C19 K2 C10 Er1 -146.8(7) . . . . ? C20' K2 C10 Er1 -136.6(7) . . . . ? C20 K2 C10 Er1 -128.5(7) . . . . ? C15 K2 C10 Er1 26.5(4) . . . . ? C18' K2 C10 Er1 176.1(8) . . . . ? C16 K2 C10 Er1 50.2(4) . . . . ? C17' K2 C10 Er1 150.9(8) . . . . ? C9 C10 C11 C12 5(3) . . . . ? Er1 C10 C11 C12 51.1(18) . . . . ? K2 C10 C11 C12 -53.5(18) . . . . ? C9 C10 C11 Er1 -45.8(15) . . . . ? K2 C10 C11 Er1 -104.6(3) . . . . ? C9 C10 C11 K2 58.8(15) . . . . ? Er1 C10 C11 K2 104.6(3) . . . . ? C3 Er1 C11 C12 108.1(8) . . . . ? C13 Er1 C11 C12 -18.6(7) . . . . ? C7 Er1 C11 C12 -56(11) . . . . ? C2 Er1 C11 C12 138.0(7) . . . . ? C6 Er1 C11 C12 30.7(12) . . . . ? C1 Er1 C11 C12 163.1(7) . . . . ? C8 Er1 C11 C12 -175.3(7) . . . . ? C4 Er1 C11 C12 78.3(8) . . . . ? C9 Er1 C11 C12 -128.4(9) . . . . ? C14 Er1 C11 C12 -43.4(7) . . . . ? C16 Er1 C11 C12 -103.5(8) . . . . ? C3 Er1 C11 C10 -104.7(8) . . . . ? C13 Er1 C11 C10 128.6(9) . . . . ? C7 Er1 C11 C10 91(11) . . . . ? C2 Er1 C11 C10 -74.8(8) . . . . ? C6 Er1 C11 C10 177.8(7) . . . . ? C1 Er1 C11 C10 -49.7(9) . . . . ? C8 Er1 C11 C10 -28.1(12) . . . . ? C4 Er1 C11 C10 -134.6(8) . . . . ? C9 Er1 C11 C10 18.8(7) . . . . ? C14 Er1 C11 C10 103.8(8) . . . . ? C16 Er1 C11 C10 43.6(8) . . . . ? C3 Er1 C11 K2 -178.0(5) . . . . ? C13 Er1 C11 K2 55.3(4) . . . . ? C7 Er1 C11 K2 18(11) . . . . ? C2 Er1 C11 K2 -148.1(4) . . . . ? C6 Er1 C11 K2 104.6(7) . . . . ? C1 Er1 C11 K2 -123.0(4) . . . . ? C8 Er1 C11 K2 -101.4(8) . . . . ? C4 Er1 C11 K2 152.2(5) . . . . ? C9 Er1 C11 K2 -54.5(5) . . . . ? C14 Er1 C11 K2 30.5(4) . . . . ? C16 Er1 C11 K2 -29.6(4) . . . . ? C18 K2 C11 C12 -130.4(10) . . . . ? C19' K2 C11 C12 -116.6(10) . . . . ? C17 K2 C11 C12 -154.3(9) . . . . ? C21' K2 C11 C12 -69.2(10) . . . . ? C24 K2 C11 C12 -170.8(9) . . . . ? C19 K2 C11 C12 -103.6(10) . . . . ? C20' K2 C11 C12 -90.6(10) . . . . ? C20 K2 C11 C12 -79.5(10) . . . . ? C15 K2 C11 C12 72.9(7) . . . . ? C18' K2 C11 C12 -141.8(10) . . . . ? C16 K2 C11 C12 99.9(8) . . . . ? C17' K2 C11 C12 -163.2(9) . . . . ? C18 K2 C11 C10 83.5(10) . . . . ? C19' K2 C11 C10 97.3(11) . . . . ? C17 K2 C11 C10 59.6(11) . . . . ? C21' K2 C11 C10 144.7(9) . . . . ? C24 K2 C11 C10 43.1(12) . . . . ? C19 K2 C11 C10 110.3(10) . . . . ? C20' K2 C11 C10 123.3(10) . . . . ? C20 K2 C11 C10 134.4(10) . . . . ? C15 K2 C11 C10 -73.2(8) . . . . ? C18' K2 C11 C10 72.1(10) . . . . ? C16 K2 C11 C10 -46.2(8) . . . . ? C17' K2 C11 C10 50.7(11) . . . . ? C18 K2 C11 Er1 156.6(8) . . . . ? C19' K2 C11 Er1 170.4(8) . . . . ? C17 K2 C11 Er1 132.7(8) . . . . ? C21' K2 C11 Er1 -142.3(7) . . . . ? C24 K2 C11 Er1 116.2(8) . . . . ? C19 K2 C11 Er1 -176.7(8) . . . . ? C20' K2 C11 Er1 -163.7(8) . . . . ? C20 K2 C11 Er1 -152.6(7) . . . . ? C15 K2 C11 Er1 -0.1(4) . . . . ? C18' K2 C11 Er1 145.1(8) . . . . ? C16 K2 C11 Er1 26.9(4) . . . . ? C17' K2 C11 Er1 123.8(8) . . . . ? C10 C11 C12 C13 -7(3) . . . . ? Er1 C11 C12 C13 44.3(15) . . . . ? K2 C11 C12 C13 -60.1(15) . . . . ? C10 C11 C12 Er1 -51.2(18) . . . . ? K2 C11 C12 Er1 -104.4(3) . . . . ? C10 C11 C12 K2 53.3(19) . . . . ? Er1 C11 C12 K2 104.4(3) . . . . ? C3 Er1 C12 C11 -76.2(8) . . . . ? C13 Er1 C12 C11 148.0(11) . . . . ? C7 Er1 C12 C11 176.3(7) . . . . ? C2 Er1 C12 C11 -51.2(8) . . . . ? C6 Er1 C12 C11 -162.0(7) . . . . ? C1 Er1 C12 C11 -30.6(11) . . . . ? C8 Er1 C12 C11 119(9) . . . . ? C4 Er1 C12 C11 -105.6(8) . . . . ? C9 Er1 C12 C11 43.0(8) . . . . ? C14 Er1 C12 C11 128.1(8) . . . . ? C16 Er1 C12 C11 73.3(8) . . . . ? C3 Er1 C12 C13 135.7(7) . . . . ? C11 Er1 C12 C13 -148.0(11) . . . . ? C7 Er1 C12 C13 28.3(11) . . . . ? C2 Er1 C12 C13 160.7(7) . . . . ? C6 Er1 C12 C13 50.0(8) . . . . ? C1 Er1 C12 C13 -178.7(7) . . . . ? C8 Er1 C12 C13 -29(10) . . . . ? C4 Er1 C12 C13 106.4(8) . . . . ? C9 Er1 C12 C13 -105.0(7) . . . . ? C14 Er1 C12 C13 -19.9(6) . . . . ? C16 Er1 C12 C13 -74.8(8) . . . . ? C3 Er1 C12 K2 -149.7(5) . . . . ? C11 Er1 C12 K2 -73.5(7) . . . . ? C13 Er1 C12 K2 74.5(7) . . . . ? C7 Er1 C12 K2 102.8(7) . . . . ? C2 Er1 C12 K2 -124.7(4) . . . . ? C6 Er1 C12 K2 124.5(4) . . . . ? C1 Er1 C12 K2 -104.1(7) . . . . ? C8 Er1 C12 K2 45(10) . . . . ? C4 Er1 C12 K2 -179.1(5) . . . . ? C9 Er1 C12 K2 -30.5(5) . . . . ? C14 Er1 C12 K2 54.6(4) . . . . ? C16 Er1 C12 K2 -0.3(5) . . . . ? C18 K2 C12 C11 57.1(10) . . . . ? C19' K2 C12 C11 69.8(10) . . . . ? C17 K2 C12 C11 36.1(11) . . . . ? C21' K2 C12 C11 123.8(10) . . . . ? C24 K2 C12 C11 23(2) . . . . ? C19 K2 C12 C11 82.7(10) . . . . ? C20' K2 C12 C11 96.9(10) . . . . ? C20 K2 C12 C11 109.8(10) . . . . ? C15 K2 C12 C11 -97.0(8) . . . . ? C18' K2 C12 C11 47.2(10) . . . . ? C16 K2 C12 C11 -70.0(8) . . . . ? C17' K2 C12 C11 27.7(13) . . . . ? C18 K2 C12 C13 -162.8(10) . . . . ? C19' K2 C12 C13 -150.0(10) . . . . ? C17 K2 C12 C13 176.3(10) . . . . ? C21' K2 C12 C13 -96.1(10) . . . . ? C24 K2 C12 C13 163.4(17) . . . . ? C19 K2 C12 C13 -137.1(10) . . . . ? C20' K2 C12 C13 -123.0(10) . . . . ? C20 K2 C12 C13 -110.1(10) . . . . ? C15 K2 C12 C13 43.2(7) . . . . ? C18' K2 C12 C13 -172.6(9) . . . . ? C16 K2 C12 C13 70.1(7) . . . . ? C17' K2 C12 C13 167.8(11) . . . . ? C18 K2 C12 Er1 127.3(8) . . . . ? C19' K2 C12 Er1 140.1(8) . . . . ? C17 K2 C12 Er1 106.4(9) . . . . ? C21' K2 C12 Er1 -166.0(8) . . . . ? C24 K2 C12 Er1 93.5(18) . . . . ? C19 K2 C12 Er1 153.0(8) . . . . ? C20' K2 C12 Er1 167.1(8) . . . . ? C20 K2 C12 Er1 -180.0(7) . . . . ? C15 K2 C12 Er1 -26.7(4) . . . . ? C18' K2 C12 Er1 117.5(8) . . . . ? C16 K2 C12 Er1 0.2(4) . . . . ? C17' K2 C12 Er1 97.9(10) . . . . ? C11 C12 C13 C14 7(3) . . . . ? Er1 C12 C13 C14 51.6(15) . . . . ? K2 C12 C13 C14 -52.6(16) . . . . ? C11 C12 C13 Er1 -44.5(15) . . . . ? K2 C12 C13 Er1 -104.2(3) . . . . ? C11 C12 C13 K2 59.7(15) . . . . ? Er1 C12 C13 K2 104.2(3) . . . . ? C3 Er1 C13 C12 -54.4(8) . . . . ? C11 Er1 C13 C12 18.3(6) . . . . ? C7 Er1 C13 C12 -163.3(7) . . . . ? C2 Er1 C13 C12 -34.7(11) . . . . ? C6 Er1 C13 C12 -138.0(7) . . . . ? C1 Er1 C13 C12 166(8) . . . . ? C8 Er1 C13 C12 177.7(7) . . . . ? C4 Er1 C13 C12 -77.7(8) . . . . ? C9 Er1 C13 C12 72.0(7) . . . . ? C14 Er1 C13 C12 145.8(11) . . . . ? C16 Er1 C13 C12 102.1(8) . . . . ? C3 Er1 C13 C14 159.8(7) . . . . ? C11 Er1 C13 C14 -127.4(8) . . . . ? C7 Er1 C13 C14 50.9(8) . . . . ? C2 Er1 C13 C14 179.5(7) . . . . ? C6 Er1 C13 C14 76.2(8) . . . . ? C1 Er1 C13 C14 20(8) . . . . ? C8 Er1 C13 C14 31.9(11) . . . . ? C4 Er1 C13 C14 136.5(8) . . . . ? C9 Er1 C13 C14 -73.8(7) . . . . ? C16 Er1 C13 C14 -43.6(7) . . . . ? C3 Er1 C13 K2 -127.1(5) . . . . ? C11 Er1 C13 K2 -54.4(4) . . . . ? C7 Er1 C13 K2 124.0(4) . . . . ? C2 Er1 C13 K2 -107.4(7) . . . . ? C6 Er1 C13 K2 149.3(4) . . . . ? C1 Er1 C13 K2 93(8) . . . . ? C8 Er1 C13 K2 105.0(7) . . . . ? C4 Er1 C13 K2 -150.4(5) . . . . ? C9 Er1 C13 K2 -0.7(4) . . . . ? C14 Er1 C13 K2 73.1(7) . . . . ? C16 Er1 C13 K2 29.4(4) . . . . ? C18 K2 C13 C12 25.0(13) . . . . ? C19' K2 C13 C12 38.8(12) . . . . ? C17 K2 C13 C12 -9(3) . . . . ? C21' K2 C13 C12 95.3(11) . . . . ? C24 K2 C13 C12 -159(3) . . . . ? C19 K2 C13 C12 51.9(11) . . . . ? C20' K2 C13 C12 66.2(11) . . . . ? C20 K2 C13 C12 79.3(10) . . . . ? C15 K2 C13 C12 -123.9(9) . . . . ? C18' K2 C13 C12 12.7(15) . . . . ? C16 K2 C13 C12 -99.8(8) . . . . ? C17' K2 C13 C12 -57(6) . . . . ? C18 K2 C13 C14 170.4(10) . . . . ? C19' K2 C13 C14 -175.9(11) . . . . ? C17 K2 C13 C14 136(2) . . . . ? C21' K2 C13 C14 -119.3(10) . . . . ? C24 K2 C13 C14 -14(3) . . . . ? C19 K2 C13 C14 -162.8(10) . . . . ? C20' K2 C13 C14 -148.4(10) . . . . ? C20 K2 C13 C14 -135.3(10) . . . . ? C15 K2 C13 C14 21.5(7) . . . . ? C18' K2 C13 C14 158.0(13) . . . . ? C16 K2 C13 C14 45.6(7) . . . . ? C17' K2 C13 C14 88(6) . . . . ? C18 K2 C13 Er1 97.9(10) . . . . ? C19' K2 C13 Er1 111.7(10) . . . . ? C17 K2 C13 Er1 64(2) . . . . ? C21' K2 C13 Er1 168.3(8) . . . . ? C24 K2 C13 Er1 -86(3) . . . . ? C19 K2 C13 Er1 124.8(9) . . . . ? C20' K2 C13 Er1 139.2(9) . . . . ? C20 K2 C13 Er1 152.3(8) . . . . ? C15 K2 C13 Er1 -50.9(4) . . . . ? C18' K2 C13 Er1 85.6(12) . . . . ? C16 K2 C13 Er1 -26.8(4) . . . . ? C17' K2 C13 Er1 16(6) . . . . ? C12 C13 C14 C15 -3(3) . . . . ? Er1 C13 C14 C15 48.7(15) . . . . ? K2 C13 C14 C15 -55.6(15) . . . . ? C12 C13 C14 Er1 -51.8(15) . . . . ? K2 C13 C14 Er1 -104.3(3) . . . . ? C12 C13 C14 K2 52.4(16) . . . . ? Er1 C13 C14 K2 104.3(3) . . . . ? C3 Er1 C14 C15 178.2(8) . . . . ? C11 Er1 C14 C15 -101.5(9) . . . . ? C13 Er1 C14 C15 -145.1(12) . . . . ? C7 Er1 C14 C15 78.0(9) . . . . ? C2 Er1 C14 C15 41(10) . . . . ? C6 Er1 C14 C15 108.8(9) . . . . ? C1 Er1 C14 C15 36.5(12) . . . . ? C8 Er1 C14 C15 54.1(10) . . . . ? C4 Er1 C14 C15 161.6(8) . . . . ? C9 Er1 C14 C15 -41.7(8) . . . . ? C16 Er1 C14 C15 -17.6(8) . . . . ? C3 Er1 C14 C13 -36.7(12) . . . . ? C11 Er1 C14 C13 43.7(7) . . . . ? C7 Er1 C14 C13 -136.9(7) . . . . ? C2 Er1 C14 C13 -174(9) . . . . ? C6 Er1 C14 C13 -106.1(8) . . . . ? C1 Er1 C14 C13 -178.3(7) . . . . ? C8 Er1 C14 C13 -160.8(7) . . . . ? C4 Er1 C14 C13 -53.3(9) . . . . ? C9 Er1 C14 C13 103.4(7) . . . . ? C16 Er1 C14 C13 127.5(8) . . . . ? C3 Er1 C14 K2 -110.7(8) . . . . ? C11 Er1 C14 K2 -30.3(4) . . . . ? C13 Er1 C14 K2 -73.9(7) . . . . ? C7 Er1 C14 K2 149.2(4) . . . . ? C2 Er1 C14 K2 112(9) . . . . ? C6 Er1 C14 K2 180.0(4) . . . . ? C1 Er1 C14 K2 107.7(7) . . . . ? C8 Er1 C14 K2 125.3(4) . . . . ? C4 Er1 C14 K2 -127.2(4) . . . . ? C9 Er1 C14 K2 29.5(4) . . . . ? C16 Er1 C14 K2 53.6(4) . . . . ? C18 K2 C14 C15 115(3) . . . . ? C19' K2 C14 C15 149.1(18) . . . . ? C17 K2 C14 C15 -2(2) . . . . ? C21' K2 C14 C15 -144.9(11) . . . . ? C24 K2 C14 C15 -43.5(13) . . . . ? C19 K2 C14 C15 168.7(13) . . . . ? C20' K2 C14 C15 -174.6(11) . . . . ? C20 K2 C14 C15 -161.3(11) . . . . ? C18' K2 C14 C15 53(5) . . . . ? C16 K2 C14 C15 20.3(7) . . . . ? C17' K2 C14 C15 -22.9(17) . . . . ? C18 K2 C14 C13 -26(3) . . . . ? C19' K2 C14 C13 8(2) . . . . ? C17 K2 C14 C13 -143(2) . . . . ? C21' K2 C14 C13 74.0(11) . . . . ? C24 K2 C14 C13 175.4(11) . . . . ? C19 K2 C14 C13 27.6(14) . . . . ? C20' K2 C14 C13 44.3(12) . . . . ? C20 K2 C14 C13 57.6(11) . . . . ? C15 K2 C14 C13 -141.1(11) . . . . ? C18' K2 C14 C13 -88(5) . . . . ? C16 K2 C14 C13 -120.7(8) . . . . ? C17' K2 C14 C13 -164.0(14) . . . . ? C18 K2 C14 Er1 44(3) . . . . ? C19' K2 C14 Er1 78.1(18) . . . . ? C17 K2 C14 Er1 -73(2) . . . . ? C21' K2 C14 Er1 144.1(9) . . . . ? C24 K2 C14 Er1 -114.5(10) . . . . ? C19 K2 C14 Er1 97.7(12) . . . . ? C20' K2 C14 Er1 114.4(10) . . . . ? C20 K2 C14 Er1 127.7(9) . . . . ? C15 K2 C14 Er1 -71.0(7) . . . . ? C18' K2 C14 Er1 -18(5) . . . . ? C16 K2 C14 Er1 -50.7(4) . . . . ? C17' K2 C14 Er1 -93.9(14) . . . . ? C13 C14 C15 C16 -2(3) . . . . ? Er1 C14 C15 C16 45.7(17) . . . . ? K2 C14 C15 C16 -59.1(18) . . . . ? C13 C14 C15 Er1 -48.1(15) . . . . ? K2 C14 C15 Er1 -104.8(3) . . . . ? C13 C14 C15 K2 56.7(15) . . . . ? Er1 C14 C15 K2 104.8(3) . . . . ? C3 Er1 C15 C16 53(11) . . . . ? C11 Er1 C15 C16 -74.1(8) . . . . ? C13 Er1 C15 C16 -129.0(8) . . . . ? C7 Er1 C15 C16 106.6(8) . . . . ? C2 Er1 C15 C16 33.4(11) . . . . ? C6 Er1 C15 C16 136.9(8) . . . . ? C1 Er1 C15 C16 52.9(9) . . . . ? C8 Er1 C15 C16 76.9(8) . . . . ? C4 Er1 C15 C16 177.5(8) . . . . ? C9 Er1 C15 C16 -19.4(7) . . . . ? C14 Er1 C15 C16 -149.3(13) . . . . ? C3 Er1 C15 C14 -158(11) . . . . ? C11 Er1 C15 C14 75.2(8) . . . . ? C13 Er1 C15 C14 20.3(7) . . . . ? C7 Er1 C15 C14 -104.0(9) . . . . ? C2 Er1 C15 C14 -177.3(7) . . . . ? C6 Er1 C15 C14 -73.8(9) . . . . ? C1 Er1 C15 C14 -157.7(8) . . . . ? C8 Er1 C15 C14 -133.8(9) . . . . ? C4 Er1 C15 C14 -33.2(13) . . . . ? C9 Er1 C15 C14 129.9(9) . . . . ? C16 Er1 C15 C14 149.3(13) . . . . ? C3 Er1 C15 K2 127(11) . . . . ? C11 Er1 C15 K2 -0.1(4) . . . . ? C13 Er1 C15 K2 -55.1(4) . . . . ? C7 Er1 C15 K2 -179.4(5) . . . . ? C2 Er1 C15 K2 107.3(7) . . . . ? C6 Er1 C15 K2 -149.2(4) . . . . ? C1 Er1 C15 K2 126.9(5) . . . . ? C8 Er1 C15 K2 150.8(5) . . . . ? C4 Er1 C15 K2 -108.6(8) . . . . ? C9 Er1 C15 K2 54.5(4) . . . . ? C14 Er1 C15 K2 -75.4(8) . . . . ? C16 Er1 C15 K2 73.9(7) . . . . ? C18 K2 C15 C16 -4.5(18) . . . . ? C19' K2 C15 C16 25(3) . . . . ? C17 K2 C15 C16 -37.9(12) . . . . ? C21' K2 C15 C16 -164.6(11) . . . . ? C24 K2 C15 C16 -66.5(10) . . . . ? C19 K2 C15 C16 96(6) . . . . ? C20' K2 C15 C16 156(2) . . . . ? C20 K2 C15 C16 176.8(13) . . . . ? C18' K2 C15 C16 -22.1(14) . . . . ? C17' K2 C15 C16 -50.1(11) . . . . ? C18 K2 C15 C14 -147.4(16) . . . . ? C19' K2 C15 C14 -118(3) . . . . ? C17 K2 C15 C14 179.2(11) . . . . ? C21' K2 C15 C14 52.5(13) . . . . ? C24 K2 C15 C14 150.6(10) . . . . ? C19 K2 C15 C14 -47(6) . . . . ? C20' K2 C15 C14 13(3) . . . . ? C20 K2 C15 C14 33.8(16) . . . . ? C18' K2 C15 C14 -165.0(12) . . . . ? C16 K2 C15 C14 -142.9(11) . . . . ? C17' K2 C15 C14 167.0(10) . . . . ? C18 K2 C15 Er1 -75.9(16) . . . . ? C19' K2 C15 Er1 -46(3) . . . . ? C17 K2 C15 Er1 -109.3(10) . . . . ? C21' K2 C15 Er1 124.0(10) . . . . ? C24 K2 C15 Er1 -137.9(8) . . . . ? C19 K2 C15 Er1 25(6) . . . . ? C20' K2 C15 Er1 85(2) . . . . ? C20 K2 C15 Er1 105.4(13) . . . . ? C18' K2 C15 Er1 -93.4(11) . . . . ? C16 K2 C15 Er1 -71.4(7) . . . . ? C17' K2 C15 Er1 -121.4(9) . . . . ? C14 C15 C16 C9 3(3) . . . . ? Er1 C15 C16 C9 48.7(16) . . . . ? K2 C15 C16 C9 -56.6(16) . . . . ? C14 C15 C16 Er1 -45.7(18) . . . . ? K2 C15 C16 Er1 -105.3(3) . . . . ? C14 C15 C16 K2 59.6(18) . . . . ? Er1 C15 C16 K2 105.3(3) . . . . ? C10 C9 C16 C15 1(3) . . . . ? Er1 C9 C16 C15 -48.8(16) . . . . ? K2 C9 C16 C15 56.1(16) . . . . ? C10 C9 C16 Er1 49.7(15) . . . . ? K2 C9 C16 Er1 104.9(3) . . . . ? C10 C9 C16 K2 -55.2(15) . . . . ? Er1 C9 C16 K2 -104.9(3) . . . . ? C3 Er1 C16 C15 -176.5(8) . . . . ? C11 Er1 C16 C15 102.5(8) . . . . ? C13 Er1 C16 C15 42.6(7) . . . . ? C7 Er1 C16 C15 -75.7(8) . . . . ? C2 Er1 C16 C15 -160.0(7) . . . . ? C6 Er1 C16 C15 -51.5(9) . . . . ? C1 Er1 C16 C15 -135.0(8) . . . . ? C8 Er1 C16 C15 -105.2(8) . . . . ? C4 Er1 C16 C15 -142(14) . . . . ? C9 Er1 C16 C15 146.6(12) . . . . ? C14 Er1 C16 C15 17.8(7) . . . . ? C3 Er1 C16 C9 36.9(12) . . . . ? C11 Er1 C16 C9 -44.1(8) . . . . ? C13 Er1 C16 C9 -104.0(8) . . . . ? C7 Er1 C16 C9 137.7(8) . . . . ? C2 Er1 C16 C9 53.4(9) . . . . ? C6 Er1 C16 C9 161.9(7) . . . . ? C1 Er1 C16 C9 78.4(8) . . . . ? C8 Er1 C16 C9 108.2(8) . . . . ? C4 Er1 C16 C9 71(14) . . . . ? C14 Er1 C16 C9 -128.8(9) . . . . ? C3 Er1 C16 K2 110.9(7) . . . . ? C11 Er1 C16 K2 29.9(5) . . . . ? C13 Er1 C16 K2 -30.1(4) . . . . ? C7 Er1 C16 K2 -148.3(5) . . . . ? C2 Er1 C16 K2 127.4(4) . . . . ? C6 Er1 C16 K2 -124.2(5) . . . . ? C1 Er1 C16 K2 152.4(5) . . . . ? C8 Er1 C16 K2 -177.8(5) . . . . ? C4 Er1 C16 K2 145(14) . . . . ? C9 Er1 C16 K2 74.0(7) . . . . ? C14 Er1 C16 K2 -54.8(4) . . . . ? C18 K2 C16 C15 177.6(10) . . . . ? C19' K2 C16 C15 -171.0(9) . . . . ? C17 K2 C16 C15 152.1(10) . . . . ? C21' K2 C16 C15 42(2) . . . . ? C24 K2 C16 C15 124.2(10) . . . . ? C19 K2 C16 C15 -161.2(12) . . . . ? C20' K2 C16 C15 -150(2) . . . . ? C20 K2 C16 C15 -79(32) . . . . ? C18' K2 C16 C15 166.0(9) . . . . ? C17' K2 C16 C15 140.2(10) . . . . ? C18 K2 C16 C9 -39.5(11) . . . . ? C19' K2 C16 C9 -28.1(11) . . . . ? C17 K2 C16 C9 -64.9(10) . . . . ? C21' K2 C16 C9 -175.1(19) . . . . ? C24 K2 C16 C9 -92.9(10) . . . . ? C19 K2 C16 C9 -18.3(14) . . . . ? C20' K2 C16 C9 -7(2) . . . . ? C20 K2 C16 C9 63(32) . . . . ? C15 K2 C16 C9 142.9(10) . . . . ? C18' K2 C16 C9 -51.1(10) . . . . ? C17' K2 C16 C9 -76.9(10) . . . . ? C18 K2 C16 Er1 -110.9(9) . . . . ? C19' K2 C16 Er1 -99.6(9) . . . . ? C17 K2 C16 Er1 -136.4(8) . . . . ? C21' K2 C16 Er1 113.5(19) . . . . ? C24 K2 C16 Er1 -164.4(8) . . . . ? C19 K2 C16 Er1 -89.7(12) . . . . ? C20' K2 C16 Er1 -79(2) . . . . ? C20 K2 C16 Er1 -8(32) . . . . ? C15 K2 C16 Er1 71.4(6) . . . . ? C18' K2 C16 Er1 -122.6(8) . . . . ? C17' K2 C16 Er1 -148.4(8) . . . . ? C26 Er2 C17 C24 120.7(15) . . . . ? C29 Er2 C17 C24 -161(2) . . . . ? C28 Er2 C17 C24 173.1(13) . . . . ? C25 Er2 C17 C24 89.4(15) . . . . ? C27 Er2 C17 C24 149.6(14) . . . . ? C32 Er2 C17 C24 61.1(16) . . . . ? C31 Er2 C17 C24 38.8(18) . . . . ? C30 Er2 C17 C24 12(4) . . . . ? C18' Er2 C17 C24 -157(3) . . . . ? C20' Er2 C17 C24 -114.2(15) . . . . ? C19 Er2 C17 C24 -126.3(16) . . . . ? C26 Er2 C17 C18 -95.0(15) . . . . ? C29 Er2 C17 C18 -17(3) . . . . ? C28 Er2 C17 C18 -42.7(17) . . . . ? C25 Er2 C17 C18 -126.4(15) . . . . ? C27 Er2 C17 C18 -66.2(15) . . . . ? C32 Er2 C17 C18 -154.7(13) . . . . ? C31 Er2 C17 C18 -177.0(12) . . . . ? C30 Er2 C17 C18 156(3) . . . . ? C18' Er2 C17 C18 -13(2) . . . . ? C20' Er2 C17 C18 30.0(12) . . . . ? C19 Er2 C17 C18 17.9(12) . . . . ? C26 Er2 C17 K2 -165.6(10) . . . . ? C29 Er2 C17 K2 -87(2) . . . . ? C28 Er2 C17 K2 -113.2(9) . . . . ? C25 Er2 C17 K2 163.0(9) . . . . ? C27 Er2 C17 K2 -136.7(9) . . . . ? C32 Er2 C17 K2 134.7(8) . . . . ? C31 Er2 C17 K2 112.4(10) . . . . ? C30 Er2 C17 K2 85(3) . . . . ? C18' Er2 C17 K2 -83(3) . . . . ? C20' Er2 C17 K2 -40.5(6) . . . . ? C19 Er2 C17 K2 -52.6(7) . . . . ? C18 K2 C17 C24 142.8(19) . . . . ? C19' K2 C17 C24 132.3(17) . . . . ? C21' K2 C17 C24 83.1(13) . . . . ? C19 K2 C17 C24 121.6(15) . . . . ? C20' K2 C17 C24 109.4(13) . . . . ? C20 K2 C17 C24 98.0(12) . . . . ? C15 K2 C17 C24 -66.2(14) . . . . ? C18' K2 C17 C24 150(3) . . . . ? C16 K2 C17 C24 -83.2(14) . . . . ? C17' K2 C17 C24 -13(3) . . . . ? C19' K2 C17 C18 -10.6(11) . . . . ? C21' K2 C17 C18 -59.7(12) . . . . ? C24 K2 C17 C18 -142.8(19) . . . . ? C19 K2 C17 C18 -21.3(10) . . . . ? C20' K2 C17 C18 -33.4(11) . . . . ? C20 K2 C17 C18 -44.8(11) . . . . ? C15 K2 C17 C18 151.0(10) . . . . ? C18' K2 C17 C18 7(2) . . . . ? C16 K2 C17 C18 134.0(12) . . . . ? C17' K2 C17 C18 -156(4) . . . . ? C18 K2 C17 Er2 71.0(11) . . . . ? C19' K2 C17 Er2 60.4(9) . . . . ? C21' K2 C17 Er2 11.3(6) . . . . ? C24 K2 C17 Er2 -71.8(12) . . . . ? C19 K2 C17 Er2 49.7(7) . . . . ? C20' K2 C17 Er2 37.6(6) . . . . ? C20 K2 C17 Er2 26.2(6) . . . . ? C15 K2 C17 Er2 -138.0(7) . . . . ? C18' K2 C17 Er2 78(2) . . . . ? C16 K2 C17 Er2 -155.0(8) . . . . ? C17' K2 C17 Er2 -85(3) . . . . ? C24 C17 C18 C19 6(6) . . . . ? Er2 C17 C18 C19 -46(3) . . . . ? K2 C17 C18 C19 61(3) . . . . ? C24 C17 C18 Er2 52(3) . . . . ? K2 C17 C18 Er2 106.8(5) . . . . ? C24 C17 C18 K2 -55(3) . . . . ? Er2 C17 C18 K2 -106.8(5) . . . . ? C26 Er2 C18 C19 -123.0(15) . . . . ? C29 Er2 C18 C19 -38.7(17) . . . . ? C28 Er2 C18 C19 -63.4(15) . . . . ? C25 Er2 C18 C19 -150.9(13) . . . . ? C27 Er2 C18 C19 -92.0(15) . . . . ? C32 Er2 C18 C19 -174.3(12) . . . . ? C31 Er2 C18 C19 159(3) . . . . ? C30 Er2 C18 C19 -16(3) . . . . ? C18' Er2 C18 C19 163(4) . . . . ? C20' Er2 C18 C19 10.4(14) . . . . ? C17 Er2 C18 C19 148(2) . . . . ? C26 Er2 C18 C17 88.6(15) . . . . ? C29 Er2 C18 C17 172.9(13) . . . . ? C28 Er2 C18 C17 148.2(15) . . . . ? C25 Er2 C18 C17 60.7(15) . . . . ? C27 Er2 C18 C17 119.6(15) . . . . ? C32 Er2 C18 C17 37.3(18) . . . . ? C31 Er2 C18 C17 10(4) . . . . ? C30 Er2 C18 C17 -164.0(19) . . . . ? C18' Er2 C18 C17 15(3) . . . . ? C20' Er2 C18 C17 -138.0(17) . . . . ? C19 Er2 C18 C17 -148(2) . . . . ? C26 Er2 C18 K2 162.4(10) . . . . ? C29 Er2 C18 K2 -113.2(9) . . . . ? C28 Er2 C18 K2 -138.0(9) . . . . ? C25 Er2 C18 K2 134.6(8) . . . . ? C27 Er2 C18 K2 -166.6(10) . . . . ? C32 Er2 C18 K2 111.2(10) . . . . ? C31 Er2 C18 K2 84(3) . . . . ? C30 Er2 C18 K2 -90(2) . . . . ? C18' Er2 C18 K2 89(3) . . . . ? C20' Er2 C18 K2 -64.2(9) . . . . ? C19 Er2 C18 K2 -74.6(13) . . . . ? C17 Er2 C18 K2 73.8(13) . . . . ? C19' K2 C18 C19 10(2) . . . . ? C17 K2 C18 C19 -141.1(17) . . . . ? C21' K2 C18 C19 -32.3(11) . . . . ? C24 K2 C18 C19 -120.6(13) . . . . ? C20' K2 C18 C19 -10.2(12) . . . . ? C20 K2 C18 C19 -19.3(10) . . . . ? C15 K2 C18 C19 161.4(11) . . . . ? C18' K2 C18 C19 -149(3) . . . . ? C16 K2 C18 C19 158.9(12) . . . . ? C17' K2 C18 C19 -133.3(15) . . . . ? C19' K2 C18 C17 151(3) . . . . ? C21' K2 C18 C17 108.8(13) . . . . ? C24 K2 C18 C17 20.5(11) . . . . ? C19 K2 C18 C17 141.1(17) . . . . ? C20' K2 C18 C17 130.9(15) . . . . ? C20 K2 C18 C17 121.8(13) . . . . ? C15 K2 C18 C17 -57.5(17) . . . . ? C18' K2 C18 C17 -8(2) . . . . ? C16 K2 C18 C17 -60.0(13) . . . . ? C17' K2 C18 C17 7.8(12) . . . . ? C19' K2 C18 Er2 80(3) . . . . ? C17 K2 C18 Er2 -70.5(11) . . . . ? C21' K2 C18 Er2 38.3(6) . . . . ? C24 K2 C18 Er2 -50.0(7) . . . . ? C19 K2 C18 Er2 70.6(11) . . . . ? C20' K2 C18 Er2 60.4(8) . . . . ? C20 K2 C18 Er2 51.3(6) . . . . ? C15 K2 C18 Er2 -127.9(8) . . . . ? C18' K2 C18 Er2 -79(3) . . . . ? C16 K2 C18 Er2 -130.5(7) . . . . ? C17' K2 C18 Er2 -62.7(8) . . . . ? C17 C18 C19 C20 -6(6) . . . . ? Er2 C18 C19 C20 -52(3) . . . . ? K2 C18 C19 C20 54(3) . . . . ? C17 C18 C19 Er2 46(3) . . . . ? K2 C18 C19 Er2 106.6(4) . . . . ? C17 C18 C19 K2 -61(3) . . . . ? Er2 C18 C19 K2 -106.6(4) . . . . ? C26 Er2 C19 C20 -150.0(14) . . . . ? C29 Er2 C19 C20 -63.6(16) . . . . ? C28 Er2 C19 C20 -93.0(16) . . . . ? C25 Er2 C19 C20 -172.1(12) . . . . ? C27 Er2 C19 C20 -123.7(15) . . . . ? C32 Er2 C19 C20 166(3) . . . . ? C31 Er2 C19 C20 -22(3) . . . . ? C30 Er2 C19 C20 -41.1(17) . . . . ? C18' Er2 C19 C20 139.9(18) . . . . ? C20' Er2 C19 C20 -7(3) . . . . ? C17 Er2 C19 C20 127.4(16) . . . . ? C26 Er2 C19 C18 64.2(15) . . . . ? C29 Er2 C19 C18 150.6(14) . . . . ? C28 Er2 C19 C18 121.2(15) . . . . ? C25 Er2 C19 C18 42.1(17) . . . . ? C27 Er2 C19 C18 90.5(15) . . . . ? C32 Er2 C19 C18 20(4) . . . . ? C31 Er2 C19 C18 -168.0(16) . . . . ? C30 Er2 C19 C18 173.1(13) . . . . ? C18' Er2 C19 C18 -5.9(13) . . . . ? C20' Er2 C19 C18 -152(4) . . . . ? C17 Er2 C19 C18 -18.4(12) . . . . ? C26 Er2 C19 K2 135.0(8) . . . . ? C29 Er2 C19 K2 -138.6(9) . . . . ? C28 Er2 C19 K2 -168.0(10) . . . . ? C25 Er2 C19 K2 112.9(9) . . . . ? C27 Er2 C19 K2 161.4(10) . . . . ? C32 Er2 C19 K2 91(3) . . . . ? C31 Er2 C19 K2 -97.2(19) . . . . ? C30 Er2 C19 K2 -116.0(9) . . . . ? C18' Er2 C19 K2 65.0(10) . . . . ? C20' Er2 C19 K2 -82(3) . . . . ? C17 Er2 C19 K2 52.5(8) . . . . ? C18 K2 C19 C20 -144.9(18) . . . . ? C19' K2 C19 C20 -155(3) . . . . ? C17 K2 C19 C20 -123.1(14) . . . . ? C21' K2 C19 C20 -11.9(12) . . . . ? C24 K2 C19 C20 -98.6(12) . . . . ? C20' K2 C19 C20 7(2) . . . . ? C15 K2 C19 C20 98(5) . . . . ? C18' K2 C19 C20 -134.4(16) . . . . ? C16 K2 C19 C20 176.7(11) . . . . ? C17' K2 C19 C20 -113.2(13) . . . . ? C19' K2 C19 C18 -10(2) . . . . ? C17 K2 C19 C18 21.8(10) . . . . ? C21' K2 C19 C18 133.1(15) . . . . ? C24 K2 C19 C18 46.4(11) . . . . ? C20' K2 C19 C18 152(3) . . . . ? C20 K2 C19 C18 144.9(18) . . . . ? C15 K2 C19 C18 -117(5) . . . . ? C18' K2 C19 C18 10.5(10) . . . . ? C16 K2 C19 C18 -38.3(18) . . . . ? C17' K2 C19 C18 31.7(11) . . . . ? C18 K2 C19 Er2 -71.9(11) . . . . ? C19' K2 C19 Er2 -82(3) . . . . ? C17 K2 C19 Er2 -50.0(7) . . . . ? C21' K2 C19 Er2 61.2(8) . . . . ? C24 K2 C19 Er2 -25.5(6) . . . . ? C20' K2 C19 Er2 80(3) . . . . ? C20 K2 C19 Er2 73.1(12) . . . . ? C15 K2 C19 Er2 171(5) . . . . ? C18' K2 C19 Er2 -61.4(8) . . . . ? C16 K2 C19 Er2 -110.2(10) . . . . ? C17' K2 C19 Er2 -40.1(6) . . . . ? C18 C19 C20 C21 5(6) . . . . ? Er2 C19 C20 C21 -47(3) . . . . ? K2 C19 C20 C21 58(3) . . . . ? C18 C19 C20 Er2 52(3) . . . . ? K2 C19 C20 Er2 105.3(4) . . . . ? C18 C19 C20 K2 -53(3) . . . . ? Er2 C19 C20 K2 -105.3(4) . . . . ? C26 Er2 C20 C21 -169.9(12) . . . . ? C29 Er2 C20 C21 -92.3(15) . . . . ? C28 Er2 C20 C21 -124.1(15) . . . . ? C25 Er2 C20 C21 172(2) . . . . ? C27 Er2 C20 C21 -150.3(13) . . . . ? C32 Er2 C20 C21 -25(3) . . . . ? C31 Er2 C20 C21 -42.5(16) . . . . ? C30 Er2 C20 C21 -63.8(15) . . . . ? C18' Er2 C20 C21 118.7(14) . . . . ? C20' Er2 C20 C21 155(4) . . . . ? C19 Er2 C20 C21 147(2) . . . . ? C17 Er2 C20 C21 103.8(14) . . . . ? C26 Er2 C20 C19 42.7(18) . . . . ? C29 Er2 C20 C19 120.3(16) . . . . ? C28 Er2 C20 C19 88.6(16) . . . . ? C25 Er2 C20 C19 25(3) . . . . ? C27 Er2 C20 C19 62.3(16) . . . . ? C32 Er2 C20 C19 -172.2(16) . . . . ? C31 Er2 C20 C19 170.2(13) . . . . ? C30 Er2 C20 C19 148.9(15) . . . . ? C18' Er2 C20 C19 -28.6(13) . . . . ? C20' Er2 C20 C19 7(3) . . . . ? C17 Er2 C20 C19 -43.5(14) . . . . ? C26 Er2 C20 K2 114.2(9) . . . . ? C29 Er2 C20 K2 -168.1(10) . . . . ? C28 Er2 C20 K2 160.1(10) . . . . ? C25 Er2 C20 K2 97(3) . . . . ? C27 Er2 C20 K2 133.8(8) . . . . ? C32 Er2 C20 K2 -100.7(17) . . . . ? C31 Er2 C20 K2 -118.3(8) . . . . ? C30 Er2 C20 K2 -139.6(8) . . . . ? C18' Er2 C20 K2 42.9(7) . . . . ? C20' Er2 C20 K2 79(3) . . . . ? C19 Er2 C20 K2 71.5(13) . . . . ? C17 Er2 C20 K2 28.0(7) . . . . ? C18 K2 C20 C21 -122.4(14) . . . . ? C19' K2 C20 C21 -133.1(16) . . . . ? C17 K2 C20 C21 -97.6(12) . . . . ? C21' K2 C20 C21 7(2) . . . . ? C24 K2 C20 C21 -70.0(12) . . . . ? C19 K2 C20 C21 -141.8(18) . . . . ? C20' K2 C20 C21 -150(3) . . . . ? C15 K2 C20 C21 57.0(17) . . . . ? C18' K2 C20 C21 -111.1(13) . . . . ? C16 K2 C20 C21 133(31) . . . . ? C17' K2 C20 C21 -85.8(12) . . . . ? C18 K2 C20 C19 19.5(10) . . . . ? C19' K2 C20 C19 8.7(11) . . . . ? C17 K2 C20 C19 44.2(12) . . . . ? C21' K2 C20 C19 149(3) . . . . ? C24 K2 C20 C19 71.9(12) . . . . ? C20' K2 C20 C19 -8(3) . . . . ? C15 K2 C20 C19 -161.2(10) . . . . ? C18' K2 C20 C19 30.7(11) . . . . ? C16 K2 C20 C19 -85(31) . . . . ? C17' K2 C20 C19 56.0(12) . . . . ? C18 K2 C20 Er2 -50.6(7) . . . . ? C19' K2 C20 Er2 -61.4(8) . . . . ? C17 K2 C20 Er2 -25.9(6) . . . . ? C21' K2 C20 Er2 79(2) . . . . ? C24 K2 C20 Er2 1.8(6) . . . . ? C19 K2 C20 Er2 -70.1(11) . . . . ? C20' K2 C20 Er2 -78(3) . . . . ? C15 K2 C20 Er2 128.7(8) . . . . ? C18' K2 C20 Er2 -39.4(6) . . . . ? C16 K2 C20 Er2 -155(31) . . . . ? C17' K2 C20 Er2 -14.1(6) . . . . ? C19 C20 C21 C22 -2(6) . . . . ? Er2 C20 C21 C22 -48(3) . . . . ? K2 C20 C21 C22 56(3) . . . . ? C19 C20 C21 Er2 47(3) . . . . ? K2 C20 C21 Er2 103.8(4) . . . . ? C19 C20 C21 K2 -57(3) . . . . ? Er2 C20 C21 K2 -103.8(4) . . . . ? C26 Er2 C21 C20 30(3) . . . . ? C29 Er2 C21 C20 88.5(15) . . . . ? C28 Er2 C21 C20 61.4(15) . . . . ? C25 Er2 C21 C20 -174.7(17) . . . . ? C27 Er2 C21 C20 41.5(17) . . . . ? C32 Er2 C21 C20 169.1(12) . . . . ? C31 Er2 C21 C20 147.9(14) . . . . ? C30 Er2 C21 C20 120.5(15) . . . . ? C18' Er2 C21 C20 -55.3(14) . . . . ? C20' Er2 C21 C20 -8.9(13) . . . . ? C19 Er2 C21 C20 -18.7(12) . . . . ? C17 Er2 C21 C20 -72.4(13) . . . . ? C26 Er2 C21 C22 177(2) . . . . ? C29 Er2 C21 C22 -124.5(15) . . . . ? C28 Er2 C21 C22 -151.6(13) . . . . ? C25 Er2 C21 C22 -28(3) . . . . ? C27 Er2 C21 C22 -171.6(12) . . . . ? C32 Er2 C21 C22 -43.9(16) . . . . ? C31 Er2 C21 C22 -65.2(15) . . . . ? C30 Er2 C21 C22 -92.5(15) . . . . ? C18' Er2 C21 C22 91.6(13) . . . . ? C20' Er2 C21 C22 138.1(17) . . . . ? C19 Er2 C21 C22 128.3(15) . . . . ? C17 Er2 C21 C22 74.5(13) . . . . ? C26 Er2 C21 K2 101(2) . . . . ? C29 Er2 C21 K2 160.2(9) . . . . ? C28 Er2 C21 K2 133.0(8) . . . . ? C25 Er2 C21 K2 -103.1(19) . . . . ? C27 Er2 C21 K2 113.1(8) . . . . ? C32 Er2 C21 K2 -119.2(8) . . . . ? C31 Er2 C21 K2 -140.5(8) . . . . ? C30 Er2 C21 K2 -167.8(9) . . . . ? C18' Er2 C21 K2 16.3(7) . . . . ? C20' Er2 C21 K2 62.7(9) . . . . ? C19 Er2 C21 K2 53.0(7) . . . . ? C17 Er2 C21 K2 -0.8(7) . . . . ? C18 K2 C21 C20 44.7(11) . . . . ? C19' K2 C21 C20 31.9(11) . . . . ? C17 K2 C21 C20 72.7(12) . . . . ? C21' K2 C21 C20 -9(3) . . . . ? C24 K2 C21 C20 100.4(13) . . . . ? C19 K2 C21 C20 21.1(11) . . . . ? C20' K2 C21 C20 10.5(12) . . . . ? C15 K2 C21 C20 -148.8(12) . . . . ? C18' K2 C21 C20 57.4(12) . . . . ? C16 K2 C21 C20 -177.5(12) . . . . ? C17' K2 C21 C20 85.3(13) . . . . ? C18 K2 C21 C22 -99.0(12) . . . . ? C19' K2 C21 C22 -111.8(13) . . . . ? C17 K2 C21 C22 -70.9(12) . . . . ? C21' K2 C21 C22 -153(4) . . . . ? C24 K2 C21 C22 -43.3(11) . . . . ? C19 K2 C21 C22 -122.6(14) . . . . ? C20' K2 C21 C22 -133.2(16) . . . . ? C20 K2 C21 C22 -143.7(19) . . . . ? C15 K2 C21 C22 67.6(13) . . . . ? C18' K2 C21 C22 -86.2(12) . . . . ? C16 K2 C21 C22 38.8(18) . . . . ? C17' K2 C21 C22 -58.3(12) . . . . ? C18 K2 C21 Er2 -27.4(6) . . . . ? C19' K2 C21 Er2 -40.2(6) . . . . ? C17 K2 C21 Er2 0.7(6) . . . . ? C21' K2 C21 Er2 -81(3) . . . . ? C24 K2 C21 Er2 28.3(6) . . . . ? C19 K2 C21 Er2 -51.0(7) . . . . ? C20' K2 C21 Er2 -61.6(8) . . . . ? C20 K2 C21 Er2 -72.0(12) . . . . ? C15 K2 C21 Er2 139.2(6) . . . . ? C18' K2 C21 Er2 -14.6(6) . . . . ? C16 K2 C21 Er2 110.5(11) . . . . ? C17' K2 C21 Er2 13.3(6) . . . . ? C20 C21 C22 C23 -3(5) . . . . ? Er2 C21 C22 C23 -51(3) . . . . ? K2 C21 C22 C23 52(3) . . . . ? C20 C21 C22 Er2 49(3) . . . . ? K2 C21 C22 Er2 102.9(4) . . . . ? C20 C21 C22 K2 -54(3) . . . . ? Er2 C21 C22 K2 -102.9(4) . . . . ? C26 Er2 C22 C21 -177.4(17) . . . . ? C29 Er2 C22 C21 60.4(15) . . . . ? C28 Er2 C22 C21 39.7(17) . . . . ? C25 Er2 C22 C21 168.7(13) . . . . ? C27 Er2 C22 C21 24(3) . . . . ? C32 Er2 C22 C21 146.9(14) . . . . ? C31 Er2 C22 C21 119.4(15) . . . . ? C30 Er2 C22 C21 88.7(15) . . . . ? C18' Er2 C22 C21 -86.3(13) . . . . ? C20' Er2 C22 C21 -29.7(13) . . . . ? C19 Er2 C22 C21 -42.6(13) . . . . ? C17 Er2 C22 C21 -101.9(13) . . . . ? C26 Er2 C22 C23 -33(3) . . . . ? C29 Er2 C22 C23 -155.5(13) . . . . ? C28 Er2 C22 C23 -176.2(12) . . . . ? C25 Er2 C22 C23 -47.2(16) . . . . ? C27 Er2 C22 C23 168.4(19) . . . . ? C32 Er2 C22 C23 -69.0(14) . . . . ? C31 Er2 C22 C23 -96.5(14) . . . . ? C30 Er2 C22 C23 -127.2(14) . . . . ? C18' Er2 C22 C23 57.8(13) . . . . ? C20' Er2 C22 C23 114.4(14) . . . . ? C19 Er2 C22 C23 101.6(13) . . . . ? C17 Er2 C22 C23 42.2(12) . . . . ? C26 Er2 C22 K2 -104.7(19) . . . . ? C29 Er2 C22 K2 133.1(7) . . . . ? C28 Er2 C22 K2 112.4(9) . . . . ? C25 Er2 C22 K2 -118.6(8) . . . . ? C27 Er2 C22 K2 97(2) . . . . ? C32 Er2 C22 K2 -140.4(7) . . . . ? C31 Er2 C22 K2 -167.9(9) . . . . ? C30 Er2 C22 K2 161.4(9) . . . . ? C18' Er2 C22 K2 -13.6(7) . . . . ? C20' Er2 C22 K2 43.0(6) . . . . ? C19 Er2 C22 K2 30.2(7) . . . . ? C17 Er2 C22 K2 -29.2(6) . . . . ? C18 K2 C22 C21 71.3(12) . . . . ? C19' K2 C22 C21 57.0(12) . . . . ? C17 K2 C22 C21 99.3(12) . . . . ? C21' K2 C22 C21 8.8(12) . . . . ? C24 K2 C22 C21 123.9(14) . . . . ? C19 K2 C22 C21 44.2(11) . . . . ? C20' K2 C22 C21 31.5(11) . . . . ? C20 K2 C22 C21 20.1(11) . . . . ? C15 K2 C22 C21 -130.0(12) . . . . ? C18' K2 C22 C21 84.3(12) . . . . ? C16 K2 C22 C21 -159.1(12) . . . . ? C17' K2 C22 C21 111.0(13) . . . . ? C18 K2 C22 C23 -72.6(12) . . . . ? C19' K2 C22 C23 -86.9(13) . . . . ? C17 K2 C22 C23 -44.5(12) . . . . ? C21' K2 C22 C23 -135.1(16) . . . . ? C24 K2 C22 C23 -20.0(11) . . . . ? C19 K2 C22 C23 -99.7(13) . . . . ? C20' K2 C22 C23 -112.4(13) . . . . ? C20 K2 C22 C23 -123.8(14) . . . . ? C15 K2 C22 C23 86.2(13) . . . . ? C18' K2 C22 C23 -59.5(12) . . . . ? C16 K2 C22 C23 57.1(15) . . . . ? C17' K2 C22 C23 -32.8(12) . . . . ? C18 K2 C22 Er2 -0.9(6) . . . . ? C19' K2 C22 Er2 -15.2(6) . . . . ? C17 K2 C22 Er2 27.2(6) . . . . ? C21' K2 C22 Er2 -63.4(9) . . . . ? C24 K2 C22 Er2 51.7(7) . . . . ? C19 K2 C22 Er2 -28.0(6) . . . . ? C20' K2 C22 Er2 -40.7(6) . . . . ? C20 K2 C22 Er2 -52.1(7) . . . . ? C15 K2 C22 Er2 157.9(6) . . . . ? C18' K2 C22 Er2 12.2(6) . . . . ? C16 K2 C22 Er2 128.8(7) . . . . ? C17' K2 C22 Er2 38.9(6) . . . . ? C21 C22 C23 C24 3(6) . . . . ? Er2 C22 C23 C24 -48(3) . . . . ? K2 C22 C23 C24 55(3) . . . . ? C21 C22 C23 Er2 51(3) . . . . ? K2 C22 C23 Er2 103.3(4) . . . . ? C21 C22 C23 K2 -52(3) . . . . ? Er2 C22 C23 K2 -103.3(4) . . . . ? C26 Er2 C23 C24 -45.0(17) . . . . ? C29 Er2 C23 C24 -177.7(13) . . . . ? C28 Er2 C23 C24 159(2) . . . . ? C25 Er2 C23 C24 -66.9(16) . . . . ? C27 Er2 C23 C24 -22(3) . . . . ? C32 Er2 C23 C24 -95.8(15) . . . . ? C31 Er2 C23 C24 -126.6(15) . . . . ? C30 Er2 C23 C24 -154.0(14) . . . . ? C18' Er2 C23 C24 31.0(13) . . . . ? C20' Er2 C23 C24 89.0(14) . . . . ? C19 Er2 C23 C24 73.3(14) . . . . ? C17 Er2 C23 C24 19.0(12) . . . . ? C26 Er2 C23 C22 167.1(11) . . . . ? C29 Er2 C23 C22 34.4(17) . . . . ? C28 Er2 C23 C22 11(3) . . . . ? C25 Er2 C23 C22 145.1(13) . . . . ? C27 Er2 C23 C22 -170.0(17) . . . . ? C32 Er2 C23 C22 116.3(14) . . . . ? C31 Er2 C23 C22 85.5(14) . . . . ? C30 Er2 C23 C22 58.1(14) . . . . ? C18' Er2 C23 C22 -117.0(13) . . . . ? C20' Er2 C23 C22 -58.9(13) . . . . ? C19 Er2 C23 C22 -74.6(12) . . . . ? C17 Er2 C23 C22 -128.9(14) . . . . ? C26 Er2 C23 K2 -116.6(8) . . . . ? C29 Er2 C23 K2 110.7(9) . . . . ? C28 Er2 C23 K2 88(3) . . . . ? C25 Er2 C23 K2 -138.5(8) . . . . ? C27 Er2 C23 K2 -94(2) . . . . ? C32 Er2 C23 K2 -167.4(9) . . . . ? C31 Er2 C23 K2 161.8(9) . . . . ? C30 Er2 C23 K2 134.4(8) . . . . ? C18' Er2 C23 K2 -40.6(6) . . . . ? C20' Er2 C23 K2 17.4(7) . . . . ? C19 Er2 C23 K2 1.7(7) . . . . ? C17 Er2 C23 K2 -52.6(7) . . . . ? C18 K2 C23 C24 -46.0(12) . . . . ? C19' K2 C23 C24 -59.9(13) . . . . ? C17 K2 C23 C24 -21.3(11) . . . . ? C21' K2 C23 C24 -113.9(14) . . . . ? C19 K2 C23 C24 -73.4(13) . . . . ? C20' K2 C23 C24 -87.7(13) . . . . ? C20 K2 C23 C24 -100.5(13) . . . . ? C15 K2 C23 C24 108.3(14) . . . . ? C18' K2 C23 C24 -34.5(12) . . . . ? C16 K2 C23 C24 79.6(14) . . . . ? C17' K2 C23 C24 -10.8(13) . . . . ? C18 K2 C23 C22 97.8(12) . . . . ? C19' K2 C23 C22 83.8(12) . . . . ? C17 K2 C23 C22 122.5(14) . . . . ? C21' K2 C23 C22 29.8(11) . . . . ? C24 K2 C23 C22 144(2) . . . . ? C19 K2 C23 C22 70.3(12) . . . . ? C20' K2 C23 C22 56.1(12) . . . . ? C20 K2 C23 C22 43.3(11) . . . . ? C15 K2 C23 C22 -107.9(13) . . . . ? C18' K2 C23 C22 109.3(13) . . . . ? C16 K2 C23 C22 -136.6(13) . . . . ? C17' K2 C23 C22 132.9(16) . . . . ? C18 K2 C23 Er2 25.9(6) . . . . ? C19' K2 C23 Er2 11.9(6) . . . . ? C17 K2 C23 Er2 50.6(7) . . . . ? C21' K2 C23 Er2 -42.1(6) . . . . ? C24 K2 C23 Er2 71.9(12) . . . . ? C19 K2 C23 Er2 -1.6(6) . . . . ? C20' K2 C23 Er2 -15.9(6) . . . . ? C20 K2 C23 Er2 -28.6(6) . . . . ? C15 K2 C23 Er2 -179.9(6) . . . . ? C18' K2 C23 Er2 37.4(6) . . . . ? C16 K2 C23 Er2 151.5(7) . . . . ? C17' K2 C23 Er2 61.0(9) . . . . ? C22 C23 C24 C17 0(6) . . . . ? Er2 C23 C24 C17 -47(3) . . . . ? K2 C23 C24 C17 57(3) . . . . ? C22 C23 C24 Er2 48(3) . . . . ? K2 C23 C24 Er2 104.6(4) . . . . ? C22 C23 C24 K2 -57(3) . . . . ? Er2 C23 C24 K2 -104.6(4) . . . . ? C18 C17 C24 C23 -4(6) . . . . ? Er2 C17 C24 C23 47(3) . . . . ? K2 C17 C24 C23 -58(4) . . . . ? C18 C17 C24 Er2 -52(3) . . . . ? K2 C17 C24 Er2 -105.8(4) . . . . ? C18 C17 C24 K2 54(3) . . . . ? Er2 C17 C24 K2 105.8(4) . . . . ? C26 Er2 C24 C23 147.2(14) . . . . ? C29 Er2 C24 C23 7(4) . . . . ? C28 Er2 C24 C23 -163.9(19) . . . . ? C25 Er2 C24 C23 119.0(15) . . . . ? C27 Er2 C24 C23 171.3(12) . . . . ? C32 Er2 C24 C23 87.0(15) . . . . ? C31 Er2 C24 C23 59.7(15) . . . . ? C30 Er2 C24 C23 36.7(18) . . . . ? C18' Er2 C24 C23 -138.1(18) . . . . ? C20' Er2 C24 C23 -87.7(14) . . . . ? C19 Er2 C24 C23 -102.8(14) . . . . ? C17 Er2 C24 C23 -147(2) . . . . ? C26 Er2 C24 C17 -65.7(15) . . . . ? C29 Er2 C24 C17 154(3) . . . . ? C28 Er2 C24 C17 -17(3) . . . . ? C25 Er2 C24 C17 -93.9(15) . . . . ? C27 Er2 C24 C17 -41.6(17) . . . . ? C32 Er2 C24 C17 -125.9(15) . . . . ? C31 Er2 C24 C17 -153.2(14) . . . . ? C30 Er2 C24 C17 -176.2(13) . . . . ? C18' Er2 C24 C17 9.1(13) . . . . ? C20' Er2 C24 C17 59.4(14) . . . . ? C19 Er2 C24 C17 44.3(13) . . . . ? C26 Er2 C24 K2 -137.4(8) . . . . ? C29 Er2 C24 K2 82(3) . . . . ? C28 Er2 C24 K2 -89(2) . . . . ? C25 Er2 C24 K2 -165.6(9) . . . . ? C27 Er2 C24 K2 -113.3(9) . . . . ? C32 Er2 C24 K2 162.3(9) . . . . ? C31 Er2 C24 K2 135.0(8) . . . . ? C30 Er2 C24 K2 112.0(9) . . . . ? C18' Er2 C24 K2 -62.7(8) . . . . ? C20' Er2 C24 K2 -12.4(7) . . . . ? C19 Er2 C24 K2 -27.4(6) . . . . ? C17 Er2 C24 K2 -71.8(13) . . . . ? C18 K2 C24 C23 121.2(14) . . . . ? C19' K2 C24 C23 109.1(14) . . . . ? C17 K2 C24 C23 142.0(19) . . . . ? C21' K2 C24 C23 54.6(12) . . . . ? C19 K2 C24 C23 96.8(13) . . . . ? C20' K2 C24 C23 82.8(13) . . . . ? C20 K2 C24 C23 69.8(12) . . . . ? C15 K2 C24 C23 -85.9(13) . . . . ? C18' K2 C24 C23 130.5(16) . . . . ? C16 K2 C24 C23 -110.8(13) . . . . ? C17' K2 C24 C23 153(3) . . . . ? C18 K2 C24 C17 -20.8(11) . . . . ? C19' K2 C24 C17 -32.9(12) . . . . ? C21' K2 C24 C17 -87.3(13) . . . . ? C19 K2 C24 C17 -45.2(12) . . . . ? C20' K2 C24 C17 -59.2(12) . . . . ? C20 K2 C24 C17 -72.1(12) . . . . ? C15 K2 C24 C17 132.1(13) . . . . ? C18' K2 C24 C17 -11.5(12) . . . . ? C16 K2 C24 C17 107.3(14) . . . . ? C17' K2 C24 C17 11(2) . . . . ? C18 K2 C24 Er2 49.6(7) . . . . ? C19' K2 C24 Er2 37.5(6) . . . . ? C17 K2 C24 Er2 70.4(12) . . . . ? C21' K2 C24 Er2 -17.0(6) . . . . ? C19 K2 C24 Er2 25.1(6) . . . . ? C20' K2 C24 Er2 11.2(6) . . . . ? C20 K2 C24 Er2 -1.8(6) . . . . ? C15 K2 C24 Er2 -157.5(7) . . . . ? C18' K2 C24 Er2 58.9(8) . . . . ? C16 K2 C24 Er2 177.6(8) . . . . ? C17' K2 C24 Er2 81(3) . . . . ? C26 Er2 C17' C24' 133.1(14) . . . . ? C29 Er2 C17' C24' -135(8) . . . . ? C28 Er2 C17' C24' -179.3(12) . . . . ? C25 Er2 C17' C24' 102.4(15) . . . . ? C27 Er2 C17' C24' 159.3(12) . . . . ? C32 Er2 C17' C24' 72.0(15) . . . . ? C31 Er2 C17' C24' 48.3(16) . . . . ? C30 Er2 C17' C24' 27(2) . . . . ? C18' Er2 C17' C24' -146(2) . . . . ? C20' Er2 C17' C24' -103.0(14) . . . . ? C19 Er2 C17' C24' -116.3(14) . . . . ? C17 Er2 C17' C24' -151(4) . . . . ? C26 Er2 C17' C18' -80.5(15) . . . . ? C29 Er2 C17' C18' 12(9) . . . . ? C28 Er2 C17' C18' -32.9(19) . . . . ? C25 Er2 C17' C18' -111.1(15) . . . . ? C27 Er2 C17' C18' -54.2(15) . . . . ? C32 Er2 C17' C18' -141.6(14) . . . . ? C31 Er2 C17' C18' -165.3(13) . . . . ? C30 Er2 C17' C18' 173.8(14) . . . . ? C20' Er2 C17' C18' 43.4(12) . . . . ? C19 Er2 C17' C18' 30.2(13) . . . . ? C17 Er2 C17' C18' -5(3) . . . . ? C26 Er2 C17' K2 -152.5(9) . . . . ? C29 Er2 C17' K2 -61(8) . . . . ? C28 Er2 C17' K2 -104.9(11) . . . . ? C25 Er2 C17' K2 176.8(10) . . . . ? C27 Er2 C17' K2 -126.3(8) . . . . ? C32 Er2 C17' K2 146.4(9) . . . . ? C31 Er2 C17' K2 122.7(8) . . . . ? C30 Er2 C17' K2 101.7(14) . . . . ? C18' Er2 C17' K2 -72.1(12) . . . . ? C20' Er2 C17' K2 -28.6(7) . . . . ? C19 Er2 C17' K2 -41.9(6) . . . . ? C17 Er2 C17' K2 -77(3) . . . . ? C18 K2 C17' C24' 133.1(16) . . . . ? C19' K2 C17' C24' 122.3(14) . . . . ? C17 K2 C17' C24' 150(4) . . . . ? C21' K2 C17' C24' 70.6(12) . . . . ? C24 K2 C17' C24' -6(2) . . . . ? C19 K2 C17' C24' 111.0(14) . . . . ? C20' K2 C17' C24' 98.1(13) . . . . ? C20 K2 C17' C24' 85.9(13) . . . . ? C15 K2 C17' C24' -74.3(14) . . . . ? C18' K2 C17' C24' 140.8(19) . . . . ? C16 K2 C17' C24' -95.0(14) . . . . ? C18 K2 C17' C18' -7.7(11) . . . . ? C19' K2 C17' C18' -18.5(11) . . . . ? C17 K2 C17' C18' 10(3) . . . . ? C21' K2 C17' C18' -70.2(12) . . . . ? C24 K2 C17' C18' -147(3) . . . . ? C19 K2 C17' C18' -29.8(11) . . . . ? C20' K2 C17' C18' -42.7(11) . . . . ? C20 K2 C17' C18' -54.9(12) . . . . ? C15 K2 C17' C18' 144.9(11) . . . . ? C16 K2 C17' C18' 124.2(13) . . . . ? C18 K2 C17' Er2 61.2(8) . . . . ? C19' K2 C17' Er2 50.4(7) . . . . ? C17 K2 C17' Er2 78(3) . . . . ? C21' K2 C17' Er2 -1.3(6) . . . . ? C24 K2 C17' Er2 -78(2) . . . . ? C19 K2 C17' Er2 39.1(6) . . . . ? C20' K2 C17' Er2 26.2(6) . . . . ? C20 K2 C17' Er2 14.0(6) . . . . ? C15 K2 C17' Er2 -146.2(7) . . . . ? C18' K2 C17' Er2 68.9(11) . . . . ? C16 K2 C17' Er2 -166.9(8) . . . . ? C24' C17' C18' C19' -7(6) . . . . ? Er2 C17' C18' C19' -54(4) . . . . ? K2 C17' C18' C19' 51(4) . . . . ? C24' C17' C18' Er2 47(3) . . . . ? K2 C17' C18' Er2 105.0(5) . . . . ? C24' C17' C18' K2 -58(3) . . . . ? Er2 C17' C18' K2 -105.0(5) . . . . ? C26 Er2 C18' C19' -112.1(16) . . . . ? C29 Er2 C18' C19' -33(2) . . . . ? C28 Er2 C18' C19' -55.6(16) . . . . ? C25 Er2 C18' C19' -142.0(15) . . . . ? C27 Er2 C18' C19' -81.3(16) . . . . ? C32 Er2 C18' C19' -166.6(13) . . . . ? C31 Er2 C18' C19' 173.6(14) . . . . ? C30 Er2 C18' C19' -1(9) . . . . ? C20' Er2 C18' C19' 17.8(13) . . . . ? C19 Er2 C18' C19' 7.5(13) . . . . ? C17 Er2 C18' C19' 149(4) . . . . ? C26 Er2 C18' C17' 103.0(15) . . . . ? C29 Er2 C18' C17' -178.2(13) . . . . ? C28 Er2 C18' C17' 159.4(13) . . . . ? C25 Er2 C18' C17' 73.1(15) . . . . ? C27 Er2 C18' C17' 133.7(15) . . . . ? C32 Er2 C18' C17' 48.4(16) . . . . ? C31 Er2 C18' C17' 29(2) . . . . ? C30 Er2 C18' C17' -146(7) . . . . ? C20' Er2 C18' C17' -127.2(14) . . . . ? C19 Er2 C18' C17' -137.4(18) . . . . ? C17 Er2 C18' C17' 4(3) . . . . ? C26 Er2 C18' K2 177.1(10) . . . . ? C29 Er2 C18' K2 -104.1(11) . . . . ? C28 Er2 C18' K2 -126.5(8) . . . . ? C25 Er2 C18' K2 147.1(9) . . . . ? C27 Er2 C18' K2 -152.2(9) . . . . ? C32 Er2 C18' K2 122.5(8) . . . . ? C31 Er2 C18' K2 102.7(15) . . . . ? C30 Er2 C18' K2 -72(8) . . . . ? C20' Er2 C18' K2 -53.1(7) . . . . ? C19 Er2 C18' K2 -63.4(9) . . . . ? C17 Er2 C18' K2 78(3) . . . . ? C18 K2 C18' C19' 11(2) . . . . ? C17 K2 C18' C19' -154(3) . . . . ? C21' K2 C18' C19' -46.1(13) . . . . ? C24 K2 C18' C19' -133.4(17) . . . . ? C19 K2 C18' C19' -10.4(12) . . . . ? C20' K2 C18' C19' -21.7(12) . . . . ? C20 K2 C18' C19' -32.0(12) . . . . ? C15 K2 C18' C19' 157.6(11) . . . . ? C16 K2 C18' C19' 146.5(14) . . . . ? C17' K2 C18' C19' -146(2) . . . . ? C18 K2 C18' C17' 157(3) . . . . ? C19' K2 C18' C17' 146(2) . . . . ? C17 K2 C18' C17' -8(2) . . . . ? C21' K2 C18' C17' 100.0(12) . . . . ? C24 K2 C18' C17' 12.7(12) . . . . ? C19 K2 C18' C17' 135.7(16) . . . . ? C20' K2 C18' C17' 124.4(13) . . . . ? C20 K2 C18' C17' 114.1(13) . . . . ? C15 K2 C18' C17' -56.3(15) . . . . ? C16 K2 C18' C17' -67.4(13) . . . . ? C18 K2 C18' Er2 84(3) . . . . ? C19' K2 C18' Er2 72.5(13) . . . . ? C17 K2 C18' Er2 -81(2) . . . . ? C21' K2 C18' Er2 26.4(6) . . . . ? C24 K2 C18' Er2 -60.8(8) . . . . ? C19 K2 C18' Er2 62.1(9) . . . . ? C20' K2 C18' Er2 50.8(7) . . . . ? C20 K2 C18' Er2 40.5(6) . . . . ? C15 K2 C18' Er2 -129.9(7) . . . . ? C16 K2 C18' Er2 -141.0(8) . . . . ? C17' K2 C18' Er2 -73.6(11) . . . . ? C17' C18' C19' C20' 9(7) . . . . ? Er2 C18' C19' C20' -45(4) . . . . ? K2 C18' C19' C20' 61(4) . . . . ? C17' C18' C19' Er2 54(4) . . . . ? K2 C18' C19' Er2 106.0(4) . . . . ? C17' C18' C19' K2 -52(4) . . . . ? Er2 C18' C19' K2 -106.0(4) . . . . ? C26 Er2 C19' C20' -138.7(15) . . . . ? C29 Er2 C19' C20' -52.1(16) . . . . ? C28 Er2 C19' C20' -79.0(16) . . . . ? C25 Er2 C19' C20' -163.5(13) . . . . ? C27 Er2 C19' C20' -109.4(16) . . . . ? C32 Er2 C19' C20' 174.9(14) . . . . ? C31 Er2 C19' C20' 1(8) . . . . ? C30 Er2 C19' C20' -31(2) . . . . ? C18' Er2 C19' C20' 149(2) . . . . ? C19 Er2 C19' C20' -10(3) . . . . ? C17 Er2 C19' C20' 136.8(18) . . . . ? C26 Er2 C19' C18' 72.2(16) . . . . ? C29 Er2 C19' C18' 158.7(14) . . . . ? C28 Er2 C19' C18' 131.9(16) . . . . ? C25 Er2 C19' C18' 47.4(17) . . . . ? C27 Er2 C19' C18' 101.5(16) . . . . ? C32 Er2 C19' C18' 26(2) . . . . ? C31 Er2 C19' C18' -148(7) . . . . ? C30 Er2 C19' C18' 179.9(13) . . . . ? C20' Er2 C19' C18' -149(2) . . . . ? C19 Er2 C19' C18' -159(4) . . . . ? C17 Er2 C19' C18' -12.3(14) . . . . ? C26 Er2 C19' K2 147.5(9) . . . . ? C29 Er2 C19' K2 -126.0(9) . . . . ? C28 Er2 C19' K2 -152.8(10) . . . . ? C25 Er2 C19' K2 122.7(8) . . . . ? C27 Er2 C19' K2 176.8(10) . . . . ? C32 Er2 C19' K2 101.1(14) . . . . ? C31 Er2 C19' K2 -73(8) . . . . ? C30 Er2 C19' K2 -104.9(12) . . . . ? C18' Er2 C19' K2 75.3(14) . . . . ? C20' Er2 C19' K2 -73.8(13) . . . . ? C19 Er2 C19' K2 -84(3) . . . . ? C17 Er2 C19' K2 62.9(10) . . . . ? C18 K2 C19' C20' -151(3) . . . . ? C17 K2 C19' C20' -130.8(16) . . . . ? C21' K2 C19' C20' -20.1(10) . . . . ? C24 K2 C19' C20' -108.4(13) . . . . ? C19 K2 C19' C20' 9(2) . . . . ? C20 K2 C19' C20' -8.0(11) . . . . ? C15 K2 C19' C20' 152(2) . . . . ? C18' K2 C19' C20' -141(2) . . . . ? C16 K2 C19' C20' 169.7(11) . . . . ? C17' K2 C19' C20' -122.0(14) . . . . ? C18 K2 C19' C18' -10(2) . . . . ? C17 K2 C19' C18' 10.1(12) . . . . ? C21' K2 C19' C18' 120.8(15) . . . . ? C24 K2 C19' C18' 32.5(12) . . . . ? C19 K2 C19' C18' 150(3) . . . . ? C20' K2 C19' C18' 141(2) . . . . ? C20 K2 C19' C18' 133.0(17) . . . . ? C15 K2 C19' C18' -67(3) . . . . ? C16 K2 C19' C18' -49.4(17) . . . . ? C17' K2 C19' C18' 18.9(11) . . . . ? C18 K2 C19' Er2 -81(2) . . . . ? C17 K2 C19' Er2 -60.3(8) . . . . ? C21' K2 C19' Er2 50.5(7) . . . . ? C24 K2 C19' Er2 -37.8(6) . . . . ? C19 K2 C19' Er2 80(3) . . . . ? C20' K2 C19' Er2 70.6(11) . . . . ? C20 K2 C19' Er2 62.6(8) . . . . ? C15 K2 C19' Er2 -137(2) . . . . ? C18' K2 C19' Er2 -70.4(12) . . . . ? C16 K2 C19' Er2 -119.7(9) . . . . ? C17' K2 C19' Er2 -51.4(7) . . . . ? C18' C19' C20' C21' -9(6) . . . . ? Er2 C19' C20' C21' -53(3) . . . . ? K2 C19' C20' C21' 53(3) . . . . ? C18' C19' C20' Er2 44(4) . . . . ? K2 C19' C20' Er2 106.4(4) . . . . ? C18' C19' C20' K2 -62(4) . . . . ? Er2 C19' C20' K2 -106.4(4) . . . . ? C26 Er2 C20' C19' 51.4(17) . . . . ? C29 Er2 C20' C19' 134.9(16) . . . . ? C28 Er2 C20' C19' 103.4(16) . . . . ? C25 Er2 C20' C19' 31(2) . . . . ? C27 Er2 C20' C19' 74.4(16) . . . . ? C32 Er2 C20' C19' -155(6) . . . . ? C31 Er2 C20' C19' -179.8(13) . . . . ? C30 Er2 C20' C19' 160.5(14) . . . . ? C18' Er2 C20' C19' -17.6(13) . . . . ? C19 Er2 C20' C19' 9(3) . . . . ? C17 Er2 C20' C19' -31.3(14) . . . . ? C26 Er2 C20' C21' -164.6(13) . . . . ? C29 Er2 C20' C21' -81.2(15) . . . . ? C28 Er2 C20' C21' -112.6(15) . . . . ? C25 Er2 C20' C21' 175.1(13) . . . . ? C27 Er2 C20' C21' -141.7(14) . . . . ? C32 Er2 C20' C21' -11(7) . . . . ? C31 Er2 C20' C21' -35.8(19) . . . . ? C30 Er2 C20' C21' -55.5(15) . . . . ? C18' Er2 C20' C21' 126.3(15) . . . . ? C19 Er2 C20' C21' 153(4) . . . . ? C17 Er2 C20' C21' 112.6(15) . . . . ? C26 Er2 C20' K2 123.1(8) . . . . ? C29 Er2 C20' K2 -153.5(10) . . . . ? C28 Er2 C20' K2 175.1(11) . . . . ? C25 Er2 C20' K2 102.8(14) . . . . ? C27 Er2 C20' K2 146.0(9) . . . . ? C32 Er2 C20' K2 -84(7) . . . . ? C31 Er2 C20' K2 -108.1(11) . . . . ? C30 Er2 C20' K2 -127.8(8) . . . . ? C18' Er2 C20' K2 54.0(7) . . . . ? C19 Er2 C20' K2 81(3) . . . . ? C17 Er2 C20' K2 40.4(7) . . . . ? C18 K2 C20' C19' 10.5(12) . . . . ? C17 K2 C20' C19' 33.9(12) . . . . ? C21' K2 C20' C19' 143.9(18) . . . . ? C24 K2 C20' C19' 60.4(12) . . . . ? C19 K2 C20' C19' -9(2) . . . . ? C20 K2 C20' C19' 157(3) . . . . ? C15 K2 C20' C19' -157.3(15) . . . . ? C18' K2 C20' C19' 21.4(11) . . . . ? C16 K2 C20' C19' -30(3) . . . . ? C17' K2 C20' C19' 44.9(11) . . . . ? C18 K2 C20' C21' -133.4(15) . . . . ? C19' K2 C20' C21' -143.9(18) . . . . ? C17 K2 C20' C21' -110.0(13) . . . . ? C24 K2 C20' C21' -83.5(12) . . . . ? C19 K2 C20' C21' -153(3) . . . . ? C20 K2 C20' C21' 13(3) . . . . ? C15 K2 C20' C21' 59(2) . . . . ? C18' K2 C20' C21' -122.6(13) . . . . ? C16 K2 C20' C21' -173.5(17) . . . . ? C17' K2 C20' C21' -99.0(12) . . . . ? C18 K2 C20' Er2 -61.3(8) . . . . ? C19' K2 C20' Er2 -71.8(11) . . . . ? C17 K2 C20' Er2 -37.9(6) . . . . ? C21' K2 C20' Er2 72.1(11) . . . . ? C24 K2 C20' Er2 -11.4(6) . . . . ? C19 K2 C20' Er2 -81(3) . . . . ? C20 K2 C20' Er2 85(3) . . . . ? C15 K2 C20' Er2 130.9(15) . . . . ? C18' K2 C20' Er2 -50.5(6) . . . . ? C16 K2 C20' Er2 -101(2) . . . . ? C17' K2 C20' Er2 -26.9(6) . . . . ? C19' C20' C21' C22' 8(6) . . . . ? Er2 C20' C21' C22' -45(3) . . . . ? K2 C20' C21' C22' 61(3) . . . . ? C19' C20' C21' Er2 53(3) . . . . ? K2 C20' C21' Er2 106.1(4) . . . . ? C19' C20' C21' K2 -53(3) . . . . ? Er2 C20' C21' K2 -106.1(4) . . . . ? C26 Er2 C21' C22' 178.3(13) . . . . ? C29 Er2 C21' C22' -109.9(15) . . . . ? C28 Er2 C21' C22' -140.0(14) . . . . ? C25 Er2 C21' C22' -3(9) . . . . ? C27 Er2 C21' C22' -163.4(12) . . . . ? C32 Er2 C21' C22' -32.7(19) . . . . ? C31 Er2 C21' C22' -53.4(15) . . . . ? C30 Er2 C21' C22' -78.6(15) . . . . ? C18' Er2 C21' C22' 104.9(13) . . . . ? C20' Er2 C21' C22' 149(2) . . . . ? C19 Er2 C21' C22' 139.1(17) . . . . ? C17 Er2 C21' C22' 88.4(13) . . . . ? C26 Er2 C21' C20' 29(2) . . . . ? C29 Er2 C21' C20' 101.0(15) . . . . ? C28 Er2 C21' C20' 70.9(15) . . . . ? C25 Er2 C21' C20' -152(8) . . . . ? C27 Er2 C21' C20' 47.5(16) . . . . ? C32 Er2 C21' C20' 178.2(12) . . . . ? C31 Er2 C21' C20' 157.5(13) . . . . ? C30 Er2 C21' C20' 132.4(15) . . . . ? C18' Er2 C21' C20' -44.2(13) . . . . ? C19 Er2 C21' C20' -10.0(14) . . . . ? C17 Er2 C21' C20' -60.7(14) . . . . ? C26 Er2 C21' K2 102.2(14) . . . . ? C29 Er2 C21' K2 173.9(10) . . . . ? C28 Er2 C21' K2 143.9(9) . . . . ? C25 Er2 C21' K2 -79(8) . . . . ? C27 Er2 C21' K2 120.5(8) . . . . ? C32 Er2 C21' K2 -108.9(11) . . . . ? C31 Er2 C21' K2 -129.6(8) . . . . ? C30 Er2 C21' K2 -154.7(9) . . . . ? C18' Er2 C21' K2 28.8(7) . . . . ? C20' Er2 C21' K2 72.9(13) . . . . ? C19 Er2 C21' K2 63.0(9) . . . . ? C17 Er2 C21' K2 12.3(7) . . . . ? C18 K2 C21' C22' -109.8(13) . . . . ? C19' K2 C21' C22' -121.7(13) . . . . ? C17 K2 C21' C22' -82.8(12) . . . . ? C24 K2 C21' C22' -54.6(12) . . . . ? C19 K2 C21' C22' -131.7(15) . . . . ? C20' K2 C21' C22' -141.5(18) . . . . ? C20 K2 C21' C22' -152(3) . . . . ? C15 K2 C21' C22' 61.2(14) . . . . ? C18' K2 C21' C22' -97.6(12) . . . . ? C16 K2 C21' C22' 32(3) . . . . ? C17' K2 C21' C22' -70.3(12) . . . . ? C18 K2 C21' C20' 31.8(11) . . . . ? C19' K2 C21' C20' 19.8(10) . . . . ? C17 K2 C21' C20' 58.7(12) . . . . ? C24 K2 C21' C20' 86.9(12) . . . . ? C19 K2 C21' C20' 9.9(12) . . . . ? C20 K2 C21' C20' -11(2) . . . . ? C15 K2 C21' C20' -157.3(10) . . . . ? C18' K2 C21' C20' 44.0(11) . . . . ? C16 K2 C21' C20' 173.9(16) . . . . ? C17' K2 C21' C20' 71.2(12) . . . . ? C18 K2 C21' Er2 -38.1(6) . . . . ? C19' K2 C21' Er2 -50.1(6) . . . . ? C17 K2 C21' Er2 -11.2(6) . . . . ? C24 K2 C21' Er2 17.0(6) . . . . ? C19 K2 C21' Er2 -60.0(8) . . . . ? C20' K2 C21' Er2 -69.9(11) . . . . ? C20 K2 C21' Er2 -81(2) . . . . ? C15 K2 C21' Er2 132.8(7) . . . . ? C18' K2 C21' Er2 -25.9(6) . . . . ? C16 K2 C21' Er2 104.0(18) . . . . ? C17' K2 C21' Er2 1.3(6) . . . . ? C20' C21' C22' C23' -7(6) . . . . ? Er2 C21' C22' C23' -52(3) . . . . ? K2 C21' C22' C23' 53(3) . . . . ? C20' C21' C22' Er2 45(3) . . . . ? K2 C21' C22' Er2 104.9(5) . . . . ? C20' C21' C22' K2 -60(3) . . . . ? Er2 C21' C22' K2 -104.9(5) . . . . ? C26 Er2 C22' C21' -170(8) . . . . ? C29 Er2 C22' C21' 73.3(15) . . . . ? C28 Er2 C22' C21' 49.7(16) . . . . ? C25 Er2 C22' C21' 179.6(13) . . . . ? C27 Er2 C22' C21' 31(2) . . . . ? C32 Er2 C22' C21' 159.3(13) . . . . ? C31 Er2 C22' C21' 134.1(14) . . . . ? C30 Er2 C22' C21' 103.9(15) . . . . ? C18' Er2 C22' C21' -71.3(13) . . . . ? C20' Er2 C22' C21' -17.8(12) . . . . ? C19 Er2 C22' C21' -29.6(13) . . . . ? C17 Er2 C22' C21' -88.0(13) . . . . ? C26 Er2 C22' C23' -26(9) . . . . ? C29 Er2 C22' C23' -143.2(15) . . . . ? C28 Er2 C22' C23' -166.9(13) . . . . ? C25 Er2 C22' C23' -37(2) . . . . ? C27 Er2 C22' C23' 174.7(13) . . . . ? C32 Er2 C22' C23' -57.2(16) . . . . ? C31 Er2 C22' C23' -82.4(15) . . . . ? C30 Er2 C22' C23' -112.6(16) . . . . ? C18' Er2 C22' C23' 72.2(14) . . . . ? C20' Er2 C22' C23' 125.7(15) . . . . ? C19 Er2 C22' C23' 113.9(15) . . . . ? C17 Er2 C22' C23' 55.4(14) . . . . ? C26 Er2 C22' K2 -100(8) . . . . ? C29 Er2 C22' K2 143.4(8) . . . . ? C28 Er2 C22' K2 119.7(8) . . . . ? C25 Er2 C22' K2 -110.3(10) . . . . ? C27 Er2 C22' K2 101.3(13) . . . . ? C32 Er2 C22' K2 -130.6(7) . . . . ? C31 Er2 C22' K2 -155.8(9) . . . . ? C30 Er2 C22' K2 174.0(9) . . . . ? C18' Er2 C22' K2 -1.2(7) . . . . ? C20' Er2 C22' K2 52.3(7) . . . . ? C19 Er2 C22' K2 40.5(6) . . . . ? C17 Er2 C22' K2 -18.0(6) . . . . ? C18 K2 C22' C21' 59.1(12) . . . . ? C19' K2 C22' C21' 45.2(11) . . . . ? C17 K2 C22' C21' 87.7(12) . . . . ? C24 K2 C22' C21' 113.7(13) . . . . ? C19 K2 C22' C21' 33.2(11) . . . . ? C20' K2 C22' C21' 21.4(11) . . . . ? C20 K2 C22' C21' 10.5(12) . . . . ? C15 K2 C22' C21' -139.3(12) . . . . ? C18' K2 C22' C21' 72.3(12) . . . . ? C16 K2 C22' C21' -168.2(11) . . . . ? C17' K2 C22' C21' 99.9(12) . . . . ? C18 K2 C22' C23' -84.0(13) . . . . ? C19' K2 C22' C23' -97.9(13) . . . . ? C17 K2 C22' C23' -55.5(13) . . . . ? C21' K2 C22' C23' -143(2) . . . . ? C24 K2 C22' C23' -29.4(12) . . . . ? C19 K2 C22' C23' -109.9(14) . . . . ? C20' K2 C22' C23' -121.8(15) . . . . ? C20 K2 C22' C23' -132.6(17) . . . . ? C15 K2 C22' C23' 77.6(14) . . . . ? C18' K2 C22' C23' -70.8(13) . . . . ? C16 K2 C22' C23' 48.7(16) . . . . ? C17' K2 C22' C23' -43.3(12) . . . . ? C18 K2 C22' Er2 -12.1(6) . . . . ? C19' K2 C22' Er2 -25.9(6) . . . . ? C17 K2 C22' Er2 16.5(6) . . . . ? C21' K2 C22' Er2 -71.2(11) . . . . ? C24 K2 C22' Er2 42.5(6) . . . . ? C19 K2 C22' Er2 -38.0(6) . . . . ? C20' K2 C22' Er2 -49.8(6) . . . . ? C20 K2 C22' Er2 -60.7(8) . . . . ? C15 K2 C22' Er2 149.5(6) . . . . ? C18' K2 C22' Er2 1.1(6) . . . . ? C16 K2 C22' Er2 120.6(8) . . . . ? C17' K2 C22' Er2 28.7(6) . . . . ? C21' C22' C23' C24' 4(6) . . . . ? Er2 C22' C23' C24' -48(4) . . . . ? K2 C22' C23' C24' 56(4) . . . . ? C21' C22' C23' Er2 52(3) . . . . ? K2 C22' C23' Er2 103.9(4) . . . . ? C21' C22' C23' K2 -52(3) . . . . ? Er2 C22' C23' K2 -103.9(4) . . . . ? C26 Er2 C23' C24' -35.2(19) . . . . ? C29 Er2 C23' C24' -166.4(14) . . . . ? C28 Er2 C23' C24' 173.1(15) . . . . ? C25 Er2 C23' C24' -55.0(16) . . . . ? C27 Er2 C23' C24' 0(9) . . . . ? C32 Er2 C23' C24' -81.4(16) . . . . ? C31 Er2 C23' C24' -111.7(16) . . . . ? C30 Er2 C23' C24' -141.1(15) . . . . ? C18' Er2 C23' C24' 43.9(13) . . . . ? C20' Er2 C23' C24' 103.0(14) . . . . ? C19 Er2 C23' C24' 88.1(14) . . . . ? C17 Er2 C23' C24' 30.5(13) . . . . ? C26 Er2 C23' C22' 176.7(12) . . . . ? C29 Er2 C23' C22' 45.5(17) . . . . ? C28 Er2 C23' C22' 25(2) . . . . ? C25 Er2 C23' C22' 156.9(14) . . . . ? C27 Er2 C23' C22' -148(7) . . . . ? C32 Er2 C23' C22' 130.5(15) . . . . ? C31 Er2 C23' C22' 100.2(16) . . . . ? C30 Er2 C23' C22' 70.8(15) . . . . ? C18' Er2 C23' C22' -104.2(14) . . . . ? C20' Er2 C23' C22' -45.1(13) . . . . ? C19 Er2 C23' C22' -60.0(14) . . . . ? C17 Er2 C23' C22' -117.6(15) . . . . ? C26 Er2 C23' K2 -109.6(10) . . . . ? C29 Er2 C23' K2 119.2(8) . . . . ? C28 Er2 C23' K2 98.8(14) . . . . ? C25 Er2 C23' K2 -129.4(7) . . . . ? C27 Er2 C23' K2 -74(8) . . . . ? C32 Er2 C23' K2 -155.7(9) . . . . ? C31 Er2 C23' K2 173.9(9) . . . . ? C30 Er2 C23' K2 144.6(8) . . . . ? C18' Er2 C23' K2 -30.4(7) . . . . ? C20' Er2 C23' K2 28.6(6) . . . . ? C19 Er2 C23' K2 13.7(6) . . . . ? C17 Er2 C23' K2 -43.9(6) . . . . ? C18 K2 C23' C24' -57.3(13) . . . . ? C19' K2 C23' C24' -71.7(13) . . . . ? C17 K2 C23' C24' -31.1(12) . . . . ? C21' K2 C23' C24' -123.6(14) . . . . ? C24 K2 C23' C24' -8.9(13) . . . . ? C19 K2 C23' C24' -85.1(13) . . . . ? C20' K2 C23' C24' -98.9(13) . . . . ? C20 K2 C23' C24' -111.1(14) . . . . ? C15 K2 C23' C24' 98.3(14) . . . . ? C18' K2 C23' C24' -45.1(12) . . . . ? C16 K2 C23' C24' 69.3(14) . . . . ? C17' K2 C23' C24' -20.3(11) . . . . ? C18 K2 C23' C22' 86.7(13) . . . . ? C19' K2 C23' C22' 72.4(13) . . . . ? C17 K2 C23' C22' 112.9(14) . . . . ? C21' K2 C23' C22' 20.5(11) . . . . ? C24 K2 C23' C22' 135.2(18) . . . . ? C19 K2 C23' C22' 59.0(13) . . . . ? C20' K2 C23' C22' 45.2(12) . . . . ? C20 K2 C23' C22' 32.9(12) . . . . ? C15 K2 C23' C22' -117.6(13) . . . . ? C18' K2 C23' C22' 99.0(13) . . . . ? C16 K2 C23' C22' -146.7(13) . . . . ? C17' K2 C23' C22' 123.8(15) . . . . ? C18 K2 C23' Er2 15.3(6) . . . . ? C19' K2 C23' Er2 1.0(6) . . . . ? C17 K2 C23' Er2 41.5(6) . . . . ? C21' K2 C23' Er2 -51.0(6) . . . . ? C24 K2 C23' Er2 63.8(9) . . . . ? C19 K2 C23' Er2 -12.5(6) . . . . ? C20' K2 C23' Er2 -26.3(6) . . . . ? C20 K2 C23' Er2 -38.5(6) . . . . ? C15 K2 C23' Er2 170.9(6) . . . . ? C18' K2 C23' Er2 27.6(6) . . . . ? C16 K2 C23' Er2 141.9(7) . . . . ? C17' K2 C23' Er2 52.3(7) . . . . ? C22' C23' C24' C17' -1(6) . . . . ? Er2 C23' C24' C17' -49(3) . . . . ? K2 C23' C24' C17' 55(3) . . . . ? C22' C23' C24' Er2 47(4) . . . . ? K2 C23' C24' Er2 103.4(4) . . . . ? C22' C23' C24' K2 -56(4) . . . . ? Er2 C23' C24' K2 -103.4(4) . . . . ? C18' C17' C24' C23' 2(6) . . . . ? Er2 C17' C24' C23' 49(3) . . . . ? K2 C17' C24' C23' -55(3) . . . . ? C18' C17' C24' Er2 -46(3) . . . . ? K2 C17' C24' Er2 -103.7(4) . . . . ? C18' C17' C24' K2 57(3) . . . . ? Er2 C17' C24' K2 103.7(4) . . . . ? C26 Er2 C24' C23' 158.1(13) . . . . ? C29 Er2 C24' C23' 25(2) . . . . ? C28 Er2 C24' C23' -142(7) . . . . ? C25 Er2 C24' C23' 132.8(15) . . . . ? C27 Er2 C24' C23' -180.0(12) . . . . ? C32 Er2 C24' C23' 101.4(15) . . . . ? C31 Er2 C24' C23' 72.1(15) . . . . ? C30 Er2 C24' C23' 48.0(16) . . . . ? C18' Er2 C24' C23' -127.1(15) . . . . ? C20' Er2 C24' C23' -73.4(14) . . . . ? C19 Er2 C24' C23' -89.1(14) . . . . ? C17 Er2 C24' C23' -136.8(18) . . . . ? C26 Er2 C24' C17' -55.4(15) . . . . ? C29 Er2 C24' C17' 171.7(14) . . . . ? C28 Er2 C24' C17' 5(8) . . . . ? C25 Er2 C24' C17' -80.6(15) . . . . ? C27 Er2 C24' C17' -33.4(19) . . . . ? C32 Er2 C24' C17' -112.1(15) . . . . ? C31 Er2 C24' C17' -141.3(14) . . . . ? C30 Er2 C24' C17' -165.4(13) . . . . ? C18' Er2 C24' C17' 19.4(12) . . . . ? C20' Er2 C24' C17' 73.2(13) . . . . ? C19 Er2 C24' C17' 57.4(13) . . . . ? C17 Er2 C24' C17' 9.7(13) . . . . ? C26 Er2 C24' K2 -128.2(7) . . . . ? C29 Er2 C24' K2 98.9(14) . . . . ? C28 Er2 C24' K2 -68(8) . . . . ? C25 Er2 C24' K2 -153.5(9) . . . . ? C27 Er2 C24' K2 -106.3(10) . . . . ? C32 Er2 C24' K2 175.1(9) . . . . ? C31 Er2 C24' K2 145.8(8) . . . . ? C30 Er2 C24' K2 121.7(8) . . . . ? C18' Er2 C24' K2 -53.4(7) . . . . ? C20' Er2 C24' K2 0.3(7) . . . . ? C19 Er2 C24' K2 -15.4(7) . . . . ? C17 Er2 C24' K2 -63.1(9) . . . . ? C18 K2 C24' C23' 111.6(14) . . . . ? C19' K2 C24' C23' 98.8(13) . . . . ? C17 K2 C24' C23' 133.7(17) . . . . ? C21' K2 C24' C23' 43.8(11) . . . . ? C24 K2 C24' C23' 152(4) . . . . ? C19 K2 C24' C23' 85.8(13) . . . . ? C20' K2 C24' C23' 71.5(12) . . . . ? C20 K2 C24' C23' 58.4(12) . . . . ? C15 K2 C24' C23' -95.0(13) . . . . ? C18' K2 C24' C23' 121.8(14) . . . . ? C16 K2 C24' C23' -121.9(13) . . . . ? C17' K2 C24' C23' 144(2) . . . . ? C18 K2 C24' C17' -31.9(12) . . . . ? C19' K2 C24' C17' -44.8(12) . . . . ? C17 K2 C24' C17' -9.8(13) . . . . ? C21' K2 C24' C17' -99.7(13) . . . . ? C24 K2 C24' C17' 9(3) . . . . ? C19 K2 C24' C17' -57.7(12) . . . . ? C20' K2 C24' C17' -72.0(12) . . . . ? C20 K2 C24' C17' -85.1(13) . . . . ? C15 K2 C24' C17' 121.4(13) . . . . ? C18' K2 C24' C17' -21.7(11) . . . . ? C16 K2 C24' C17' 94.5(14) . . . . ? C18 K2 C24' Er2 39.9(6) . . . . ? C19' K2 C24' Er2 27.0(6) . . . . ? C17 K2 C24' Er2 61.9(9) . . . . ? C21' K2 C24' Er2 -28.0(6) . . . . ? C24 K2 C24' Er2 80(3) . . . . ? C19 K2 C24' Er2 14.0(6) . . . . ? C20' K2 C24' Er2 -0.3(6) . . . . ? C20 K2 C24' Er2 -13.4(6) . . . . ? C15 K2 C24' Er2 -166.8(7) . . . . ? C18' K2 C24' Er2 50.0(7) . . . . ? C16 K2 C24' Er2 166.3(7) . . . . ? C17' K2 C24' Er2 71.8(12) . . . . ? C29 Er2 C25 C26 -71.9(10) . . . . ? C28 Er2 C25 C26 -41.3(9) . . . . ? C27 Er2 C25 C26 -17.5(9) . . . . ? C32 Er2 C25 C26 -145.5(14) . . . . ? C31 Er2 C25 C26 -126.4(10) . . . . ? C30 Er2 C25 C26 -102.6(10) . . . . ? C18' Er2 C25 C26 74.2(12) . . . . ? C20' Er2 C25 C26 33.3(18) . . . . ? C19 Er2 C25 C26 42.1(14) . . . . ? C17 Er2 C25 C26 90.2(12) . . . . ? C26 Er2 C25 C32 145.5(14) . . . . ? C29 Er2 C25 C32 73.6(9) . . . . ? C28 Er2 C25 C32 104.2(10) . . . . ? C27 Er2 C25 C32 128.0(10) . . . . ? C31 Er2 C25 C32 19.1(9) . . . . ? C30 Er2 C25 C32 42.9(9) . . . . ? C18' Er2 C25 C32 -140.3(12) . . . . ? C20' Er2 C25 C32 178.8(13) . . . . ? C19 Er2 C25 C32 -172.3(11) . . . . ? C17 Er2 C25 C32 -124.2(12) . . . . ? C32 C25 C26 C27 -1(3) . . . . ? Er2 C25 C26 C27 47(2) . . . . ? C32 C25 C26 Er2 -48.3(16) . . . . ? C29 Er2 C26 C27 -44.0(10) . . . . ? C28 Er2 C26 C27 -19.3(10) . . . . ? C25 Er2 C26 C27 -149.7(16) . . . . ? C32 Er2 C26 C27 -129.4(12) . . . . ? C31 Er2 C26 C27 -104.9(11) . . . . ? C30 Er2 C26 C27 -75.1(10) . . . . ? C18' Er2 C26 C27 100.2(13) . . . . ? C20' Er2 C26 C27 47.8(14) . . . . ? C19 Er2 C26 C27 59.3(13) . . . . ? C17 Er2 C26 C27 117.1(13) . . . . ? C29 Er2 C26 C25 105.7(10) . . . . ? C28 Er2 C26 C25 130.4(10) . . . . ? C27 Er2 C26 C25 149.7(16) . . . . ? C32 Er2 C26 C25 20.2(9) . . . . ? C31 Er2 C26 C25 44.8(9) . . . . ? C30 Er2 C26 C25 74.5(10) . . . . ? C18' Er2 C26 C25 -110.2(13) . . . . ? C20' Er2 C26 C25 -162.5(11) . . . . ? C19 Er2 C26 C25 -151.1(12) . . . . ? C17 Er2 C26 C25 -93.2(12) . . . . ? C25 C26 C27 C28 0(3) . . . . ? Er2 C26 C27 C28 47.4(17) . . . . ? C25 C26 C27 Er2 -47.0(19) . . . . ? C29 Er2 C27 C26 127.6(12) . . . . ? C28 Er2 C27 C26 146.4(16) . . . . ? C25 Er2 C27 C26 17.6(10) . . . . ? C32 Er2 C27 C26 42.5(10) . . . . ? C31 Er2 C27 C26 72.3(11) . . . . ? C30 Er2 C27 C26 102.1(11) . . . . ? C18' Er2 C27 C26 -82.9(13) . . . . ? C20' Er2 C27 C26 -141.6(12) . . . . ? C19 Er2 C27 C26 -127.2(13) . . . . ? C17 Er2 C27 C26 -69.1(13) . . . . ? C26 Er2 C27 C28 -146.4(16) . . . . ? C29 Er2 C27 C28 -18.8(9) . . . . ? C25 Er2 C27 C28 -128.8(10) . . . . ? C32 Er2 C27 C28 -103.9(10) . . . . ? C31 Er2 C27 C28 -74.1(10) . . . . ? C30 Er2 C27 C28 -44.3(10) . . . . ? C18' Er2 C27 C28 130.7(12) . . . . ? C20' Er2 C27 C28 72.0(12) . . . . ? C19 Er2 C27 C28 86.4(12) . . . . ? C17 Er2 C27 C28 144.5(12) . . . . ? C26 C27 C28 C29 0(3) . . . . ? Er2 C27 C28 C29 46.8(18) . . . . ? C26 C27 C28 Er2 -47.2(17) . . . . ? C26 Er2 C28 C27 19.4(9) . . . . ? C29 Er2 C28 C27 148.1(15) . . . . ? C25 Er2 C28 C27 43.0(9) . . . . ? C32 Er2 C28 C27 73.8(10) . . . . ? C31 Er2 C28 C27 103.4(10) . . . . ? C30 Er2 C28 C27 127.5(10) . . . . ? C18' Er2 C28 C27 -57.2(12) . . . . ? C20' Er2 C28 C27 -111.4(13) . . . . ? C19 Er2 C28 C27 -95.6(12) . . . . ? C17 Er2 C28 C27 -47.7(13) . . . . ? C26 Er2 C28 C29 -128.6(11) . . . . ? C25 Er2 C28 C29 -105.1(10) . . . . ? C27 Er2 C28 C29 -148.1(15) . . . . ? C32 Er2 C28 C29 -74.3(10) . . . . ? C31 Er2 C28 C29 -44.6(9) . . . . ? C30 Er2 C28 C29 -20.5(9) . . . . ? C18' Er2 C28 C29 154.8(11) . . . . ? C20' Er2 C28 C29 100.5(13) . . . . ? C19 Er2 C28 C29 116.4(12) . . . . ? C17 Er2 C28 C29 164.2(11) . . . . ? C27 C28 C29 C30 3(3) . . . . ? Er2 C28 C29 C30 50.0(17) . . . . ? C27 C28 C29 Er2 -47.1(18) . . . . ? C26 Er2 C29 C30 -102.2(10) . . . . ? C28 Er2 C29 C30 -144.8(14) . . . . ? C25 Er2 C29 C30 -72.4(10) . . . . ? C27 Er2 C29 C30 -126.6(10) . . . . ? C32 Er2 C29 C30 -41.5(10) . . . . ? C31 Er2 C29 C30 -18.1(10) . . . . ? C18' Er2 C29 C30 174.9(12) . . . . ? C20' Er2 C29 C30 133.5(12) . . . . ? C19 Er2 C29 C30 146.8(11) . . . . ? C17 Er2 C29 C30 176.8(18) . . . . ? C26 Er2 C29 C28 42.6(9) . . . . ? C25 Er2 C29 C28 72.5(10) . . . . ? C27 Er2 C29 C28 18.2(8) . . . . ? C32 Er2 C29 C28 103.3(10) . . . . ? C31 Er2 C29 C28 126.7(10) . . . . ? C30 Er2 C29 C28 144.8(14) . . . . ? C18' Er2 C29 C28 -40.2(15) . . . . ? C20' Er2 C29 C28 -81.7(12) . . . . ? C19 Er2 C29 C28 -68.4(12) . . . . ? C17 Er2 C29 C28 -38(2) . . . . ? C28 C29 C30 C31 -4(3) . . . . ? Er2 C29 C30 C31 46(2) . . . . ? C28 C29 C30 Er2 -49.8(17) . . . . ? C26 Er2 C30 C31 -73.3(12) . . . . ? C29 Er2 C30 C31 -148.2(17) . . . . ? C28 Er2 C30 C31 -127.7(13) . . . . ? C25 Er2 C30 C31 -43.0(11) . . . . ? C27 Er2 C30 C31 -103.6(12) . . . . ? C32 Er2 C30 C31 -18.2(11) . . . . ? C18' Er2 C30 C31 175(7) . . . . ? C20' Er2 C30 C31 157.5(13) . . . . ? C19 Er2 C30 C31 167.6(11) . . . . ? C17 Er2 C30 C31 36(3) . . . . ? C26 Er2 C30 C29 74.8(10) . . . . ? C28 Er2 C30 C29 20.4(9) . . . . ? C25 Er2 C30 C29 105.2(10) . . . . ? C27 Er2 C30 C29 44.6(9) . . . . ? C32 Er2 C30 C29 130.0(11) . . . . ? C31 Er2 C30 C29 148.2(17) . . . . ? C18' Er2 C30 C29 -36(8) . . . . ? C20' Er2 C30 C29 -54.3(12) . . . . ? C19 Er2 C30 C29 -44.3(13) . . . . ? C17 Er2 C30 C29 -175(3) . . . . ? C29 C30 C31 C32 1(4) . . . . ? Er2 C30 C31 C32 46(2) . . . . ? C29 C30 C31 Er2 -45(2) . . . . ? C26 Er2 C31 C32 -44.8(10) . . . . ? C29 Er2 C31 C32 -129.7(11) . . . . ? C28 Er2 C31 C32 -104.4(10) . . . . ? C25 Er2 C31 C32 -19.8(9) . . . . ? C27 Er2 C31 C32 -74.6(10) . . . . ? C30 Er2 C31 C32 -148.5(18) . . . . ? C18' Er2 C31 C32 32.5(19) . . . . ? C20' Er2 C31 C32 175.7(12) . . . . ? C19 Er2 C31 C32 -177.0(16) . . . . ? C17 Er2 C31 C32 43.1(15) . . . . ? C26 Er2 C31 C30 103.7(12) . . . . ? C29 Er2 C31 C30 18.8(11) . . . . ? C28 Er2 C31 C30 44.1(12) . . . . ? C25 Er2 C31 C30 128.7(13) . . . . ? C27 Er2 C31 C30 73.9(12) . . . . ? C32 Er2 C31 C30 148.5(18) . . . . ? C18' Er2 C31 C30 -179.1(14) . . . . ? C20' Er2 C31 C30 -35.8(18) . . . . ? C19 Er2 C31 C30 -29(2) . . . . ? C17 Er2 C31 C30 -168.4(12) . . . . ? C30 C31 C32 C25 2(3) . . . . ? Er2 C31 C32 C25 48.4(17) . . . . ? C30 C31 C32 Er2 -47(2) . . . . ? C26 C25 C32 C31 -1(3) . . . . ? Er2 C25 C32 C31 -48.8(17) . . . . ? C26 C25 C32 Er2 48.1(16) . . . . ? C26 Er2 C32 C31 126.7(11) . . . . ? C29 Er2 C32 C31 42.4(10) . . . . ? C28 Er2 C32 C31 73.3(10) . . . . ? C25 Er2 C32 C31 146.5(15) . . . . ? C27 Er2 C32 C31 103.0(10) . . . . ? C30 Er2 C32 C31 18.2(10) . . . . ? C18' Er2 C32 C31 -163.3(11) . . . . ? C20' Er2 C32 C31 -28(7) . . . . ? C19 Er2 C32 C31 175(3) . . . . ? C17 Er2 C32 C31 -150.3(12) . . . . ? C26 Er2 C32 C25 -19.8(8) . . . . ? C29 Er2 C32 C25 -104.0(10) . . . . ? C28 Er2 C32 C25 -73.2(10) . . . . ? C27 Er2 C32 C25 -43.5(9) . . . . ? C31 Er2 C32 C25 -146.5(15) . . . . ? C30 Er2 C32 C25 -128.3(10) . . . . ? C18' Er2 C32 C25 50.3(12) . . . . ? C20' Er2 C32 C25 -174(6) . . . . ? C19 Er2 C32 C25 28(3) . . . . ? C17 Er2 C32 C25 63.2(12) . . . . ? C36 O1 C33 C34 -7.3(16) . . . . ? K1 O1 C33 C34 177.2(9) . . . . ? O1 C33 C34 C35 25.3(17) . . . . ? C33 C34 C35 C36 -32.6(17) . . . . ? C33 O1 C36 C35 -14.1(16) . . . . ? K1 O1 C36 C35 161.6(9) . . . . ? C34 C35 C36 O1 29.9(17) . . . . ? C40 O2 C37 C38 -28(2) . . . . ? K1 O2 C37 C38 139.1(14) . . . . ? O2 C37 C38 C39 31(2) . . . . ? C37 C38 C39 C40 -23(3) . . . . ? C37 O2 C40 C39 14(2) . . . . ? K1 O2 C40 C39 -155.4(13) . . . . ? C38 C39 C40 O2 6(2) . . . . ? C44 O3 C41 C42 -7(2) . . . . ? K1 O3 C41 C42 149.3(14) . . . . ? C41 O3 C44 C43 0(2) . . . . ? K1 O3 C44 C43 -153.4(12) . . . . ? O3 C44 C43 C42 8(2) . . . . ? C44 C43 C42 C41 -13(3) . . . . ? O3 C41 C42 C43 13(3) . . . . ? C48 O4 C45 C46 13.6(19) . . . . ? K1 O4 C45 C46 -131.8(12) . . . . ? C45 O4 C48 C47 4(2) . . . . ? K1 O4 C48 C47 147.8(12) . . . . ? C46 C47 C48 O4 -19(2) . . . . ? C48 C47 C46 C45 26(2) . . . . ? O4 C45 C46 C47 -25(2) . . . . ? _diffrn_measured_fraction_theta_max 0.900 _diffrn_reflns_theta_full 30.55 _diffrn_measured_fraction_theta_full 0.900 _refine_diff_density_max 4.926 _refine_diff_density_min -4.549 _refine_diff_density_rms 0.309 data_mm272_5 _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C48 H64 Gd2 K2 O4' _chemical_formula_weight 1097.69 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'K' 'K' 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Gd' 'Gd' -0.1653 3.9035 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.5506(3) _cell_length_b 12.9933(3) _cell_length_c 16.7384(4) _cell_angle_alpha 107.0633(13) _cell_angle_beta 98.5557(14) _cell_angle_gamma 112.1212(13) _cell_volume 2311.45(10) _cell_formula_units_Z 2 _cell_measurement_temperature 200(2) _cell_measurement_reflns_used 9884 _cell_measurement_theta_min 2.43 _cell_measurement_theta_max 28.84 _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_density_meas n/a _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.577 _exptl_crystal_F_000 1100 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.170 _exptl_crystal_size_mid 0.130 _exptl_crystal_size_min 0.120 _exptl_absorpt_coefficient_mu 3.065 _shelx_estimated_absorpt_T_min 0.624 _shelx_estimated_absorpt_T_max 0.710 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.624 _exptl_absorpt_correction_T_max 0.710 _exptl_absorpt_process_details 'SADABS, Bruker (2003)' _exptl_special_details ; Data collection is performed with four batch runs at phi = 0.00 deg (600 frames), at phi = 90.00 deg (600 frames), at phi = 180.00 deg (600 frames), and at phi = 270.00 deg (600 frames). A fifth batch run is collected at phi = 0.00 deg (50 frames) to monitor crystal and diffractometer stability. Frame width = 0.30 deg in omega. Data is merged, corrected for decay (if any), and treated with multi-scan absorption corrections (if required). All symmetry-equivalent reflections are merged for centrosymmetric data. Friedel pairs are not merged for noncentrosymmetric data. ; _diffrn_ambient_temperature 200(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 13089 _diffrn_reflns_av_unetI/netI 0.0566 _diffrn_reflns_av_R_equivalents ? _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_theta_min 1.806 _diffrn_reflns_theta_max 30.574 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.925 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.925 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.925 _diffrn_reflns_point_group_measured_fraction_full 0.997 _reflns_number_total 13089 _reflns_number_gt 9370 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX II, Bruker (2009)' _computing_cell_refinement 'APEX II, Bruker (2009)' _computing_data_reduction 'XPREP, Bruker (2009)' _computing_structure_solution 'SHELXS-03 (Sheldrick, 2003)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'SHELXTL, Bruker (2004)' _computing_publication_material 'SHELXTL, Bruker (2004)' _refine_special_details ; Refined as a 2-component twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0429P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 13089 _refine_ls_number_parameters 587 _refine_ls_number_restraints 300 _refine_ls_R_factor_all 0.0723 _refine_ls_R_factor_gt 0.0409 _refine_ls_wR_factor_ref 0.0948 _refine_ls_wR_factor_gt 0.0826 _refine_ls_goodness_of_fit_ref 1.034 _refine_ls_restrained_S_all 1.023 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Gd1 Gd -0.17177(2) 0.97603(2) 0.29010(2) 0.02901(7) Uani 1 1 d . . . . . Gd2 Gd 0.19965(2) 0.50382(2) 0.23295(2) 0.02552(6) Uani 1 1 d . . . . . K1 K -0.00069(12) 0.72571(11) 0.23533(8) 0.0476(3) Uani 1 1 d . . . . . K2 K 0.40609(9) 0.27945(9) 0.22585(6) 0.0336(2) Uani 1 1 d . . . . . O1 O 0.2995(4) 0.0613(3) 0.0938(3) 0.0673(13) Uani 1 1 d . . . . . O2 O 0.3721(4) 0.1673(3) 0.3392(2) 0.0578(11) Uani 1 1 d . . . . . O3 O 0.6232(4) 0.3948(3) 0.3469(3) 0.0566(11) Uani 1 1 d . . . . . O4 O 0.5420(4) 0.2989(4) 0.1151(2) 0.0554(10) Uani 1 1 d . . . . . C1 C -0.1295(6) 1.1752(5) 0.4173(4) 0.0553(17) Uani 1 1 d . . . . . H1A H -0.0682 1.2262 0.4712 0.066 Uiso 1 1 calc R U . . . C2 C -0.2246(6) 1.0861(6) 0.4264(4) 0.0553(16) Uani 1 1 d . . . . . H2A H -0.2133 1.0909 0.4850 0.066 Uiso 1 1 calc R U . . . C3 C -0.3321(7) 0.9915(6) 0.3706(5) 0.0620(19) Uani 1 1 d . . . . . H3A H -0.3760 0.9454 0.3997 0.074 Uiso 1 1 calc R U . . . C4 C -0.3922(5) 0.9472(6) 0.2808(6) 0.066(2) Uani 1 1 d . . . . . H4A H -0.4677 0.8790 0.2637 0.080 Uiso 1 1 calc R U . . . C5 C -0.3669(7) 0.9797(7) 0.2121(5) 0.070(2) Uani 1 1 d . . . . . H5A H -0.4281 0.9272 0.1585 0.085 Uiso 1 1 calc R U . . . C6 C -0.2724(9) 1.0718(8) 0.2022(4) 0.074(3) Uani 1 1 d . . . . . H6A H -0.2867 1.0702 0.1444 0.089 Uiso 1 1 calc R U . . . C7 C -0.1615(8) 1.1656(7) 0.2586(6) 0.071(2) Uani 1 1 d . . . . . H7A H -0.1160 1.2108 0.2297 0.085 Uiso 1 1 calc R U . . . C8 C -0.1019(7) 1.2083(5) 0.3489(5) 0.0653(19) Uani 1 1 d . . . . . H8A H -0.0252 1.2751 0.3664 0.078 Uiso 1 1 calc R U . . . C9 C 0.0521(13) 0.9949(13) 0.3075(13) 0.039(4) Uani 0.5 1 d D U P A 1 H9A H 0.1264 1.0657 0.3311 0.047 Uiso 0.5 1 calc R U P A 1 C10 C 0.0174(16) 0.9517(17) 0.3724(8) 0.037(4) Uani 0.5 1 d D U P A 1 H10A H 0.0779 0.9939 0.4271 0.044 Uiso 0.5 1 calc R U P A 1 C11 C -0.085(2) 0.8618(19) 0.3739(9) 0.041(4) Uani 0.5 1 d D U P A 1 H11A H -0.0793 0.8570 0.4298 0.050 Uiso 0.5 1 calc R U P A 1 C12 C -0.1963(16) 0.7753(15) 0.3113(14) 0.038(3) Uani 0.5 1 d D U P A 1 H12A H -0.2513 0.7318 0.3364 0.046 Uiso 0.5 1 calc R U P A 1 C13 C -0.2447(13) 0.7386(13) 0.2205(13) 0.044(4) Uani 0.5 1 d D U P A 1 H13A H -0.3219 0.6716 0.1982 0.053 Uiso 0.5 1 calc R U P A 1 C14 C -0.2074(18) 0.7764(17) 0.1561(9) 0.039(4) Uani 0.5 1 d D U P A 1 H14A H -0.2645 0.7290 0.1000 0.047 Uiso 0.5 1 calc R U P A 1 C15 C -0.104(2) 0.8690(19) 0.1547(8) 0.040(4) Uani 0.5 1 d D U P A 1 H15A H -0.1088 0.8708 0.0979 0.048 Uiso 0.5 1 calc R U P A 1 C16 C 0.0049(18) 0.9600(16) 0.2173(12) 0.037(4) Uani 0.5 1 d D U P A 1 H16A H 0.0575 1.0077 0.1931 0.045 Uiso 0.5 1 calc R U P A 1 C9' C 0.0459(13) 0.9824(14) 0.3394(13) 0.040(4) Uani 0.5 1 d D U P A 2 H9'A H 0.1205 1.0445 0.3792 0.048 Uiso 0.5 1 calc R U P A 2 C10' C -0.0252(17) 0.913(2) 0.3800(8) 0.043(5) Uani 0.5 1 d D U P A 2 H10B H 0.0128 0.9401 0.4406 0.052 Uiso 0.5 1 calc R U P A 2 C11' C -0.138(2) 0.8156(18) 0.3520(11) 0.042(4) Uani 0.5 1 d D U P A 2 H11B H -0.1580 0.7900 0.3976 0.050 Uiso 0.5 1 calc R U P A 2 C12' C -0.2289(14) 0.7454(12) 0.2709(14) 0.042(4) Uani 0.5 1 d D U P A 2 H12B H -0.2974 0.6855 0.2756 0.050 Uiso 0.5 1 calc R U P A 2 C13' C -0.2428(12) 0.7426(14) 0.1861(11) 0.036(3) Uani 0.5 1 d D U P A 2 H13B H -0.3169 0.6792 0.1463 0.043 Uiso 0.5 1 calc R U P A 2 C14' C -0.1741(18) 0.8105(18) 0.1462(8) 0.033(3) Uani 0.5 1 d D U P A 2 H14B H -0.2133 0.7845 0.0859 0.039 Uiso 0.5 1 calc R U P A 2 C15' C -0.0599(19) 0.9089(18) 0.1737(11) 0.037(4) Uani 0.5 1 d D U P A 2 H15B H -0.0399 0.9324 0.1271 0.044 Uiso 0.5 1 calc R U P A 2 C16' C 0.0323(14) 0.9812(15) 0.2536(14) 0.038(4) Uani 0.5 1 d D U P A 2 H16B H 0.0997 1.0420 0.2487 0.045 Uiso 0.5 1 calc R U P A 2 C17 C 0.2541(5) 0.7367(4) 0.2942(5) 0.0543(17) Uani 1 1 d . . . . . H17A H 0.3279 0.8069 0.3253 0.065 Uiso 1 1 calc R U . . . C18 C 0.1948(6) 0.6917(5) 0.3496(3) 0.0551(17) Uani 1 1 d . . . . . H18A H 0.2373 0.7393 0.4095 0.066 Uiso 1 1 calc R U . . . C19 C 0.0876(6) 0.5930(6) 0.3379(4) 0.0473(14) Uani 1 1 d . . . . . H19A H 0.0737 0.5903 0.3917 0.057 Uiso 1 1 calc R U . . . C20 C -0.0039(5) 0.4974(5) 0.2651(4) 0.0481(14) Uani 1 1 d . . . . . H20A H -0.0644 0.4436 0.2809 0.058 Uiso 1 1 calc R U . . . C21 C -0.0264(5) 0.4629(4) 0.1743(4) 0.0487(15) Uani 1 1 d . . . . . H21A H -0.0987 0.3912 0.1429 0.058 Uiso 1 1 calc R U . . . C22 C 0.0328(5) 0.5094(5) 0.1192(3) 0.0475(14) Uani 1 1 d . . . . . H22A H -0.0093 0.4622 0.0591 0.057 Uiso 1 1 calc R U . . . C23 C 0.1388(6) 0.6088(6) 0.1318(4) 0.0495(15) Uani 1 1 d . . . . . H23A H 0.1516 0.6131 0.0781 0.059 Uiso 1 1 calc R U . . . C24 C 0.2299(5) 0.7026(5) 0.2034(5) 0.0492(15) Uani 1 1 d . . . . . H24A H 0.2900 0.7562 0.1873 0.059 Uiso 1 1 calc R U . . . C25 C 0.4272(5) 0.5482(4) 0.2838(5) 0.0501(16) Uani 1 1 d . . . . . H25A H 0.4998 0.6202 0.3133 0.060 Uiso 1 1 calc R U . . . C26 C 0.3751(6) 0.5038(5) 0.3408(3) 0.0510(16) Uani 1 1 d . . . . . H26A H 0.4198 0.5535 0.4001 0.061 Uiso 1 1 calc R U . . . C27 C 0.2724(6) 0.4035(6) 0.3326(4) 0.0510(16) Uani 1 1 d . . . . . H27A H 0.2650 0.4000 0.3875 0.061 Uiso 1 1 calc R U . . . C28 C 0.1781(5) 0.3071(5) 0.2623(4) 0.0471(14) Uani 1 1 d . . . . . H28A H 0.1209 0.2535 0.2803 0.056 Uiso 1 1 calc R U . . . C29 C 0.1491(5) 0.2721(4) 0.1716(5) 0.0548(17) Uani 1 1 d . . . . . H29A H 0.0768 0.1998 0.1423 0.066 Uiso 1 1 calc R U . . . C30 C 0.2009(6) 0.3177(5) 0.1131(3) 0.0515(16) Uani 1 1 d . . . . . H30A H 0.1549 0.2699 0.0537 0.062 Uiso 1 1 calc R U . . . C31 C 0.3038(6) 0.4166(6) 0.1223(4) 0.0513(16) Uani 1 1 d . . . . . H31A H 0.3118 0.4202 0.0675 0.062 Uiso 1 1 calc R U . . . C32 C 0.3994(6) 0.5130(5) 0.1924(5) 0.0556(17) Uani 1 1 d . . . . . H32A H 0.4575 0.5656 0.1744 0.067 Uiso 1 1 calc R U . . . C33 C 0.3647(7) -0.0075(7) 0.0806(6) 0.086(2) Uani 1 1 d . . . . . H33A H 0.4134 0.0037 0.1375 0.103 Uiso 1 1 calc R U . . . H33B H 0.4196 0.0184 0.0460 0.103 Uiso 1 1 calc R U . . . C34 C 0.2779(9) -0.1338(6) 0.0336(6) 0.090(3) Uani 1 1 d . . . . . H34A H 0.2886 -0.1828 0.0668 0.108 Uiso 1 1 calc R U . . . H34B H 0.2881 -0.1658 -0.0247 0.108 Uiso 1 1 calc R U . . . C35 C 0.1566(8) -0.1362(6) 0.0250(7) 0.100(3) Uani 1 1 d . . . . . H35A H 0.1007 -0.1924 -0.0338 0.119 Uiso 1 1 calc R U . . . H35B H 0.1220 -0.1606 0.0696 0.119 Uiso 1 1 calc R U . . . C36 C 0.1799(6) -0.0115(6) 0.0387(5) 0.0681(19) Uani 1 1 d . . . . . H36A H 0.1713 -0.0008 -0.0177 0.082 Uiso 1 1 calc R U . . . H36B H 0.1230 0.0097 0.0667 0.082 Uiso 1 1 calc R U . . . C37 C 0.3981(7) 0.2396(5) 0.4284(4) 0.0615(18) Uani 1 1 d D . . . . H37A H 0.3234 0.2270 0.4456 0.074 Uiso 0.5 1 calc R U P B 1 H37B H 0.4443 0.3259 0.4401 0.074 Uiso 0.5 1 calc R U P B 1 H37C H 0.3343 0.2657 0.4355 0.074 Uiso 0.5 1 calc R U P C 2 H37D H 0.4754 0.3122 0.4465 0.074 Uiso 0.5 1 calc R U P C 2 C38 C 0.4721(13) 0.1955(9) 0.4753(9) 0.063(5) Uani 0.5 1 d D . P D 1 H38A H 0.5566 0.2314 0.4745 0.075 Uiso 0.5 1 calc R U P D 1 H38B H 0.4701 0.2136 0.5366 0.075 Uiso 0.5 1 calc R U P D 1 C38' C 0.4054(19) 0.1723(11) 0.4843(8) 0.073(6) Uani 0.5 1 d D . P D 2 H38C H 0.3335 0.1481 0.5052 0.088 Uiso 0.5 1 calc R U P D 2 H38D H 0.4783 0.2202 0.5353 0.088 Uiso 0.5 1 calc R U P D 2 C39 C 0.4114(9) 0.0649(6) 0.4238(5) 0.084(3) Uani 1 1 d D . . . . H39A H 0.4658 0.0275 0.4314 0.101 Uiso 0.5 1 calc R U P D 1 H39B H 0.3383 0.0246 0.4398 0.101 Uiso 0.5 1 calc R U P D 1 H39C H 0.4933 0.0711 0.4405 0.101 Uiso 0.5 1 calc R U P D 2 H39D H 0.3539 -0.0094 0.4275 0.101 Uiso 0.5 1 calc R U P D 2 C40 C 0.3810(7) 0.0605(5) 0.3343(4) 0.0592(16) Uani 1 1 d . . . . . H40A H 0.4443 0.0545 0.3069 0.071 Uiso 1 1 calc R U . . . H40B H 0.3036 -0.0104 0.2985 0.071 Uiso 1 1 calc R U . . . C41 C 0.6769(5) 0.5190(5) 0.4016(4) 0.0521(15) Uani 1 1 d . . . . . H41A H 0.6405 0.5318 0.4500 0.063 Uiso 1 1 calc R U . . . H41B H 0.6647 0.5665 0.3676 0.063 Uiso 1 1 calc R U . . . C42 C 0.8065(6) 0.5558(5) 0.4364(4) 0.0556(15) Uani 1 1 d . . . . . H42A H 0.8413 0.6215 0.4949 0.067 Uiso 1 1 calc R U . . . H42B H 0.8515 0.5822 0.3966 0.067 Uiso 1 1 calc R U . . . C43 C 0.8071(6) 0.4425(6) 0.4409(4) 0.0604(16) Uani 1 1 d . . . . . H43A H 0.8842 0.4405 0.4367 0.072 Uiso 1 1 calc R U . . . H43B H 0.7930 0.4338 0.4957 0.072 Uiso 1 1 calc R U . . . C44 C 0.7055(6) 0.3474(6) 0.3633(5) 0.0657(18) Uani 1 1 d . . . . . H44A H 0.7351 0.3265 0.3121 0.079 Uiso 1 1 calc R U . . . H44B H 0.6661 0.2740 0.3752 0.079 Uiso 1 1 calc R U . . . C45 C 0.6512(7) 0.3998(7) 0.1382(4) 0.080(2) Uani 1 1 d . . . . . H45A H 0.7171 0.3862 0.1663 0.097 Uiso 1 1 calc R U . . . H45B H 0.6496 0.4702 0.1807 0.097 Uiso 1 1 calc R U . . . C46 C 0.6733(6) 0.4239(5) 0.0602(4) 0.0605(17) Uani 1 1 d . . . . . H46A H 0.7298 0.3940 0.0392 0.073 Uiso 1 1 calc R U . . . H46B H 0.7061 0.5110 0.0722 0.073 Uiso 1 1 calc R U . . . C47 C 0.5504(7) 0.3556(7) -0.0049(5) 0.078(2) Uani 1 1 d . . . . . H47A H 0.5098 0.4080 -0.0042 0.094 Uiso 1 1 calc R U . . . H47B H 0.5550 0.3213 -0.0647 0.094 Uiso 1 1 calc R U . . . C48 C 0.4860(6) 0.2587(6) 0.0254(4) 0.0649(18) Uani 1 1 d . . . . . H48A H 0.4003 0.2418 0.0150 0.078 Uiso 1 1 calc R U . . . H48B H 0.4904 0.1840 -0.0069 0.078 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Gd1 0.02993(13) 0.02907(11) 0.03239(12) 0.00996(9) 0.01018(10) 0.01845(10) Gd2 0.02684(12) 0.02481(11) 0.02831(11) 0.00961(8) 0.00708(9) 0.01568(9) K1 0.0518(8) 0.0448(6) 0.0601(7) 0.0193(5) 0.0156(6) 0.0364(6) K2 0.0331(5) 0.0318(5) 0.0356(5) 0.0104(4) 0.0083(4) 0.0167(4) O1 0.058(3) 0.036(2) 0.081(3) -0.0031(19) 0.005(2) 0.019(2) O2 0.089(3) 0.0397(19) 0.044(2) 0.0184(17) 0.012(2) 0.029(2) O3 0.038(2) 0.052(2) 0.061(3) 0.0066(19) -0.0047(19) 0.0199(19) O4 0.050(3) 0.064(2) 0.044(2) 0.0217(18) 0.015(2) 0.015(2) C1 0.055(4) 0.045(3) 0.044(3) -0.013(3) -0.006(3) 0.030(3) C2 0.075(5) 0.072(4) 0.038(3) 0.018(3) 0.025(3) 0.052(4) C3 0.065(5) 0.072(4) 0.085(5) 0.044(4) 0.056(4) 0.044(4) C4 0.029(3) 0.053(3) 0.101(6) 0.006(4) 0.020(4) 0.019(3) C5 0.057(4) 0.092(5) 0.050(4) -0.006(4) -0.007(3) 0.055(4) C6 0.122(8) 0.119(7) 0.045(3) 0.046(4) 0.035(4) 0.103(7) C7 0.102(7) 0.074(4) 0.110(6) 0.069(5) 0.073(6) 0.072(5) C8 0.062(4) 0.033(3) 0.101(6) 0.018(3) 0.024(4) 0.028(3) C9 0.033(6) 0.030(6) 0.050(9) 0.004(8) 0.014(7) 0.017(5) C10 0.033(9) 0.050(10) 0.028(6) 0.005(5) 0.000(6) 0.030(6) C11 0.050(13) 0.056(13) 0.037(7) 0.026(7) 0.010(6) 0.037(8) C12 0.050(10) 0.033(9) 0.044(9) 0.022(8) 0.024(7) 0.022(6) C13 0.041(6) 0.027(5) 0.040(9) -0.006(8) 0.012(8) 0.003(4) C14 0.047(10) 0.035(11) 0.028(6) 0.000(5) 0.000(6) 0.023(6) C15 0.059(13) 0.042(12) 0.028(5) 0.010(6) 0.015(6) 0.033(8) C16 0.048(10) 0.034(8) 0.040(8) 0.015(8) 0.024(7) 0.025(6) C9' 0.027(7) 0.036(7) 0.047(9) 0.010(7) -0.011(8) 0.016(5) C10' 0.030(10) 0.061(13) 0.036(6) 0.012(6) -0.002(6) 0.027(7) C11' 0.054(12) 0.046(11) 0.035(7) 0.021(7) 0.020(7) 0.026(7) C12' 0.046(8) 0.024(6) 0.043(8) 0.008(8) 0.018(8) 0.005(5) C13' 0.033(6) 0.035(6) 0.035(8) 0.002(7) 0.010(6) 0.018(5) C14' 0.041(9) 0.035(10) 0.028(5) 0.008(5) 0.012(5) 0.025(6) C15' 0.050(11) 0.037(11) 0.041(8) 0.026(8) 0.023(7) 0.026(7) C16' 0.027(7) 0.033(7) 0.055(10) 0.015(10) 0.019(8) 0.014(5) C17 0.040(3) 0.022(2) 0.086(5) 0.009(3) 0.004(3) 0.013(2) C18 0.063(4) 0.057(3) 0.034(3) -0.010(3) -0.012(3) 0.046(3) C19 0.070(4) 0.074(4) 0.038(3) 0.032(3) 0.031(3) 0.058(4) C20 0.038(3) 0.054(3) 0.084(4) 0.045(3) 0.035(3) 0.032(3) C21 0.028(3) 0.026(2) 0.074(4) 0.002(2) -0.003(3) 0.014(2) C22 0.054(4) 0.056(3) 0.033(3) 0.006(2) -0.002(2) 0.039(3) C23 0.066(4) 0.075(4) 0.047(3) 0.040(3) 0.029(3) 0.054(4) C24 0.046(3) 0.044(3) 0.089(5) 0.046(3) 0.036(3) 0.030(3) C25 0.021(2) 0.027(2) 0.085(5) 0.006(3) -0.001(3) 0.011(2) C26 0.061(4) 0.058(3) 0.032(3) -0.001(2) -0.006(3) 0.045(3) C27 0.083(5) 0.069(4) 0.049(3) 0.040(3) 0.040(3) 0.062(4) C28 0.047(3) 0.041(3) 0.080(4) 0.040(3) 0.036(3) 0.028(3) C29 0.036(3) 0.021(2) 0.091(5) 0.003(3) 0.003(3) 0.015(2) C30 0.061(4) 0.060(3) 0.031(3) -0.003(2) -0.003(3) 0.045(3) C31 0.079(5) 0.076(4) 0.044(3) 0.035(3) 0.039(3) 0.062(4) C32 0.050(4) 0.059(3) 0.102(5) 0.054(4) 0.051(4) 0.041(3) C33 0.066(5) 0.067(4) 0.105(6) 0.013(4) -0.003(4) 0.036(4) C34 0.115(8) 0.052(4) 0.116(7) 0.039(4) 0.039(6) 0.044(5) C35 0.076(6) 0.045(4) 0.143(8) 0.007(4) 0.019(6) 0.019(4) C36 0.050(4) 0.057(4) 0.081(5) 0.012(3) 0.012(4) 0.022(3) C37 0.093(5) 0.039(3) 0.052(3) 0.017(3) 0.015(4) 0.031(3) C38 0.074(11) 0.042(8) 0.040(7) 0.013(5) 0.003(7) 0.002(7) C38' 0.125(17) 0.036(7) 0.038(7) 0.021(5) 0.007(9) 0.016(9) C39 0.142(8) 0.072(5) 0.074(5) 0.041(4) 0.035(5) 0.072(5) C40 0.079(5) 0.050(3) 0.060(4) 0.023(3) 0.024(4) 0.039(3) C41 0.039(3) 0.048(3) 0.064(4) 0.018(3) -0.002(3) 0.024(3) C42 0.045(3) 0.054(3) 0.056(4) 0.011(3) 0.008(3) 0.020(3) C43 0.055(4) 0.084(4) 0.059(4) 0.033(3) 0.014(3) 0.045(4) C44 0.053(4) 0.057(4) 0.091(5) 0.026(3) 0.020(4) 0.032(3) C45 0.052(4) 0.096(5) 0.054(4) 0.024(4) 0.013(3) -0.003(4) C46 0.061(4) 0.044(3) 0.069(4) 0.020(3) 0.024(3) 0.014(3) C47 0.074(5) 0.087(5) 0.075(5) 0.049(4) 0.013(4) 0.026(4) C48 0.057(4) 0.073(4) 0.044(3) 0.019(3) 0.010(3) 0.012(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Gd1 C8 2.618(5) . ? Gd1 C3 2.619(5) . ? Gd1 C5 2.623(6) . ? Gd1 C4 2.622(6) . ? Gd1 C7 2.627(6) . ? Gd1 C1 2.629(5) . ? Gd1 C2 2.633(5) . ? Gd1 C12 2.645(13) . ? Gd1 C6 2.648(6) . ? Gd1 C9' 2.696(18) . ? Gd1 C16' 2.702(17) . ? Gd1 C13 2.675(16) . ? Gd2 C26 2.631(5) . ? Gd2 C25 2.639(5) . ? Gd2 C21 2.650(5) . ? Gd2 C22 2.651(5) . ? Gd2 C31 2.651(5) . ? Gd2 C27 2.652(5) . ? Gd2 C29 2.660(5) . ? Gd2 C30 2.658(5) . ? Gd2 C23 2.658(5) . ? Gd2 C32 2.662(5) . ? Gd2 C20 2.664(5) . ? Gd2 C28 2.665(5) . ? K1 C10' 3.037(17) . ? K1 C11' 3.050(16) . ? K1 C10 3.054(15) . ? K1 C11 3.059(15) . ? K1 C9' 3.053(19) . ? K1 C13 3.108(19) . ? K1 C12' 3.097(16) . ? K1 C9 3.110(18) . ? K1 C14 3.11(2) . ? K1 C12 3.115(14) . ? K1 C16 3.122(19) . ? K1 C16' 3.101(18) . ? K2 O3 2.697(4) . ? K2 O4 2.702(4) . ? K2 O2 2.702(4) . ? K2 O1 2.702(4) . ? K2 C28 3.139(5) . ? K2 C27 3.137(5) . ? K2 C29 3.175(6) . ? K2 C26 3.184(5) . ? K2 C25 3.231(5) . ? K2 C30 3.242(6) . ? K2 C31 3.272(6) . ? K2 C32 3.272(5) . ? O1 C36 1.416(8) . ? O1 C33 1.417(8) . ? O2 C40 1.413(6) . ? O2 C37 1.421(7) . ? O3 C44 1.420(7) . ? O3 C41 1.423(7) . ? O4 C45 1.392(7) . ? O4 C48 1.404(7) . ? C1 C2 1.379(9) . ? C1 C8 1.383(10) . ? C2 C3 1.380(10) . ? C3 C4 1.410(11) . ? C4 C5 1.376(11) . ? C5 C6 1.404(12) . ? C6 C7 1.404(12) . ? C7 C8 1.417(11) . ? C9 C16 1.403(17) . ? C9 C10 1.413(17) . ? C10 C11 1.385(18) . ? C11 C12 1.415(18) . ? C12 C13 1.411(17) . ? C13 C14 1.383(17) . ? C14 C15 1.408(17) . ? C15 C16 1.413(17) . ? C9' C10' 1.413(18) . ? C9' C16' 1.416(17) . ? C10' C11' 1.388(17) . ? C11' C12' 1.418(18) . ? C12' C13' 1.393(16) . ? C13' C14' 1.383(16) . ? C14' C15' 1.407(16) . ? C15' C16' 1.412(16) . ? C17 C18 1.397(10) . ? C17 C24 1.402(9) . ? C18 C19 1.403(9) . ? C19 C20 1.403(9) . ? C20 C21 1.403(9) . ? C21 C22 1.400(9) . ? C22 C23 1.395(9) . ? C23 C24 1.384(9) . ? C25 C26 1.376(9) . ? C25 C32 1.407(9) . ? C26 C27 1.399(9) . ? C27 C28 1.400(9) . ? C28 C29 1.397(9) . ? C29 C30 1.405(9) . ? C30 C31 1.385(9) . ? C31 C32 1.404(10) . ? C33 C34 1.463(11) . ? C34 C35 1.496(12) . ? C35 C36 1.473(10) . ? C37 C38' 1.472(11) . ? C37 C38 1.502(13) . ? C38 C39 1.475(11) . ? C38' C39 1.501(12) . ? C39 C40 1.469(9) . ? C41 C42 1.477(8) . ? C42 C43 1.499(9) . ? C43 C44 1.489(9) . ? C45 C46 1.471(9) . ? C46 C47 1.502(10) . ? C47 C48 1.492(10) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C8 Gd1 C3 79.4(2) . . ? C8 Gd1 C5 80.4(2) . . ? C3 Gd1 C5 58.8(2) . . ? C8 Gd1 C4 88.1(2) . . ? C3 Gd1 C4 31.2(2) . . ? C5 Gd1 C4 30.4(2) . . ? C8 Gd1 C7 31.4(2) . . ? C3 Gd1 C7 87.8(2) . . ? C5 Gd1 C7 59.1(3) . . ? C4 Gd1 C7 79.7(2) . . ? C8 Gd1 C1 30.6(2) . . ? C3 Gd1 C1 58.2(2) . . ? C5 Gd1 C1 87.82(19) . . ? C4 Gd1 C1 79.6(2) . . ? C7 Gd1 C1 58.9(2) . . ? C8 Gd1 C2 58.3(2) . . ? C3 Gd1 C2 30.5(2) . . ? C5 Gd1 C2 79.5(2) . . ? C4 Gd1 C2 58.8(2) . . ? C7 Gd1 C2 79.5(2) . . ? C1 Gd1 C2 30.4(2) . . ? C8 Gd1 C12 152.5(5) . . ? C3 Gd1 C12 91.7(3) . . ? C5 Gd1 C12 117.2(5) . . ? C4 Gd1 C12 97.7(4) . . ? C7 Gd1 C12 175.7(5) . . ? C1 Gd1 C12 124.2(5) . . ? C2 Gd1 C12 102.1(4) . . ? C8 Gd1 C6 59.3(3) . . ? C3 Gd1 C6 79.6(2) . . ? C5 Gd1 C6 30.9(3) . . ? C4 Gd1 C6 58.4(3) . . ? C7 Gd1 C6 30.9(3) . . ? C1 Gd1 C6 79.6(2) . . ? C2 Gd1 C6 87.38(19) . . ? C12 Gd1 C6 144.9(5) . . ? C8 Gd1 C9' 97.6(4) . . ? C3 Gd1 C9' 133.9(5) . . ? C5 Gd1 C9' 166.8(5) . . ? C4 Gd1 C9' 162.6(5) . . ? C7 Gd1 C9' 113.3(4) . . ? C1 Gd1 C9' 97.0(4) . . ? C2 Gd1 C9' 110.7(5) . . ? C6 Gd1 C9' 138.1(5) . . ? C8 Gd1 C16' 97.0(4) . . ? C3 Gd1 C16' 163.8(5) . . ? C5 Gd1 C16' 136.6(5) . . ? C4 Gd1 C16' 164.9(5) . . ? C7 Gd1 C16' 97.3(4) . . ? C1 Gd1 C16' 111.7(4) . . ? C2 Gd1 C16' 135.5(5) . . ? C6 Gd1 C16' 112.4(5) . . ? C9' Gd1 C16' 30.4(4) . . ? C8 Gd1 C13 176.6(5) . . ? C3 Gd1 C13 102.3(4) . . ? C5 Gd1 C13 98.0(5) . . ? C4 Gd1 C13 92.0(4) . . ? C7 Gd1 C13 145.4(5) . . ? C1 Gd1 C13 152.7(5) . . ? C2 Gd1 C13 124.5(4) . . ? C12 Gd1 C13 30.7(4) . . ? C6 Gd1 C13 118.0(5) . . ? C26 Gd2 C25 30.3(2) . . ? C26 Gd2 C21 153.0(2) . . ? C25 Gd2 C21 176.7(2) . . ? C26 Gd2 C22 176.4(2) . . ? C25 Gd2 C22 146.1(2) . . ? C21 Gd2 C22 30.6(2) . . ? C26 Gd2 C31 78.99(18) . . ? C25 Gd2 C31 58.5(2) . . ? C21 Gd2 C31 119.4(2) . . ? C22 Gd2 C31 98.38(18) . . ? C26 Gd2 C27 30.7(2) . . ? C25 Gd2 C27 58.1(2) . . ? C21 Gd2 C27 124.9(2) . . ? C22 Gd2 C27 152.2(2) . . ? C31 Gd2 C27 86.85(16) . . ? C26 Gd2 C29 78.91(18) . . ? C25 Gd2 C29 86.76(16) . . ? C21 Gd2 C29 93.98(16) . . ? C22 Gd2 C29 101.88(18) . . ? C31 Gd2 C29 57.9(2) . . ? C27 Gd2 C29 58.1(2) . . ? C26 Gd2 C30 87.11(16) . . ? C25 Gd2 C30 79.02(17) . . ? C21 Gd2 C30 100.01(17) . . ? C22 Gd2 C30 91.83(16) . . ? C31 Gd2 C30 30.2(2) . . ? C27 Gd2 C30 79.02(17) . . ? C29 Gd2 C30 30.6(2) . . ? C26 Gd2 C23 146.5(2) . . ? C25 Gd2 C23 118.7(2) . . ? C21 Gd2 C23 58.2(2) . . ? C22 Gd2 C23 30.47(19) . . ? C31 Gd2 C23 90.86(17) . . ? C27 Gd2 C23 176.79(19) . . ? C29 Gd2 C23 122.3(2) . . ? C30 Gd2 C23 100.07(18) . . ? C26 Gd2 C32 58.3(2) . . ? C25 Gd2 C32 30.8(2) . . ? C21 Gd2 C32 146.3(2) . . ? C22 Gd2 C32 118.3(2) . . ? C31 Gd2 C32 30.6(2) . . ? C27 Gd2 C32 79.02(18) . . ? C29 Gd2 C32 78.81(18) . . ? C30 Gd2 C32 58.2(2) . . ? C23 Gd2 C32 97.87(19) . . ? C26 Gd2 C20 125.1(2) . . ? C25 Gd2 C20 152.2(2) . . ? C21 Gd2 C20 30.61(19) . . ? C22 Gd2 C20 58.31(19) . . ? C31 Gd2 C20 147.6(2) . . ? C27 Gd2 C20 104.28(18) . . ? C29 Gd2 C20 102.10(17) . . ? C30 Gd2 C20 121.3(2) . . ? C23 Gd2 C20 78.84(18) . . ? C32 Gd2 C20 176.58(19) . . ? C26 Gd2 C28 58.4(2) . . ? C25 Gd2 C28 78.85(18) . . ? C21 Gd2 C28 103.37(18) . . ? C22 Gd2 C28 123.75(19) . . ? C31 Gd2 C28 78.74(17) . . ? C27 Gd2 C28 30.5(2) . . ? C29 Gd2 C28 30.4(2) . . ? C30 Gd2 C28 58.31(19) . . ? C23 Gd2 C28 150.8(2) . . ? C32 Gd2 C28 86.99(16) . . ? C20 Gd2 C28 95.44(16) . . ? C10' K1 C11' 26.4(3) . . ? C10 K1 C11 26.2(3) . . ? C10' K1 C9' 26.8(4) . . ? C11' K1 C9' 50.2(4) . . ? C10 K1 C13 66.7(4) . . ? C11 K1 C13 50.1(4) . . ? C10' K1 C12' 49.9(4) . . ? C11' K1 C12' 26.7(3) . . ? C9' K1 C12' 66.7(4) . . ? C10 K1 C9 26.5(3) . . ? C11 K1 C9 49.4(4) . . ? C13 K1 C9 71.8(4) . . ? C10 K1 C14 73.2(4) . . ? C11 K1 C14 66.8(4) . . ? C13 K1 C14 25.7(3) . . ? C9 K1 C14 65.9(4) . . ? C10 K1 C12 49.5(4) . . ? C11 K1 C12 26.5(3) . . ? C13 K1 C12 26.2(3) . . ? C9 K1 C12 65.5(4) . . ? C14 K1 C12 49.1(4) . . ? C10 K1 C16 50.1(4) . . ? C11 K1 C16 66.7(4) . . ? C13 K1 C16 65.8(4) . . ? C9 K1 C16 26.0(3) . . ? C14 K1 C16 49.5(4) . . ? C12 K1 C16 72.0(4) . . ? C10' K1 C16' 50.5(4) . . ? C11' K1 C16' 67.1(4) . . ? C9' K1 C16' 26.6(3) . . ? C12' K1 C16' 72.6(4) . . ? O3 K2 O4 82.50(13) . . ? O3 K2 O2 77.11(14) . . ? O4 K2 O2 135.06(14) . . ? O3 K2 O1 130.70(13) . . ? O4 K2 O1 75.22(13) . . ? O2 K2 O1 88.52(14) . . ? O3 K2 C28 123.26(15) . . ? O4 K2 C28 141.88(15) . . ? O2 K2 C28 81.55(15) . . ? O1 K2 C28 100.14(15) . . ? O3 K2 C27 98.18(16) . . ? O4 K2 C27 143.50(14) . . ? O2 K2 C27 79.48(13) . . ? O1 K2 C27 125.47(17) . . ? C28 K2 C27 25.77(17) . . ? O3 K2 C29 145.49(13) . . ? O4 K2 C29 118.68(17) . . ? O2 K2 C29 99.92(17) . . ? O1 K2 C29 83.01(14) . . ? C28 K2 C29 25.55(17) . . ? C27 K2 C29 48.20(17) . . ? O3 K2 C26 82.01(13) . . ? O4 K2 C26 121.38(16) . . ? O2 K2 C26 95.00(14) . . ? O1 K2 C26 146.80(15) . . ? C28 K2 C26 48.23(16) . . ? C27 K2 C26 25.56(17) . . ? C29 K2 C26 63.85(14) . . ? O3 K2 C25 82.01(13) . . ? O4 K2 C25 97.07(16) . . ? O2 K2 C25 118.76(16) . . ? O1 K2 C25 143.33(16) . . ? C28 K2 C25 63.82(14) . . ? C27 K2 C25 47.56(16) . . ? C29 K2 C25 69.23(13) . . ? C26 K2 C25 24.77(17) . . ? O3 K2 C30 144.03(14) . . ? O4 K2 C30 94.34(15) . . ? O2 K2 C30 124.96(17) . . ? O1 K2 C30 81.86(14) . . ? C28 K2 C30 47.92(16) . . ? C27 K2 C30 63.93(15) . . ? C29 K2 C30 25.26(17) . . ? C26 K2 C30 69.10(13) . . ? C25 K2 C30 62.74(14) . . ? O3 K2 C31 121.80(16) . . ? O4 K2 C31 79.34(14) . . ? O2 K2 C31 144.98(15) . . ? O1 K2 C31 96.69(16) . . ? C28 K2 C31 63.43(14) . . ? C27 K2 C31 69.31(13) . . ? C29 K2 C31 47.01(17) . . ? C26 K2 C31 62.71(14) . . ? C25 K2 C31 46.81(16) . . ? C30 K2 C31 24.55(16) . . ? O3 K2 C32 97.74(16) . . ? O4 K2 C32 80.04(14) . . ? O2 K2 C32 141.81(14) . . ? O1 K2 C32 120.23(18) . . ? C28 K2 C32 69.73(13) . . ? C27 K2 C32 63.64(14) . . ? C29 K2 C32 63.19(15) . . ? C26 K2 C32 47.04(16) . . ? C25 K2 C32 24.98(17) . . ? C30 K2 C32 46.77(17) . . ? C31 K2 C32 24.78(17) . . ? C36 O1 C33 108.4(5) . . ? C36 O1 K2 132.6(4) . . ? C33 O1 K2 118.3(4) . . ? C40 O2 C37 108.9(4) . . ? C40 O2 K2 128.1(3) . . ? C37 O2 K2 117.5(3) . . ? C44 O3 C41 108.8(5) . . ? C44 O3 K2 127.3(4) . . ? C41 O3 K2 123.8(3) . . ? C45 O4 C48 108.8(5) . . ? C45 O4 K2 121.1(4) . . ? C48 O4 K2 119.5(4) . . ? C2 C1 C8 135.5(6) . . ? C2 C1 Gd1 75.0(3) . . ? C8 C1 Gd1 74.3(3) . . ? C1 C2 C3 135.3(6) . . ? C1 C2 Gd1 74.6(3) . . ? C3 C2 Gd1 74.2(3) . . ? C2 C3 C4 135.2(6) . . ? C2 C3 Gd1 75.4(3) . . ? C4 C3 Gd1 74.5(3) . . ? C5 C4 C3 134.9(6) . . ? C5 C4 Gd1 74.8(4) . . ? C3 C4 Gd1 74.3(4) . . ? C4 C5 C6 135.4(7) . . ? C4 C5 Gd1 74.8(4) . . ? C6 C5 Gd1 75.6(4) . . ? C5 C6 C7 134.3(7) . . ? C5 C6 Gd1 73.5(4) . . ? C7 C6 Gd1 73.7(4) . . ? C8 C7 C6 134.7(6) . . ? C8 C7 Gd1 74.0(3) . . ? C6 C7 Gd1 75.4(4) . . ? C1 C8 C7 134.7(7) . . ? C1 C8 Gd1 75.2(3) . . ? C7 C8 Gd1 74.7(3) . . ? C16 C9 C10 136.3(11) . . ? C16 C9 Gd1 76.6(11) . . ? C10 C9 Gd1 76.7(10) . . ? C16 C9 K1 77.5(11) . . ? C10 C9 K1 74.6(10) . . ? Gd1 C9 K1 101.1(4) . . ? C11 C10 C9 134.3(11) . . ? C11 C10 Gd1 74.3(9) . . ? C9 C10 Gd1 73.2(10) . . ? C11 C10 K1 77.1(9) . . ? C9 C10 K1 79.0(10) . . ? Gd1 C10 K1 101.5(3) . . ? C10 C11 C12 134.7(11) . . ? C10 C11 Gd1 76.3(9) . . ? C12 C11 Gd1 72.2(8) . . ? C10 C11 K1 76.7(9) . . ? C12 C11 K1 78.9(8) . . ? Gd1 C11 K1 101.9(4) . . ? C11 C12 C13 135.0(11) . . ? C11 C12 Gd1 77.2(8) . . ? C13 C12 Gd1 75.8(9) . . ? C11 C12 K1 74.6(8) . . ? C13 C12 K1 76.6(9) . . ? Gd1 C12 K1 102.0(3) . . ? C14 C13 C12 135.6(11) . . ? C14 C13 Gd1 76.8(10) . . ? C12 C13 Gd1 73.4(8) . . ? C14 C13 K1 77.4(11) . . ? C12 C13 K1 77.2(10) . . ? Gd1 C13 K1 101.5(4) . . ? C13 C14 C15 134.6(11) . . ? C13 C14 Gd1 73.5(10) . . ? C15 C14 Gd1 75.2(9) . . ? C13 C14 K1 76.9(11) . . ? C15 C14 K1 77.3(11) . . ? Gd1 C14 K1 100.4(4) . . ? C16 C15 C14 135.4(11) . . ? C16 C15 Gd1 75.3(9) . . ? C14 C15 Gd1 74.8(9) . . ? C16 C15 K1 76.9(10) . . ? C14 C15 K1 76.7(11) . . ? Gd1 C15 K1 100.1(4) . . ? C15 C16 C9 133.7(11) . . ? C15 C16 Gd1 74.7(9) . . ? C9 C16 Gd1 73.4(10) . . ? C15 C16 K1 76.9(10) . . ? C9 C16 K1 76.5(11) . . ? Gd1 C16 K1 99.9(4) . . ? C10' C9' C16' 135.2(10) . . ? C10' C9' Gd1 75.3(10) . . ? C16' C9' Gd1 75.0(9) . . ? C10' C9' K1 76.0(10) . . ? C16' C9' K1 78.6(10) . . ? Gd1 C9' K1 102.4(3) . . ? C11' C10' C9' 135.0(11) . . ? C11' C10' Gd1 75.8(9) . . ? C9' C10' Gd1 74.4(10) . . ? C11' C10' K1 77.3(10) . . ? C9' C10' K1 77.2(10) . . ? Gd1 C10' K1 102.5(4) . . ? C10' C11' C12' 134.6(11) . . ? C10' C11' Gd1 74.6(9) . . ? C12' C11' Gd1 74.4(9) . . ? C10' C11' K1 76.3(10) . . ? C12' C11' K1 78.5(9) . . ? Gd1 C11' K1 101.9(4) . . ? C13' C12' C11' 135.7(11) . . ? C13' C12' Gd1 75.7(9) . . ? C11' C12' Gd1 75.3(8) . . ? C13' C12' K1 78.6(9) . . ? C11' C12' K1 74.8(9) . . ? Gd1 C12' K1 100.9(3) . . ? C14' C13' C12' 135.0(11) . . ? C14' C13' Gd1 74.5(10) . . ? C12' C13' Gd1 74.6(8) . . ? C14' C13' K1 78.3(10) . . ? C12' C13' K1 75.6(10) . . ? Gd1 C13' K1 99.7(3) . . ? C13' C14' C15' 135.2(11) . . ? C13' C14' Gd1 76.0(10) . . ? C15' C14' Gd1 74.5(9) . . ? C13' C14' K1 76.3(10) . . ? C15' C14' K1 76.1(10) . . ? Gd1 C14' K1 99.5(3) . . ? C16' C15' C14' 135.5(10) . . ? C16' C15' Gd1 75.0(9) . . ? C14' C15' Gd1 75.3(9) . . ? C16' C15' K1 75.6(10) . . ? C14' C15' K1 78.0(10) . . ? Gd1 C15' K1 100.3(3) . . ? C15' C16' C9' 133.8(10) . . ? C15' C16' Gd1 74.6(9) . . ? C9' C16' Gd1 74.5(9) . . ? C15' C16' K1 78.3(9) . . ? C9' C16' K1 74.8(10) . . ? Gd1 C16' K1 101.0(3) . . ? C18 C17 C24 134.9(5) . . ? C18 C17 Gd2 75.0(3) . . ? C24 C17 Gd2 75.0(3) . . ? C18 C17 K1 76.7(3) . . ? C24 C17 K1 76.6(3) . . ? Gd2 C17 K1 100.75(17) . . ? C17 C18 C19 135.4(5) . . ? C17 C18 Gd2 74.6(3) . . ? C19 C18 Gd2 75.2(3) . . ? C17 C18 K1 77.5(3) . . ? C19 C18 K1 76.8(3) . . ? Gd2 C18 K1 100.86(15) . . ? C20 C19 C18 134.7(5) . . ? C20 C19 Gd2 74.2(3) . . ? C18 C19 Gd2 74.4(3) . . ? C20 C19 K1 77.6(3) . . ? C18 C19 K1 77.2(3) . . ? Gd2 C19 K1 100.74(16) . . ? C19 C20 C21 134.6(5) . . ? C19 C20 Gd2 75.4(3) . . ? C21 C20 Gd2 74.1(3) . . ? C19 C20 K1 76.6(3) . . ? C21 C20 K1 77.0(3) . . ? Gd2 C20 K1 100.77(16) . . ? C22 C21 C20 135.0(5) . . ? C22 C21 Gd2 74.7(3) . . ? C20 C21 Gd2 75.2(3) . . ? C22 C21 K1 76.7(3) . . ? C20 C21 K1 77.1(3) . . ? Gd2 C21 K1 101.12(15) . . ? C23 C22 C21 135.0(5) . . ? C23 C22 Gd2 75.0(3) . . ? C21 C22 Gd2 74.6(3) . . ? C23 C22 K1 76.9(3) . . ? C21 C22 K1 77.4(3) . . ? Gd2 C22 K1 101.32(16) . . ? C24 C23 C22 135.6(5) . . ? C24 C23 Gd2 75.4(3) . . ? C22 C23 Gd2 74.5(3) . . ? C24 C23 K1 77.4(3) . . ? C22 C23 K1 77.3(3) . . ? Gd2 C23 K1 101.30(17) . . ? C23 C24 C17 134.8(5) . . ? C23 C24 Gd2 74.5(3) . . ? C17 C24 Gd2 74.5(3) . . ? C23 C24 K1 77.0(3) . . ? C17 C24 K1 77.5(3) . . ? Gd2 C24 K1 100.90(16) . . ? C26 C25 C32 135.6(5) . . ? C26 C25 Gd2 74.6(3) . . ? C32 C25 Gd2 75.5(3) . . ? C26 C25 K2 75.7(3) . . ? C32 C25 K2 79.1(3) . . ? Gd2 C25 K2 101.49(15) . . ? C25 C26 C27 135.6(5) . . ? C25 C26 Gd2 75.2(3) . . ? C27 C26 Gd2 75.5(3) . . ? C25 C26 K2 79.6(3) . . ? C27 C26 K2 75.4(3) . . ? Gd2 C26 K2 102.92(15) . . ? C28 C27 C26 134.8(5) . . ? C28 C27 Gd2 75.2(3) . . ? C26 C27 Gd2 73.8(3) . . ? C28 C27 K2 77.2(3) . . ? C26 C27 K2 79.1(3) . . ? Gd2 C27 K2 103.64(17) . . ? C29 C28 C27 134.4(5) . . ? C29 C28 Gd2 74.6(3) . . ? C27 C28 Gd2 74.3(3) . . ? C29 C28 K2 78.7(3) . . ? C27 C28 K2 77.0(3) . . ? Gd2 C28 K2 103.30(16) . . ? C28 C29 C30 135.5(5) . . ? C28 C29 Gd2 75.0(3) . . ? C30 C29 Gd2 74.6(3) . . ? C28 C29 K2 75.8(3) . . ? C30 C29 K2 80.0(3) . . ? Gd2 C29 K2 102.46(17) . . ? C31 C30 C29 134.5(5) . . ? C31 C30 Gd2 74.6(3) . . ? C29 C30 Gd2 74.8(3) . . ? C31 C30 K2 78.9(4) . . ? C29 C30 K2 74.7(3) . . ? Gd2 C30 K2 100.79(16) . . ? C30 C31 C32 135.9(5) . . ? C30 C31 Gd2 75.1(3) . . ? C32 C31 Gd2 75.1(3) . . ? C30 C31 K2 76.5(3) . . ? C32 C31 K2 77.6(3) . . ? Gd2 C31 K2 100.20(16) . . ? C31 C32 C25 133.6(5) . . ? C31 C32 Gd2 74.3(3) . . ? C25 C32 Gd2 73.7(3) . . ? C31 C32 K2 77.6(3) . . ? C25 C32 K2 75.9(3) . . ? Gd2 C32 K2 99.96(17) . . ? O1 C33 C34 107.9(7) . . ? C33 C34 C35 105.7(6) . . ? C36 C35 C34 104.0(7) . . ? O1 C36 C35 105.8(6) . . ? O2 C37 C38' 110.8(6) . . ? O2 C37 C38 102.7(7) . . ? C39 C38 C37 102.3(8) . . ? C37 C38' C39 102.5(8) . . ? C40 C39 C38 101.7(7) . . ? C40 C39 C38' 108.5(6) . . ? O2 C40 C39 107.6(5) . . ? O3 C41 C42 106.8(4) . . ? C41 C42 C43 102.3(5) . . ? C44 C43 C42 102.7(5) . . ? O3 C44 C43 106.8(5) . . ? O4 C45 C46 110.1(5) . . ? C45 C46 C47 103.0(6) . . ? C48 C47 C46 103.6(6) . . ? O4 C48 C47 107.6(5) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C8 C1 C2 C3 0.6(13) . . . . ? Gd1 C1 C2 C3 -47.2(7) . . . . ? C8 C1 C2 Gd1 47.7(7) . . . . ? C1 C2 C3 C4 -1.8(13) . . . . ? Gd1 C2 C3 C4 -49.1(7) . . . . ? C1 C2 C3 Gd1 47.3(7) . . . . ? C2 C3 C4 C5 1.0(13) . . . . ? Gd1 C3 C4 C5 -48.4(7) . . . . ? C2 C3 C4 Gd1 49.4(7) . . . . ? C3 C4 C5 C6 -1.7(14) . . . . ? Gd1 C4 C5 C6 -49.9(8) . . . . ? C3 C4 C5 Gd1 48.2(7) . . . . ? C4 C5 C6 C7 3.7(14) . . . . ? Gd1 C5 C6 C7 -45.9(7) . . . . ? C4 C5 C6 Gd1 49.6(8) . . . . ? C5 C6 C7 C8 -2.9(13) . . . . ? Gd1 C6 C7 C8 -48.7(7) . . . . ? C5 C6 C7 Gd1 45.9(8) . . . . ? C2 C1 C8 C7 1.7(12) . . . . ? Gd1 C1 C8 C7 49.7(7) . . . . ? C2 C1 C8 Gd1 -47.9(7) . . . . ? C6 C7 C8 C1 -0.6(12) . . . . ? Gd1 C7 C8 C1 -49.8(7) . . . . ? C6 C7 C8 Gd1 49.2(7) . . . . ? C16 C9 C10 C11 -7(4) . . . . ? Gd1 C9 C10 C11 46(2) . . . . ? K1 C9 C10 C11 -59(2) . . . . ? C16 C9 C10 Gd1 -54(3) . . . . ? K1 C9 C10 Gd1 -105.7(3) . . . . ? C16 C9 C10 K1 52(3) . . . . ? Gd1 C9 C10 K1 105.7(3) . . . . ? C9 C10 C11 C12 1(4) . . . . ? Gd1 C10 C11 C12 46.8(19) . . . . ? K1 C10 C11 C12 -59(2) . . . . ? C9 C10 C11 Gd1 -46(2) . . . . ? K1 C10 C11 Gd1 -106.0(3) . . . . ? C9 C10 C11 K1 60(2) . . . . ? Gd1 C10 C11 K1 106.0(3) . . . . ? C10 C11 C12 C13 6(3) . . . . ? Gd1 C11 C12 C13 54(2) . . . . ? K1 C11 C12 C13 -52(2) . . . . ? C10 C11 C12 Gd1 -48(2) . . . . ? K1 C11 C12 Gd1 -106.5(3) . . . . ? C10 C11 C12 K1 58(2) . . . . ? Gd1 C11 C12 K1 106.5(3) . . . . ? C11 C12 C13 C14 -5(4) . . . . ? Gd1 C12 C13 C14 50(2) . . . . ? K1 C12 C13 C14 -57(2) . . . . ? C11 C12 C13 Gd1 -54.9(19) . . . . ? K1 C12 C13 Gd1 -106.3(3) . . . . ? C11 C12 C13 K1 51.4(19) . . . . ? Gd1 C12 C13 K1 106.3(3) . . . . ? C12 C13 C14 C15 0(4) . . . . ? Gd1 C13 C14 C15 48(2) . . . . ? K1 C13 C14 C15 -57(2) . . . . ? C12 C13 C14 Gd1 -49(2) . . . . ? K1 C13 C14 Gd1 -105.2(3) . . . . ? C12 C13 C14 K1 56(2) . . . . ? Gd1 C13 C14 K1 105.2(3) . . . . ? C13 C14 C15 C16 2(4) . . . . ? Gd1 C14 C15 C16 49(2) . . . . ? K1 C14 C15 C16 -55(2) . . . . ? C13 C14 C15 Gd1 -48(2) . . . . ? K1 C14 C15 Gd1 -104.5(3) . . . . ? C13 C14 C15 K1 57(2) . . . . ? Gd1 C14 C15 K1 104.5(3) . . . . ? C14 C15 C16 C9 -1(4) . . . . ? Gd1 C15 C16 C9 48(2) . . . . ? K1 C15 C16 C9 -56(2) . . . . ? C14 C15 C16 Gd1 -49(2) . . . . ? K1 C15 C16 Gd1 -104.3(3) . . . . ? C14 C15 C16 K1 55(2) . . . . ? Gd1 C15 C16 K1 104.3(3) . . . . ? C10 C9 C16 C15 5(4) . . . . ? Gd1 C9 C16 C15 -48(2) . . . . ? K1 C9 C16 C15 57(2) . . . . ? C10 C9 C16 Gd1 54(3) . . . . ? K1 C9 C16 Gd1 104.8(3) . . . . ? C10 C9 C16 K1 -51(3) . . . . ? Gd1 C9 C16 K1 -104.8(3) . . . . ? C16' C9' C10' C11' 0(4) . . . . ? Gd1 C9' C10' C11' 50(2) . . . . ? K1 C9' C10' C11' -57(2) . . . . ? C16' C9' C10' Gd1 -50(2) . . . . ? K1 C9' C10' Gd1 -107.1(3) . . . . ? C16' C9' C10' K1 57(2) . . . . ? Gd1 C9' C10' K1 107.1(3) . . . . ? C9' C10' C11' C12' -1(4) . . . . ? Gd1 C10' C11' C12' 49(2) . . . . ? K1 C10' C11' C12' -58(2) . . . . ? C9' C10' C11' Gd1 -50(2) . . . . ? K1 C10' C11' Gd1 -106.6(3) . . . . ? C9' C10' C11' K1 57(2) . . . . ? Gd1 C10' C11' K1 106.6(3) . . . . ? C10' C11' C12' C13' 2(4) . . . . ? Gd1 C11' C12' C13' 51(2) . . . . ? K1 C11' C12' C13' -55(2) . . . . ? C10' C11' C12' Gd1 -49(2) . . . . ? K1 C11' C12' Gd1 -105.9(3) . . . . ? C10' C11' C12' K1 57(2) . . . . ? Gd1 C11' C12' K1 105.9(3) . . . . ? C11' C12' C13' C14' -3(4) . . . . ? Gd1 C12' C13' C14' 48(2) . . . . ? K1 C12' C13' C14' -56(2) . . . . ? C11' C12' C13' Gd1 -51(2) . . . . ? K1 C12' C13' Gd1 -104.5(3) . . . . ? C11' C12' C13' K1 54(2) . . . . ? Gd1 C12' C13' K1 104.5(3) . . . . ? C12' C13' C14' C15' 2(4) . . . . ? Gd1 C13' C14' C15' 50(2) . . . . ? K1 C13' C14' C15' -53(2) . . . . ? C12' C13' C14' Gd1 -48(2) . . . . ? K1 C13' C14' Gd1 -103.6(3) . . . . ? C12' C13' C14' K1 56(2) . . . . ? Gd1 C13' C14' K1 103.6(3) . . . . ? C13' C14' C15' C16' -1(4) . . . . ? Gd1 C14' C15' C16' 50(2) . . . . ? K1 C14' C15' C16' -55(2) . . . . ? C13' C14' C15' Gd1 -51(2) . . . . ? K1 C14' C15' Gd1 -104.2(3) . . . . ? C13' C14' C15' K1 54(2) . . . . ? Gd1 C14' C15' K1 104.2(3) . . . . ? C14' C15' C16' C9' 0(4) . . . . ? Gd1 C15' C16' C9' 50(2) . . . . ? K1 C15' C16' C9' -55(2) . . . . ? C14' C15' C16' Gd1 -50(2) . . . . ? K1 C15' C16' Gd1 -105.1(3) . . . . ? C14' C15' C16' K1 55(2) . . . . ? Gd1 C15' C16' K1 105.1(3) . . . . ? C10' C9' C16' C15' 0(4) . . . . ? Gd1 C9' C16' C15' -50(2) . . . . ? K1 C9' C16' C15' 57(2) . . . . ? C10' C9' C16' Gd1 50(2) . . . . ? K1 C9' C16' Gd1 106.3(3) . . . . ? C10' C9' C16' K1 -56(2) . . . . ? Gd1 C9' C16' K1 -106.3(3) . . . . ? C24 C17 C18 C19 1.0(11) . . . . ? Gd2 C17 C18 C19 -48.9(6) . . . . ? K1 C17 C18 C19 56.2(6) . . . . ? C24 C17 C18 Gd2 49.9(6) . . . . ? K1 C17 C18 Gd2 105.15(13) . . . . ? C24 C17 C18 K1 -55.2(6) . . . . ? Gd2 C17 C18 K1 -105.15(13) . . . . ? C17 C18 C19 C20 1.2(11) . . . . ? Gd2 C18 C19 C20 -47.6(6) . . . . ? K1 C18 C19 C20 57.6(6) . . . . ? C17 C18 C19 Gd2 48.8(6) . . . . ? K1 C18 C19 Gd2 105.18(12) . . . . ? C17 C18 C19 K1 -56.4(6) . . . . ? Gd2 C18 C19 K1 -105.18(12) . . . . ? C18 C19 C20 C21 -1.5(11) . . . . ? Gd2 C19 C20 C21 -49.2(6) . . . . ? K1 C19 C20 C21 56.0(6) . . . . ? C18 C19 C20 Gd2 47.6(6) . . . . ? K1 C19 C20 Gd2 105.13(13) . . . . ? C18 C19 C20 K1 -57.5(6) . . . . ? Gd2 C19 C20 K1 -105.13(13) . . . . ? C19 C20 C21 C22 0.0(11) . . . . ? Gd2 C20 C21 C22 -49.5(6) . . . . ? K1 C20 C21 C22 55.8(6) . . . . ? C19 C20 C21 Gd2 49.6(6) . . . . ? K1 C20 C21 Gd2 105.35(13) . . . . ? C19 C20 C21 K1 -55.8(6) . . . . ? Gd2 C20 C21 K1 -105.35(13) . . . . ? C20 C21 C22 C23 0.5(11) . . . . ? Gd2 C21 C22 C23 -49.2(6) . . . . ? K1 C21 C22 C23 56.4(6) . . . . ? C20 C21 C22 Gd2 49.7(6) . . . . ? K1 C21 C22 Gd2 105.65(12) . . . . ? C20 C21 C22 K1 -56.0(6) . . . . ? Gd2 C21 C22 K1 -105.65(12) . . . . ? C21 C22 C23 C24 0.1(12) . . . . ? Gd2 C22 C23 C24 -48.9(7) . . . . ? K1 C22 C23 C24 56.8(7) . . . . ? C21 C22 C23 Gd2 49.1(6) . . . . ? K1 C22 C23 Gd2 105.71(12) . . . . ? C21 C22 C23 K1 -56.6(6) . . . . ? Gd2 C22 C23 K1 -105.71(12) . . . . ? C22 C23 C24 C17 0.5(12) . . . . ? Gd2 C23 C24 C17 -48.2(6) . . . . ? K1 C23 C24 C17 57.2(6) . . . . ? C22 C23 C24 Gd2 48.7(7) . . . . ? K1 C23 C24 Gd2 105.40(13) . . . . ? C22 C23 C24 K1 -56.7(7) . . . . ? Gd2 C23 C24 K1 -105.40(13) . . . . ? C18 C17 C24 C23 -1.7(11) . . . . ? Gd2 C17 C24 C23 48.2(6) . . . . ? K1 C17 C24 C23 -57.0(6) . . . . ? C18 C17 C24 Gd2 -49.9(6) . . . . ? K1 C17 C24 Gd2 -105.20(13) . . . . ? C18 C17 C24 K1 55.3(6) . . . . ? Gd2 C17 C24 K1 105.20(14) . . . . ? C32 C25 C26 C27 1.0(11) . . . . ? Gd2 C25 C26 C27 50.2(6) . . . . ? K2 C25 C26 C27 -56.3(6) . . . . ? C32 C25 C26 Gd2 -49.2(6) . . . . ? K2 C25 C26 Gd2 -106.49(12) . . . . ? C32 C25 C26 K2 57.3(6) . . . . ? Gd2 C25 C26 K2 106.49(12) . . . . ? C25 C26 C27 C28 -1.6(11) . . . . ? Gd2 C26 C27 C28 48.5(6) . . . . ? K2 C26 C27 C28 -59.3(6) . . . . ? C25 C26 C27 Gd2 -50.1(6) . . . . ? K2 C26 C27 Gd2 -107.83(12) . . . . ? C25 C26 C27 K2 57.7(6) . . . . ? Gd2 C26 C27 K2 107.83(12) . . . . ? C26 C27 C28 C29 0.5(11) . . . . ? Gd2 C27 C28 C29 48.6(6) . . . . ? K2 C27 C28 C29 -59.5(6) . . . . ? C26 C27 C28 Gd2 -48.1(6) . . . . ? K2 C27 C28 Gd2 -108.07(13) . . . . ? C26 C27 C28 K2 60.0(6) . . . . ? Gd2 C27 C28 K2 108.07(13) . . . . ? C27 C28 C29 C30 -0.3(11) . . . . ? Gd2 C28 C29 C30 48.2(6) . . . . ? K2 C28 C29 C30 -59.2(6) . . . . ? C27 C28 C29 Gd2 -48.5(6) . . . . ? K2 C28 C29 Gd2 -107.37(13) . . . . ? C27 C28 C29 K2 58.9(6) . . . . ? Gd2 C28 C29 K2 107.37(13) . . . . ? C28 C29 C30 C31 0.9(11) . . . . ? Gd2 C29 C30 C31 49.2(6) . . . . ? K2 C29 C30 C31 -56.8(6) . . . . ? C28 C29 C30 Gd2 -48.3(6) . . . . ? K2 C29 C30 Gd2 -106.00(13) . . . . ? C28 C29 C30 K2 57.7(6) . . . . ? Gd2 C29 C30 K2 106.00(13) . . . . ? C29 C30 C31 C32 -0.3(12) . . . . ? Gd2 C30 C31 C32 48.9(7) . . . . ? K2 C30 C31 C32 -55.6(7) . . . . ? C29 C30 C31 Gd2 -49.3(6) . . . . ? K2 C30 C31 Gd2 -104.58(12) . . . . ? C29 C30 C31 K2 55.3(6) . . . . ? Gd2 C30 C31 K2 104.58(12) . . . . ? C30 C31 C32 C25 -1.1(12) . . . . ? Gd2 C31 C32 C25 47.9(6) . . . . ? K2 C31 C32 C25 -56.4(6) . . . . ? C30 C31 C32 Gd2 -49.0(7) . . . . ? K2 C31 C32 Gd2 -104.24(13) . . . . ? C30 C31 C32 K2 55.3(7) . . . . ? Gd2 C31 C32 K2 104.24(13) . . . . ? C26 C25 C32 C31 0.8(11) . . . . ? Gd2 C25 C32 C31 -48.0(6) . . . . ? K2 C25 C32 C31 57.0(6) . . . . ? C26 C25 C32 Gd2 48.9(6) . . . . ? K2 C25 C32 Gd2 105.02(13) . . . . ? C26 C25 C32 K2 -56.1(6) . . . . ? Gd2 C25 C32 K2 -105.02(13) . . . . ? C36 O1 C33 C34 -14.7(9) . . . . ? K2 O1 C33 C34 157.1(5) . . . . ? O1 C33 C34 C35 -3.6(10) . . . . ? C33 C34 C35 C36 19.4(10) . . . . ? C33 O1 C36 C35 27.2(8) . . . . ? K2 O1 C36 C35 -142.8(5) . . . . ? C34 C35 C36 O1 -28.4(9) . . . . ? C40 O2 C37 C38' -9.5(12) . . . . ? K2 O2 C37 C38' -165.4(10) . . . . ? C40 O2 C37 C38 23.3(8) . . . . ? K2 O2 C37 C38 -132.6(7) . . . . ? O2 C37 C38 C39 -38.8(11) . . . . ? C38' C37 C38 C39 70.1(11) . . . . ? O2 C37 C38' C39 13.2(15) . . . . ? C38 C37 C38' C39 -67.7(12) . . . . ? C37 C38 C39 C40 38.9(12) . . . . ? C37 C38 C39 C38' -67.3(12) . . . . ? C37 C38' C39 C40 -12.2(15) . . . . ? C37 C38' C39 C38 70.4(12) . . . . ? C37 O2 C40 C39 1.2(8) . . . . ? K2 O2 C40 C39 153.8(5) . . . . ? C38 C39 C40 O2 -25.6(10) . . . . ? C38' C39 C40 O2 7.3(12) . . . . ? C44 O3 C41 C42 14.3(7) . . . . ? K2 O3 C41 C42 -161.9(4) . . . . ? O3 C41 C42 C43 -30.8(7) . . . . ? C41 C42 C43 C44 34.9(7) . . . . ? C41 O3 C44 C43 8.6(7) . . . . ? K2 O3 C44 C43 -175.4(4) . . . . ? C42 C43 C44 O3 -27.4(7) . . . . ? C48 O4 C45 C46 -3.8(9) . . . . ? K2 O4 C45 C46 -148.1(5) . . . . ? O4 C45 C46 C47 18.8(9) . . . . ? C45 C46 C47 C48 -25.4(8) . . . . ? C45 O4 C48 C47 -13.4(8) . . . . ? K2 O4 C48 C47 131.7(5) . . . . ? C46 C47 C48 O4 24.5(8) . . . . ? _refine_diff_density_max 2.275 _refine_diff_density_min -1.055 _refine_diff_density_rms 0.162 _shelxl_version_number 2013-3 _shelx_res_file ; TITL mm272_4 in P-1 CELL 0.71073 12.55060 12.99330 16.73840 107.0633 98.5557 112.1212 ZERR 2.00 0.00030 0.00030 0.00040 0.0013 0.0014 0.0013 LATT 1 SFAC C H O K GD UNIT 96 128 8 4 4 TEMP -73.15C SIZE 0.12 0.13 0.17 L.S. 80 ACTA CONF BOND FMAP 2 PLAN 5 LIST 0 SADI C38 C37 C38' C37 C38 C39 C38' C39 OMIT 5 -7 14 OMIT -3 2 0 OMIT -13 4 18 OMIT 6 -8 17 OMIT 14 -7 6 OMIT 13 -11 8 OMIT 5 -14 18 OMIT 7 -15 15 OMIT 1 -1 1 OMIT 9 -5 5 OMIT 2 -4 3 OMIT 6 -13 17 OMIT -9 2 3 OMIT 5 -14 19 OMIT 5 6 12 OMIT 11 -3 10 OMIT 6 -14 15 OMIT 10 4 7 OMIT 8 -14 14 OMIT 9 -6 15 OMIT 4 1 18 OMIT 6 -11 14 OMIT -9 -3 8 OMIT 6 -13 19 OMIT 5 -8 16 OMIT 7 -12 14 OMIT 3 -8 21 OMIT 15 -13 7 OMIT 3 -17 2 OMIT -13 2 15 OMIT 4 -9 18 OMIT -9 -6 5 OMIT 4 -11 17 OMIT -9 9 3 OMIT 7 -6 15 OMIT 7 4 3 OMIT 4 -12 18 OMIT 9 -12 12 OMIT 3 -7 16 OMIT -15 8 8 OMIT 13 -10 9 OMIT 9 -7 9 OMIT 12 -10 8 OMIT -15 6 5 OMIT 6 -7 7 OMIT 6 -15 17 OMIT 5 -14 17 OMIT 5 -12 16 OMIT 1 12 5 OMIT 7 -15 2 WGHT 0.042900 BASF 0.49836 FVAR 0.27415 GD1 5 -0.171767 0.976029 0.290100 11.00000 0.02993 0.02907 = 0.03239 0.00996 0.01018 0.01845 GD2 5 0.199650 0.503824 0.232951 11.00000 0.02684 0.02481 = 0.02831 0.00961 0.00708 0.01568 K1 4 -0.000687 0.725715 0.235333 11.00000 0.05181 0.04482 = 0.06005 0.01929 0.01559 0.03644 K2 4 0.406092 0.279450 0.225851 11.00000 0.03309 0.03181 = 0.03564 0.01039 0.00828 0.01673 O1 3 0.299499 0.061260 0.093775 11.00000 0.05781 0.03614 = 0.08117 -0.00305 0.00522 0.01884 O2 3 0.372125 0.167283 0.339181 11.00000 0.08881 0.03969 = 0.04406 0.01844 0.01159 0.02889 O3 3 0.623187 0.394776 0.346886 11.00000 0.03823 0.05229 = 0.06075 0.00663 -0.00472 0.01989 O4 3 0.541995 0.298890 0.115129 11.00000 0.05030 0.06367 = 0.04379 0.02169 0.01535 0.01545 C1 1 -0.129535 1.175202 0.417333 11.00000 0.05464 0.04493 = 0.04444 -0.01290 -0.00553 0.03013 AFIX 43 H1A 2 -0.068236 1.226218 0.471174 11.00000 -1.20000 AFIX 0 C2 1 -0.224569 1.086066 0.426355 11.00000 0.07535 0.07216 = 0.03839 0.01799 0.02514 0.05205 AFIX 43 H2A 2 -0.213327 1.090911 0.484975 11.00000 -1.20000 AFIX 0 C3 1 -0.332067 0.991535 0.370608 11.00000 0.06511 0.07220 = 0.08539 0.04419 0.05648 0.04399 AFIX 43 H3A 2 -0.376031 0.945365 0.399658 11.00000 -1.20000 AFIX 0 C4 1 -0.392179 0.947168 0.280784 11.00000 0.02944 0.05275 = 0.10089 0.00646 0.01992 0.01927 AFIX 43 H4A 2 -0.467651 0.879001 0.263729 11.00000 -1.20000 AFIX 0 C5 1 -0.366913 0.979678 0.212095 11.00000 0.05713 0.09244 = 0.04998 -0.00615 -0.00653 0.05475 AFIX 43 H5A 2 -0.428147 0.927174 0.158456 11.00000 -1.20000 AFIX 0 C6 1 -0.272428 1.071759 0.202179 11.00000 0.12244 0.11861 = 0.04531 0.04579 0.03517 0.10279 AFIX 43 H6A 2 -0.286733 1.070244 0.144399 11.00000 -1.20000 AFIX 0 C7 1 -0.161536 1.165555 0.258642 11.00000 0.10184 0.07371 = 0.11043 0.06899 0.07266 0.07173 AFIX 43 H7A 2 -0.116021 1.210775 0.229713 11.00000 -1.20000 AFIX 0 C8 1 -0.101868 1.208300 0.348893 11.00000 0.06235 0.03343 = 0.10066 0.01771 0.02363 0.02773 AFIX 43 H8A 2 -0.025207 1.275071 0.366408 11.00000 -1.20000 AFIX 0 SIMU C9 C10 C11 C12 C13 C14 C15 C16 = C9' C10' C11' C12' C13' C14' C15' C16' DELU C9 C10 C11 C12 C13 C14 C15 C16 = C9' C10' C11' C12' C13' C14' C15' C16' PART 1 SAME C9' > C16' C9 1 0.052142 0.994931 0.307533 10.50000 0.03280 0.03018 = 0.05022 0.00429 0.01442 0.01691 AFIX 43 H9A 2 0.126418 1.065718 0.331077 10.50000 -1.20000 AFIX 0 C10 1 0.017418 0.951746 0.372354 10.50000 0.03315 0.04980 = 0.02765 0.00488 0.00021 0.02979 AFIX 43 H10A 2 0.077922 0.993890 0.427146 10.50000 -1.20000 AFIX 0 C11 1 -0.085045 0.861758 0.373911 10.50000 0.04991 0.05610 = 0.03669 0.02587 0.01033 0.03702 AFIX 43 H11A 2 -0.079332 0.856953 0.429820 10.50000 -1.20000 AFIX 0 C12 1 -0.196287 0.775333 0.311344 10.50000 0.05023 0.03291 = 0.04367 0.02171 0.02414 0.02239 AFIX 43 H12A 2 -0.251258 0.731800 0.336369 10.50000 -1.20000 AFIX 0 C13 1 -0.244734 0.738629 0.220515 10.50000 0.04052 0.02654 = 0.04006 -0.00599 0.01232 0.00265 AFIX 43 H13A 2 -0.321894 0.671557 0.198155 10.50000 -1.20000 AFIX 0 C14 1 -0.207417 0.776370 0.156057 10.50000 0.04669 0.03516 = 0.02829 -0.00014 -0.00002 0.02325 AFIX 43 H14A 2 -0.264508 0.729011 0.099955 10.50000 -1.20000 AFIX 0 C15 1 -0.104063 0.869012 0.154656 10.50000 0.05858 0.04175 = 0.02784 0.00990 0.01459 0.03262 AFIX 43 H15A 2 -0.108752 0.870790 0.097940 10.50000 -1.20000 AFIX 0 C16 1 0.004944 0.959971 0.217269 10.50000 0.04847 0.03436 = 0.03986 0.01516 0.02427 0.02451 AFIX 43 H16A 2 0.057542 1.007670 0.193080 10.50000 -1.20000 AFIX 0 PART 2 SAME C9 > C16 C9' 1 0.045867 0.982447 0.339429 10.50000 0.02694 0.03643 = 0.04728 0.00979 -0.01065 0.01632 AFIX 43 H9'A 2 0.120540 1.044531 0.379246 10.50000 -1.20000 AFIX 0 C10' 1 -0.025237 0.913360 0.379992 10.50000 0.02999 0.06102 = 0.03622 0.01216 -0.00158 0.02699 AFIX 43 H10B 2 0.012801 0.940080 0.440619 10.50000 -1.20000 AFIX 0 C11' 1 -0.137588 0.815647 0.352017 10.50000 0.05371 0.04599 = 0.03533 0.02103 0.02032 0.02568 AFIX 43 H11B 2 -0.157985 0.789955 0.397605 10.50000 -1.20000 AFIX 0 C12' 1 -0.228909 0.745381 0.270934 10.50000 0.04576 0.02363 = 0.04296 0.00780 0.01751 0.00515 AFIX 43 H12B 2 -0.297398 0.685533 0.275643 10.50000 -1.20000 AFIX 0 C13' 1 -0.242825 0.742584 0.186081 10.50000 0.03251 0.03510 = 0.03519 0.00211 0.00972 0.01769 AFIX 43 H13B 2 -0.316851 0.679207 0.146311 10.50000 -1.20000 AFIX 0 C14' 1 -0.174100 0.810473 0.146198 10.50000 0.04111 0.03497 = 0.02785 0.00807 0.01188 0.02536 AFIX 43 H14B 2 -0.213348 0.784491 0.085887 10.50000 -1.20000 AFIX 0 C15' 1 -0.059857 0.908895 0.173662 10.50000 0.05007 0.03695 = 0.04121 0.02650 0.02306 0.02559 AFIX 43 H15B 2 -0.039916 0.932413 0.127138 10.50000 -1.20000 AFIX 0 C16' 1 0.032313 0.981168 0.253560 10.50000 0.02678 0.03296 = 0.05541 0.01467 0.01865 0.01392 AFIX 43 H16B 2 0.099737 1.042025 0.248683 10.50000 -1.20000 AFIX 0 PART 0 C17 1 0.254081 0.736749 0.294187 11.00000 0.04030 0.02180 = 0.08587 0.00898 0.00351 0.01314 AFIX 43 H17A 2 0.327935 0.806879 0.325308 11.00000 -1.20000 AFIX 0 C18 1 0.194818 0.691678 0.349568 11.00000 0.06308 0.05741 = 0.03381 -0.00968 -0.01245 0.04591 AFIX 43 H18A 2 0.237339 0.739276 0.409533 11.00000 -1.20000 AFIX 0 C19 1 0.087562 0.592986 0.337926 11.00000 0.07013 0.07396 = 0.03758 0.03222 0.03103 0.05810 AFIX 43 H19A 2 0.073703 0.590344 0.391721 11.00000 -1.20000 AFIX 0 C20 1 -0.003877 0.497350 0.265112 11.00000 0.03774 0.05408 = 0.08351 0.04450 0.03464 0.03168 AFIX 43 H20A 2 -0.064396 0.443621 0.280887 11.00000 -1.20000 AFIX 0 C21 1 -0.026350 0.462945 0.174332 11.00000 0.02825 0.02607 = 0.07445 0.00230 -0.00254 0.01398 AFIX 43 H21A 2 -0.098695 0.391242 0.142853 11.00000 -1.20000 AFIX 0 C22 1 0.032750 0.509414 0.119208 11.00000 0.05423 0.05592 = 0.03281 0.00594 -0.00250 0.03894 AFIX 43 H22A 2 -0.009257 0.462196 0.059118 11.00000 -1.20000 AFIX 0 C23 1 0.138830 0.608757 0.131759 11.00000 0.06581 0.07488 = 0.04696 0.03971 0.02880 0.05366 AFIX 43 H23A 2 0.151649 0.613051 0.078063 11.00000 -1.20000 AFIX 0 C24 1 0.229940 0.702579 0.203375 11.00000 0.04606 0.04427 = 0.08916 0.04640 0.03648 0.03023 AFIX 43 H24A 2 0.290027 0.756245 0.187263 11.00000 -1.20000 AFIX 0 C25 1 0.427238 0.548188 0.283751 11.00000 0.02116 0.02695 = 0.08468 0.00605 -0.00108 0.01078 AFIX 43 H25A 2 0.499811 0.620211 0.313342 11.00000 -1.20000 AFIX 0 C26 1 0.375132 0.503843 0.340754 11.00000 0.06086 0.05819 = 0.03202 -0.00059 -0.00604 0.04519 AFIX 43 H26A 2 0.419776 0.553463 0.400085 11.00000 -1.20000 AFIX 0 C27 1 0.272449 0.403508 0.332607 11.00000 0.08348 0.06861 = 0.04936 0.03992 0.04011 0.06174 AFIX 43 H27A 2 0.265036 0.399955 0.387512 11.00000 -1.20000 AFIX 0 C28 1 0.178100 0.307136 0.262279 11.00000 0.04692 0.04118 = 0.08024 0.04032 0.03573 0.02759 AFIX 43 H28A 2 0.120933 0.253528 0.280311 11.00000 -1.20000 AFIX 0 C29 1 0.149113 0.272075 0.171560 11.00000 0.03558 0.02094 = 0.09098 0.00320 0.00290 0.01489 AFIX 43 H29A 2 0.076755 0.199752 0.142295 11.00000 -1.20000 AFIX 0 C30 1 0.200906 0.317719 0.113057 11.00000 0.06085 0.05998 = 0.03058 -0.00332 -0.00282 0.04540 AFIX 43 H30A 2 0.154922 0.269924 0.053730 11.00000 -1.20000 AFIX 0 C31 1 0.303844 0.416636 0.122290 11.00000 0.07928 0.07556 = 0.04371 0.03544 0.03934 0.06180 AFIX 43 H31A 2 0.311800 0.420158 0.067470 11.00000 -1.20000 AFIX 0 C32 1 0.399369 0.513000 0.192416 11.00000 0.05003 0.05910 = 0.10187 0.05396 0.05143 0.04052 AFIX 43 H32A 2 0.457525 0.565603 0.174354 11.00000 -1.20000 AFIX 0 C33 1 0.364729 -0.007534 0.080572 11.00000 0.06636 0.06739 = 0.10542 0.01278 -0.00284 0.03620 AFIX 23 H33A 2 0.413400 0.003720 0.137494 11.00000 -1.20000 H33B 2 0.419643 0.018358 0.046048 11.00000 -1.20000 AFIX 0 C34 1 0.277930 -0.133842 0.033610 11.00000 0.11499 0.05226 = 0.11613 0.03860 0.03904 0.04389 AFIX 23 H34A 2 0.288595 -0.182790 0.066788 11.00000 -1.20000 H34B 2 0.288052 -0.165822 -0.024702 11.00000 -1.20000 AFIX 0 C35 1 0.156611 -0.136198 0.024969 11.00000 0.07569 0.04520 = 0.14311 0.00729 0.01899 0.01851 AFIX 23 H35A 2 0.100655 -0.192378 -0.033774 11.00000 -1.20000 H35B 2 0.121992 -0.160602 0.069629 11.00000 -1.20000 AFIX 0 C36 1 0.179946 -0.011472 0.038666 11.00000 0.05023 0.05743 = 0.08103 0.01174 0.01219 0.02179 AFIX 23 H36A 2 0.171301 -0.000777 -0.017732 11.00000 -1.20000 H36B 2 0.122952 0.009698 0.066716 11.00000 -1.20000 AFIX 0 C37 1 0.398088 0.239564 0.428352 11.00000 0.09272 0.03897 = 0.05176 0.01656 0.01506 0.03107 PART 1 AFIX 23 H37A 2 0.323450 0.226971 0.445581 10.50000 -1.20000 H37B 2 0.444257 0.325899 0.440075 10.50000 -1.20000 AFIX 23 PART 2 H37C 2 0.334329 0.265739 0.435541 10.50000 -1.20000 H37D 2 0.475446 0.312238 0.446473 10.50000 -1.20000 AFIX 0 PART 1 C38 1 0.472057 0.195476 0.475308 10.50000 0.07448 0.04227 = 0.03993 0.01256 0.00275 0.00165 AFIX 23 H38A 2 0.556639 0.231415 0.474468 10.50000 -1.20000 H38B 2 0.470088 0.213620 0.536643 10.50000 -1.20000 AFIX 0 PART 2 C38' 1 0.405433 0.172302 0.484333 10.50000 0.12541 0.03646 = 0.03768 0.02070 0.00675 0.01630 AFIX 23 H38C 2 0.333484 0.148141 0.505171 10.50000 -1.20000 H38D 2 0.478332 0.220188 0.535331 10.50000 -1.20000 AFIX 0 PART 0 C39 1 0.411364 0.064873 0.423781 11.00000 0.14177 0.07198 = 0.07405 0.04112 0.03550 0.07232 PART 1 AFIX 23 H39A 2 0.465844 0.027505 0.431424 10.50000 -1.20000 H39B 2 0.338292 0.024580 0.439752 10.50000 -1.20000 AFIX 23 PART 2 H39C 2 0.493282 0.071135 0.440530 10.50000 -1.20000 H39D 2 0.353859 -0.009434 0.427455 10.50000 -1.20000 AFIX 0 PART 0 C40 1 0.381012 0.060492 0.334262 11.00000 0.07937 0.05029 = 0.06050 0.02294 0.02362 0.03890 AFIX 23 H40A 2 0.444300 0.054450 0.306946 11.00000 -1.20000 H40B 2 0.303641 -0.010429 0.298457 11.00000 -1.20000 AFIX 0 C41 1 0.676869 0.518951 0.401560 11.00000 0.03925 0.04841 = 0.06403 0.01811 -0.00225 0.02379 AFIX 23 H41A 2 0.640529 0.531765 0.449962 11.00000 -1.20000 H41B 2 0.664726 0.566487 0.367555 11.00000 -1.20000 AFIX 0 C42 1 0.806491 0.555844 0.436363 11.00000 0.04498 0.05368 = 0.05647 0.01142 0.00758 0.02020 AFIX 23 H42A 2 0.841345 0.621455 0.494924 11.00000 -1.20000 H42B 2 0.851533 0.582210 0.396591 11.00000 -1.20000 AFIX 0 C43 1 0.807055 0.442498 0.440882 11.00000 0.05546 0.08391 = 0.05899 0.03283 0.01364 0.04531 AFIX 23 H43A 2 0.884151 0.440450 0.436731 11.00000 -1.20000 H43B 2 0.792970 0.433783 0.495698 11.00000 -1.20000 AFIX 0 C44 1 0.705532 0.347352 0.363289 11.00000 0.05313 0.05740 = 0.09149 0.02572 0.01971 0.03223 AFIX 23 H44A 2 0.735093 0.326529 0.312065 11.00000 -1.20000 H44B 2 0.666092 0.273966 0.375236 11.00000 -1.20000 AFIX 0 C45 1 0.651198 0.399765 0.138220 11.00000 0.05153 0.09634 = 0.05375 0.02425 0.01260 -0.00292 AFIX 23 H45A 2 0.717138 0.386188 0.166323 11.00000 -1.20000 H45B 2 0.649601 0.470181 0.180749 11.00000 -1.20000 AFIX 0 C46 1 0.673297 0.423943 0.060182 11.00000 0.06057 0.04391 = 0.06853 0.01990 0.02370 0.01400 AFIX 23 H46A 2 0.729826 0.393999 0.039185 11.00000 -1.20000 H46B 2 0.706096 0.510987 0.072223 11.00000 -1.20000 AFIX 0 C47 1 0.550357 0.355624 -0.004899 11.00000 0.07423 0.08665 = 0.07495 0.04925 0.01321 0.02554 AFIX 23 H47A 2 0.509803 0.407998 -0.004159 11.00000 -1.20000 H47B 2 0.554963 0.321336 -0.064749 11.00000 -1.20000 AFIX 0 C48 1 0.485980 0.258707 0.025400 11.00000 0.05682 0.07333 = 0.04358 0.01880 0.00952 0.01241 AFIX 23 H48A 2 0.400254 0.241810 0.015046 11.00000 -1.20000 H48B 2 0.490375 0.183958 -0.006942 11.00000 -1.20000 AFIX 0 HKLF 5 REM mm272_4 in P-1 REM R1 = 0.0409 for 9370 Fo > 4sig(Fo) and 0.0723 for all 13089 data REM 587 parameters refined using 300 restraints END WGHT 0.0495 0.0000 REM Highest difference peak 2.275, deepest hole -1.055, 1-sigma level 0.162 Q1 1 0.2631 0.5626 0.2331 11.00000 0.05 2.27 Q2 1 -0.2332 0.9101 0.2884 11.00000 0.05 1.96 Q3 1 -0.1019 1.0506 0.2873 11.00000 0.05 1.56 Q4 1 0.1213 0.4232 0.2344 11.00000 0.05 1.42 Q5 1 0.3195 0.6257 0.2406 11.00000 0.05 1.41 ; _shelx_res_checksum 32685 _shelx_hkl_file ; 0 -1 1 382.488 10.9354 -2 1 0 0 382.488 10.9354 1 0 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186.445 4.20867 -2 -5 1 0 186.445 4.20867 1 1 -4 3 1647.94 33.0747 -2 -4 1 0 1647.94 33.0747 1 1 -3 2 69.7324 4.46951 -2 -3 1 0 69.7324 4.46951 1 -2 1 0 4.34845 0.83059 1 -1 1 0 120.776 3.91236 1 -1 0 1 22.3816 1.08943 -2 0 1 0 22.3816 1.08943 1 -1 -1 2 113.565 4.03144 -2 1 1 0 113.565 4.03144 1 -1 -2 3 183.126 7.01226 -2 2 1 0 183.126 7.01226 1 -1 -3 4 203.638 7.80745 -2 3 1 0 203.638 7.80745 1 -1 -4 5 161.650 4.91372 -2 4 1 0 161.650 4.91372 1 -1 -5 6 47.6372 3.64482 -2 5 1 0 47.6372 3.64482 1 -1 -6 7 343.232 9.11557 -2 6 1 0 343.232 9.11557 1 -1 -7 8 177.538 6.69612 -2 7 1 0 177.538 6.69612 1 -1 -8 9 147.498 9.29785 -2 8 1 0 147.498 9.29785 1 -1 -9 10 282.458 14.3823 -2 9 1 0 282.458 14.3823 1 10 1 0 96.1595 5.44584 1 11 1 0 8.48511 2.76213 1 12 1 0 102.758 5.87685 1 13 1 0 12.5492 3.49514 1 14 1 0 17.7074 6.11813 1 -16 2 0 11.1018 4.79823 1 -15 2 0 8.89601 4.97878 1 -14 2 0 1.33782 2.91411 1 -13 2 0 31.4507 3.89666 1 2 -12 10 13.1900 8.01539 -2 -12 2 0 13.1900 8.01539 1 2 -11 9 106.617 9.45345 -2 -11 2 0 106.617 9.45345 1 2 -10 8 12.3959 7.92683 -2 -10 2 0 12.3959 7.92683 1 2 -9 7 95.9844 6.18757 -2 -9 2 0 95.9844 6.18757 1 2 -8 6 750.596 16.8581 -2 -8 2 0 750.596 16.8581 1 2 -7 5 304.908 8.18516 -2 -7 2 0 304.908 8.18516 1 2 -6 4 1108.14 23.1263 -2 -6 2 0 1108.14 23.1263 1 2 -5 3 1055.19 30.9358 -2 -5 2 0 1055.19 30.9358 1 -4 2 0 163.466 3.01382 1 -3 2 0 21.6276 1.05217 1 -2 2 0 1411.24 39.7212 1 -1 2 0 935.589 26.3271 1 -2 0 2 4123.05 113.569 -2 0 2 0 4123.05 113.569 1 -2 -1 3 16.9619 2.34195 -2 1 2 0 16.9619 2.34195 1 -2 -2 4 1730.84 50.5696 -2 2 2 0 1730.84 50.5696 1 -2 -3 5 891.516 27.4228 -2 3 2 0 891.516 27.4228 1 -2 -4 6 249.967 9.99282 -2 4 2 0 249.967 9.99282 1 -2 -5 7 859.760 27.5733 -2 5 2 0 859.760 27.5733 1 -2 -6 8 409.053 14.5215 -2 6 2 0 409.053 14.5215 1 -2 -7 9 370.903 15.6652 -2 7 2 0 370.903 15.6652 1 8 2 0 330.034 7.60267 1 9 2 0 31.6365 3.53730 1 10 2 0 62.6082 4.59328 1 11 2 0 66.1590 4.92563 1 12 2 0 11.1733 3.33382 1 13 2 0 29.5649 6.33992 1 14 2 0 7.13229 5.91162 1 -16 3 0 16.4776 5.30041 1 -15 3 0 137.529 7.26023 1 -14 3 0 10.9890 3.18894 1 -13 3 0 95.8642 5.52776 1 -12 3 0 231.670 8.05405 1 -11 3 0 0.50795 2.19349 1 3 -10 7 365.660 15.2802 -2 -10 3 0 365.660 15.2802 1 3 -9 6 636.172 21.7019 -2 -9 3 0 636.172 21.7019 1 -8 3 0 13.7175 1.63802 1 -7 3 0 581.542 10.7345 1 -6 3 0 23.3880 1.31575 1 -5 3 0 77.2384 1.98802 1 -4 3 0 14.8652 0.98195 1 -3 3 0 27.5273 2.05347 1 -2 3 0 93.9765 4.70174 1 -3 1 2 65.8605 5.13763 -2 -1 3 0 65.8605 5.13763 1 -3 0 3 27.0340 1.99125 -2 0 3 0 27.0340 1.99125 1 -3 -1 4 0.86815 1.77390 -2 1 3 0 0.86815 1.77390 1 -3 -2 5 12.5557 3.60070 -2 2 3 0 12.5557 3.60070 1 -3 -3 6 135.663 6.95937 -2 3 3 0 135.663 6.95937 1 -3 -4 7 101.929 6.92787 -2 4 3 0 101.929 6.92787 1 5 3 0 0.75285 1.35967 1 6 3 0 96.8760 3.72446 1 7 3 0 52.2414 3.00709 1 8 3 0 3.80385 1.97872 1 9 3 0 92.3889 5.55111 1 10 3 0 13.9949 3.19522 1 11 3 0 14.9458 3.45444 1 12 3 0 46.9507 4.80591 1 13 3 0 15.1294 6.63000 1 -15 4 0 6.06798 3.13184 1 -14 4 0 7.58739 2.90794 1 -13 4 0 -1.4314 2.35466 1 -12 4 0 14.0818 2.92766 1 -11 4 0 40.8808 3.61044 1 -10 4 0 60.0534 3.30368 1 -9 4 0 97.5110 3.65791 1 -8 4 0 40.0075 2.32622 1 -7 4 0 1.79047 1.00517 1 -6 4 0 815.104 12.4168 1 -5 4 0 1002.00 14.8869 1 -4 4 0 64.2120 3.04579 1 -3 4 0 53.6139 2.75142 1 -4 2 2 170.990 7.81863 -2 -2 4 0 170.990 7.81863 1 -4 1 3 4090.82 116.897 -2 -1 4 0 4090.82 116.897 1 -4 0 4 4575.58 74.3792 -2 0 4 0 4575.58 74.3792 1 -4 -1 5 424.921 9.82819 -2 1 4 0 424.921 9.82819 1 -4 -2 6 1130.56 34.3418 -2 2 4 0 1130.56 34.3418 1 -4 -3 7 849.459 27.0815 -2 3 4 0 849.459 27.0815 1 4 4 0 167.981 4.43661 1 -4 -5 9 1433.83 44.7412 -2 5 4 0 1433.83 44.7412 1 6 4 0 102.967 3.89118 1 7 4 0 59.8759 3.35064 1 8 4 0 272.578 9.06071 1 9 4 0 2.58648 2.52166 1 10 4 0 95.6301 5.98448 1 11 4 0 32.7299 4.30502 1 12 4 0 5.27439 5.15213 1 -15 5 0 174.908 11.3783 1 -14 5 0 4.73692 4.79713 1 -13 5 0 129.861 6.12022 1 -12 5 0 77.5847 4.77310 1 -11 5 0 3.42491 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7.18772 1 11 -10 8 -18.402 12.6832 -2 10 -11 9 -18.402 12.6832 1 11 -11 9 40.8900 15.1509 -2 11 -11 9 40.8900 15.1509 1 11 -12 10 293.803 20.7304 -2 12 -11 9 293.803 20.7304 1 11 -13 11 -25.457 16.1372 -2 13 -11 9 -25.457 16.1372 1 11 -14 12 126.901 19.6421 -2 14 -11 9 126.901 19.6421 1 11 -15 13 -5.5015 17.9344 -2 15 -11 9 -5.5015 17.9344 1 -9 -10 9 8.84485 6.43548 1 -8 -10 9 1.29718 3.62478 1 -7 -10 9 2.63692 3.24387 1 -6 -10 9 54.3512 4.96496 1 -5 -10 9 21.2203 3.61539 1 -4 -10 9 57.0921 4.63381 1 -3 -10 9 121.040 5.92331 1 -2 -10 9 4.18352 1.58548 1 -1 -10 9 292.290 5.02145 1 0 -10 9 278.754 5.27939 1 -10 1 0 229.967 10.5695 -2 1 -10 9 229.967 10.5695 1 10 -2 1 381.284 14.6013 -2 2 -10 9 381.284 14.6013 1 3 -10 9 186.912 4.78650 1 4 -10 9 230.025 6.57411 1 10 -5 4 798.778 29.1601 -2 5 -10 9 798.778 29.1601 1 10 -6 5 146.716 13.6346 -2 6 -10 9 146.716 13.6346 1 7 -10 9 126.246 7.01592 1 10 -8 7 418.839 20.2010 -2 8 -10 9 418.839 20.2010 1 10 -9 8 54.7860 12.9247 -2 9 -10 9 54.7860 12.9247 1 10 -10 9 385.646 21.1058 -2 10 -10 9 385.646 21.1058 1 10 -11 10 60.8589 15.3888 -2 11 -10 9 60.8589 15.3888 1 10 -12 11 53.7597 14.9186 -2 12 -10 9 53.7597 14.9186 1 10 -13 12 36.8631 16.5807 -2 13 -10 9 36.8631 16.5807 1 10 -14 13 -0.8809 16.8646 -2 14 -10 9 -0.8809 16.8646 1 10 -15 14 -0.7588 17.9305 -2 15 -10 9 -0.7588 17.9305 1 -10 -9 9 57.2118 9.05956 1 -9 -9 9 3.99875 3.65018 1 -8 -9 9 44.8759 4.82610 1 -7 -9 9 76.4525 5.63541 1 -6 -9 9 -0.3174 2.81133 1 -5 -9 9 171.316 6.96940 1 -4 -9 9 35.7447 3.69756 1 -3 -9 9 -0.8502 2.24509 1 -2 -9 9 46.3929 2.58381 1 -1 -9 9 21.1940 1.72980 1 9 0 0 200.954 7.17853 -2 0 -9 9 200.954 7.17853 1 9 -1 1 392.008 13.8917 -2 1 -9 9 392.008 13.8917 1 9 -2 2 92.3260 5.14131 -2 2 -9 9 92.3260 5.14131 1 9 -3 3 0.87146 3.64862 -2 3 -9 9 0.87146 3.64862 1 9 -4 4 66.0170 10.6855 -2 4 -9 9 66.0170 10.6855 1 9 -5 5 19.4576 10.5024 -2 5 -9 9 19.4576 10.5024 1 9 -6 6 17.6137 10.5598 -2 6 -9 9 17.6137 10.5598 1 9 -7 7 -6.6364 9.99675 -2 7 -9 9 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9.13259 1 8 -5 6 1221.51 27.4252 -2 5 -8 9 1221.51 27.4252 1 8 -6 7 81.3601 10.5506 -2 6 -8 9 81.3601 10.5506 1 8 -7 8 1037.45 24.0816 -2 7 -8 9 1037.45 24.0816 1 8 -8 9 264.364 15.0269 -2 8 -8 9 264.364 15.0269 1 8 -9 10 0.12992 5.33339 -2 9 -8 9 0.12992 5.33339 1 8 -10 11 355.749 11.9239 -2 10 -8 9 355.749 11.9239 1 8 -11 12 20.7495 6.04008 -2 11 -8 9 20.7495 6.04008 1 8 -12 13 115.998 8.48121 -2 12 -8 9 115.998 8.48121 1 8 -13 14 58.4639 14.5237 -2 13 -8 9 58.4639 14.5237 1 8 -14 15 13.8653 13.9727 -2 14 -8 9 13.8653 13.9727 1 8 -15 16 20.9027 16.0312 -2 15 -8 9 20.9027 16.0312 1 -11 -7 9 27.4358 6.80423 1 -10 -7 9 58.7733 5.22892 1 -9 -7 9 9.94227 3.30464 1 -8 -7 9 161.341 7.23251 1 -7 -7 9 155.458 6.76169 1 -6 -7 9 34.6761 3.62644 1 -5 -7 9 96.3012 5.15766 1 -4 -7 9 63.7981 4.00018 1 -3 -7 9 74.8531 3.68731 1 -2 -7 9 207.505 4.29869 1 -1 -7 9 15.2301 1.35553 1 7 0 2 58.5523 3.58999 -2 0 -7 9 58.5523 3.58999 1 7 -1 3 273.994 7.33144 -2 1 -7 9 273.994 7.33144 1 7 -2 4 55.8287 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1.13931 1 -1 -6 9 530.860 7.68000 1 6 0 3 429.086 9.41726 -2 0 -6 9 429.086 9.41726 1 6 -1 4 149.037 3.72929 -2 1 -6 9 149.037 3.72929 1 6 -2 5 633.096 10.5464 -2 2 -6 9 633.096 10.5464 1 6 -3 6 421.279 8.83514 -2 3 -6 9 421.279 8.83514 1 6 -4 7 830.452 19.2439 -2 4 -6 9 830.452 19.2439 1 6 -5 8 1168.23 26.0443 -2 5 -6 9 1168.23 26.0443 1 6 -6 9 44.0678 4.76107 -2 6 -6 9 44.0678 4.76107 1 6 -7 10 996.186 23.1075 -2 7 -6 9 996.186 23.1075 1 6 -8 11 265.067 9.21107 -2 8 -6 9 265.067 9.21107 1 6 -9 12 275.630 9.71961 -2 9 -6 9 275.630 9.71961 1 6 -10 13 210.721 9.07740 -2 10 -6 9 210.721 9.07740 1 6 -11 14 9.69915 6.03797 -2 11 -6 9 9.69915 6.03797 1 6 -12 15 182.306 9.43097 -2 12 -6 9 182.306 9.43097 1 6 -13 16 86.0570 8.58127 -2 13 -6 9 86.0570 8.58127 1 6 -14 17 30.8328 8.50673 -2 14 -6 9 30.8328 8.50673 1 -13 -5 9 53.8125 8.59434 1 -12 -5 9 2.46684 3.12796 1 -11 -5 9 45.1016 4.60805 1 -10 -5 9 137.931 6.67053 1 -9 -5 9 1.93382 2.50652 1 -8 -5 9 191.077 7.25195 1 -7 -5 9 112.952 5.50611 1 -6 -5 9 73.2764 3.54480 1 -5 -5 9 587.357 11.3664 1 -4 -5 9 97.8529 4.05792 1 -3 -5 9 61.4852 2.06107 1 -2 -5 9 408.275 7.70752 1 -1 -5 9 0.95175 0.96980 1 5 0 4 598.938 10.4918 -2 0 -5 9 598.938 10.4918 1 5 -1 5 311.361 5.63764 -2 1 -5 9 311.361 5.63764 1 5 -2 6 53.1717 2.83328 -2 2 -5 9 53.1717 2.83328 1 5 -3 7 135.099 4.58349 -2 3 -5 9 135.099 4.58349 1 5 -4 8 4.64864 3.47962 -2 4 -5 9 4.64864 3.47962 1 5 -5 9 203.693 7.31396 -2 5 -5 9 203.693 7.31396 1 5 -6 10 12.2753 3.95583 -2 6 -5 9 12.2753 3.95583 1 5 -7 11 6.18333 4.69264 -2 7 -5 9 6.18333 4.69264 1 5 -8 12 16.1457 4.88189 -2 8 -5 9 16.1457 4.88189 1 5 -9 13 73.2920 6.41877 -2 9 -5 9 73.2920 6.41877 1 5 -10 14 20.1792 5.85941 -2 10 -5 9 20.1792 5.85941 1 5 -11 15 39.6617 6.83694 -2 11 -5 9 39.6617 6.83694 1 5 -12 16 22.1271 7.10787 -2 12 -5 9 22.1271 7.10787 1 5 -13 17 49.5376 8.29867 -2 13 -5 9 49.5376 8.29867 1 5 -14 18 54.2009 9.40775 -2 14 -5 9 54.2009 9.40775 1 -13 -4 9 -0.1985 4.61135 1 -12 -4 9 0.28826 2.90974 1 -11 -4 9 -1.4765 2.41448 1 -10 -4 9 -3.9101 2.44468 1 -9 -4 9 5.51959 2.62812 1 -8 -4 9 4.65790 2.49993 1 -7 -4 9 67.8961 3.43485 1 -6 -4 9 26.4837 2.26727 1 -5 -4 9 6.60258 1.88000 1 -4 -4 9 188.466 5.52209 1 -3 -4 9 207.113 4.46236 1 -2 -4 9 128.314 3.17429 1 -1 -4 9 515.806 8.19923 1 4 0 5 369.726 9.68307 -2 0 -4 9 369.726 9.68307 1 4 -1 6 266.699 7.63704 -2 1 -4 9 266.699 7.63704 1 4 -2 7 931.087 16.5286 -2 2 -4 9 931.087 16.5286 1 4 -3 8 6.65528 2.94870 -2 3 -4 9 6.65528 2.94870 1 4 -4 9 845.694 15.7477 -2 4 -4 9 845.694 15.7477 1 4 -5 10 665.392 16.3756 -2 5 -4 9 665.392 16.3756 1 4 -6 11 236.682 8.66297 -2 6 -4 9 236.682 8.66297 1 4 -7 12 799.918 19.5354 -2 7 -4 9 799.918 19.5354 1 4 -8 13 55.3896 5.18664 -2 8 -4 9 55.3896 5.18664 1 4 -9 14 248.908 9.62747 -2 9 -4 9 248.908 9.62747 1 4 -10 15 224.108 9.73183 -2 10 -4 9 224.108 9.73183 1 4 -11 16 71.5096 7.41332 -2 11 -4 9 71.5096 7.41332 1 4 -12 17 113.688 8.99541 -2 12 -4 9 113.688 8.99541 1 4 -13 18 63.6618 8.76374 -2 13 -4 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-6 21 -1.8526 6.30009 1 -9 -5 21 7.32130 5.16038 1 -8 -5 21 2.96202 5.16037 1 -7 -5 21 -3.5607 3.13852 1 -6 -5 21 6.30668 3.66283 1 -5 -5 21 -0.3954 3.27010 1 -4 -5 21 -0.8706 3.07361 1 -3 -5 21 -3.4240 2.94671 1 -2 -5 21 3.07713 2.77726 1 -1 -5 21 3.06642 2.79988 1 0 -5 21 4.29394 2.79437 1 1 -5 21 5.22910 3.70329 1 2 -5 21 16.1001 3.55630 1 3 -5 21 0.33982 3.12826 1 4 -5 21 4.04871 3.84301 1 5 -5 21 38.6835 8.10030 1 -10 -4 21 21.6695 5.78234 1 -9 -4 21 13.4380 5.27867 1 -8 -4 21 10.1065 5.26526 1 -7 -4 21 36.3230 4.90713 1 -6 -4 21 2.41611 3.38144 1 -5 -4 21 43.5698 5.01932 1 -4 -4 21 57.7790 5.29585 1 -3 -4 21 5.86362 3.45080 1 -2 -4 21 64.4015 4.64099 1 -1 -4 21 15.5166 3.03503 1 0 -4 21 14.9872 3.12549 1 1 -4 21 81.1209 6.55181 1 2 -4 21 -0.2817 3.07735 1 3 -4 21 28.9933 4.63843 1 4 -4 21 29.2964 7.50551 1 -10 -3 21 2.30505 4.89738 1 -9 -3 21 17.4648 5.90329 1 -8 -3 21 8.55192 5.52370 1 -7 -3 21 14.0747 4.01153 1 -6 -3 21 2.71348 3.60106 1 -5 -3 21 0.76612 3.15213 1 -4 -3 21 4.83062 3.35634 1 -3 -3 21 2.09037 2.53393 1 -2 -3 21 2.34433 3.40336 1 -1 -3 21 4.70446 3.70201 1 0 -3 21 -5.3529 3.18980 1 1 -3 21 3.92470 3.07114 1 2 -3 21 -0.0164 2.88132 1 3 -3 21 11.2115 6.56438 1 4 -3 21 9.95864 6.52318 1 -10 -2 21 26.1100 4.58834 1 -9 -2 21 2.89186 4.94645 1 -8 -2 21 26.3527 6.54116 1 -7 -2 21 62.0250 5.78798 1 -6 -2 21 0.16996 3.13336 1 -5 -2 21 53.0251 7.70147 1 -4 -2 21 25.9265 6.28229 1 -3 -2 21 9.54932 3.67715 1 -2 -2 21 94.1015 6.67831 1 -1 -2 21 22.1285 4.29649 1 0 -2 21 38.2673 5.05393 1 1 -2 21 46.2714 4.40135 1 2 -2 21 1.02560 6.05741 1 3 -2 21 49.1809 8.62315 1 -10 -1 21 1.65866 5.32004 1 -9 -1 21 9.39624 5.99343 1 -8 -1 21 14.6212 6.33690 1 -7 -1 21 -0.4560 5.56644 1 -6 -1 21 26.6579 6.76464 1 -5 -1 21 1.03596 5.24317 1 -4 -1 21 -2.8387 3.24936 1 -3 -1 21 7.09621 3.51346 1 -2 -1 21 -0.7128 3.40417 1 -1 -1 21 -0.0711 3.45282 1 0 -1 21 -2.1756 3.40941 1 1 -1 21 2.66475 3.67880 1 2 -1 21 1.05643 6.19566 1 -10 0 21 18.5071 6.72495 1 -9 0 21 10.4070 5.96204 1 -8 0 21 27.4350 6.68015 1 -7 0 21 24.0191 7.04785 1 -6 0 21 4.38934 5.66910 1 -5 0 21 49.6365 7.74544 1 -4 0 21 20.7449 4.30069 1 -3 0 21 11.6716 3.86970 1 -2 0 21 47.1988 5.13305 1 -1 0 21 4.62218 3.67070 1 0 0 21 43.5674 4.35867 1 1 0 21 46.7918 8.24938 1 -10 1 21 -2.9004 5.49971 1 -9 1 21 30.8547 7.23082 1 -8 1 21 2.36815 5.63112 1 -7 1 21 18.4045 6.73576 1 -6 1 21 13.4775 6.33558 1 -5 1 21 5.82349 5.58441 1 -4 1 21 11.4630 6.08405 1 -3 1 21 -2.7326 5.42295 1 -2 1 21 -5.4780 3.35057 1 -1 1 21 -2.0164 3.28208 1 0 1 21 3.49507 5.81994 1 -9 2 21 0.91463 6.21654 1 -8 2 21 18.1512 6.89721 1 -7 2 21 23.7085 7.16449 1 -6 2 21 6.73844 6.04691 1 -5 2 21 35.5936 7.97993 1 -4 2 21 -0.9431 5.63406 1 -3 2 21 8.02701 5.75694 1 -2 2 21 66.0128 8.74109 1 -8 3 21 -3.0307 5.86976 1 -7 3 21 22.6668 7.40761 1 -6 3 21 20.7194 7.11380 1 -5 3 21 -5.6328 5.46136 1 -4 3 21 -4.0026 5.73997 1 -3 3 21 10.7109 6.31429 1 0 -12 22 -5.8167 4.38281 1 1 -12 22 7.33689 4.50134 1 -3 -11 22 24.8659 4.41159 1 -2 -11 22 35.5093 4.82188 1 -1 -11 22 3.41099 3.39101 1 0 -11 22 19.9527 5.82491 1 1 -11 22 0.45986 4.04004 1 -4 -10 22 3.08298 3.52125 1 -3 -10 22 -0.0963 3.28140 1 -2 -10 22 2.03796 3.31368 1 -1 -10 22 19.1325 4.05255 1 0 -10 22 6.49824 3.26539 1 1 -10 22 16.1630 3.75138 1 -5 -9 22 37.7401 4.92474 1 -4 -9 22 -0.3472 3.34719 1 -3 -9 22 48.6263 5.45355 1 -2 -9 22 24.0790 4.31632 1 -1 -9 22 6.04871 3.58688 1 0 -9 22 44.1662 5.00411 1 1 -9 22 3.46473 3.17638 1 2 -9 22 18.2474 5.63890 1 4 -9 22 -1.9694 6.43577 1 -6 -8 22 -4.1072 3.20118 1 -5 -8 22 -3.0473 3.24479 1 -4 -8 22 1.36745 3.43236 1 -3 -8 22 2.06949 3.58774 1 -2 -8 22 1.09127 3.48556 1 -1 -8 22 2.52733 3.43852 1 0 -8 22 4.41045 3.00442 1 1 -8 22 19.1336 3.48896 1 2 -8 22 19.6612 5.89564 1 3 -8 22 6.01558 4.76445 1 4 -8 22 19.6013 7.29905 1 -7 -7 22 -0.3606 3.49836 1 -6 -7 22 25.5510 4.39731 1 -5 -7 22 20.3204 4.36569 1 -4 -7 22 -1.9853 3.40983 1 -3 -7 22 49.5064 5.38286 1 -2 -7 22 28.4852 4.60644 1 -1 -7 22 20.1459 4.25871 1 0 -7 22 47.5154 4.42543 1 1 -7 22 3.75918 3.74206 1 2 -7 22 26.3338 6.36890 1 3 -7 22 23.9416 4.61795 1 4 -7 22 3.55940 6.60733 1 -8 -6 22 -2.8300 3.42491 1 -7 -6 22 -3.7205 3.22567 1 -6 -6 22 -3.4623 3.27025 1 -5 -6 22 -1.5492 3.45105 1 -4 -6 22 -1.8822 3.24285 1 -3 -6 22 -1.2850 3.19708 1 -2 -6 22 -3.3151 3.01527 1 -1 -6 22 14.3345 3.49224 1 0 -6 22 2.72819 2.85901 1 1 -6 22 13.4767 4.27735 1 2 -6 22 2.68351 4.79649 1 3 -6 22 5.11369 3.91031 1 4 -6 22 29.1569 4.97079 1 -8 -5 22 30.1667 4.76159 1 -7 -5 22 -5.6179 3.31055 1 -6 -5 22 40.1962 5.04798 1 -5 -5 22 29.9558 4.76844 1 -4 -5 22 15.0396 4.00626 1 -3 -5 22 54.0058 5.50450 1 -2 -5 22 13.1012 3.26189 1 -1 -5 22 39.2432 4.12350 1 0 -5 22 47.4949 4.33753 1 1 -5 22 -2.1541 3.70759 1 2 -5 22 22.2295 6.04614 1 3 -5 22 25.1858 4.74596 1 -9 -4 22 -0.7667 4.80877 1 -8 -4 22 2.05601 3.58763 1 -7 -4 22 2.29758 3.70261 1 -6 -4 22 -0.1328 3.45518 1 -5 -4 22 -0.2217 3.38601 1 -4 -4 22 0.52173 3.45808 1 -3 -4 22 -2.4477 3.17519 1 -2 -4 22 -1.2815 2.77164 1 -1 -4 22 -4.6653 3.41732 1 0 -4 22 1.65448 3.83957 1 1 -4 22 5.19443 4.89492 1 2 -4 22 9.57790 3.99522 1 3 -4 22 -0.5840 6.35345 1 -9 -3 22 7.82686 5.45010 1 -8 -3 22 31.1786 4.87403 1 -7 -3 22 -1.6368 3.54438 1 -6 -3 22 57.3143 5.77297 1 -5 -3 22 14.5713 4.12080 1 -4 -3 22 5.12317 4.88965 1 -3 -3 22 82.1680 6.57573 1 -2 -3 22 -0.8996 3.55171 1 -1 -3 22 25.6903 4.73345 1 0 -3 22 28.5951 4.93163 1 1 -3 22 -11.114 4.29515 1 2 -3 22 49.7222 5.73227 1 -9 -2 22 0.20062 5.29528 1 -8 -2 22 6.05919 4.06222 1 -7 -2 22 6.73086 5.73978 1 -6 -2 22 -4.3934 5.16489 1 -5 -2 22 5.70036 5.41470 1 -4 -2 22 6.21371 5.42252 1 -3 -2 22 -3.3414 3.30144 1 -2 -2 22 -0.5877 3.46616 1 -1 -2 22 0.07962 3.52111 1 0 -2 22 -3.7375 4.77145 1 1 -2 22 3.06955 3.90663 1 -9 -1 22 25.1971 7.07585 1 -8 -1 22 5.46881 6.05659 1 -7 -1 22 4.50860 5.56093 1 -6 -1 22 49.8549 8.40174 1 -5 -1 22 21.5473 6.28301 1 -4 -1 22 29.0678 6.92125 1 -3 -1 22 31.7790 4.79758 1 -2 -1 22 -0.0927 3.55032 1 -1 -1 22 48.4052 5.66246 1 0 -1 22 34.3431 7.07914 1 -8 0 22 16.7610 6.91557 1 -7 0 22 9.88381 6.10012 1 -6 0 22 -2.5006 5.35468 1 -5 0 22 16.0866 6.64821 1 -4 0 22 -2.2409 3.34014 1 -3 0 22 -2.0839 3.35665 1 -2 0 22 -0.2973 3.57180 1 -1 0 22 -13.439 4.41461 1 -8 1 22 1.83736 6.26389 1 -7 1 22 6.24287 6.60127 1 -6 1 22 20.6428 6.95561 1 -5 1 22 4.21553 6.17436 1 -4 1 22 25.5223 7.01441 1 -3 1 22 38.7846 7.87509 1 -1 -10 23 27.4475 4.61722 1 0 -10 23 9.68067 3.78698 1 -3 -9 23 1.50782 3.40944 1 -2 -9 23 -0.7326 3.25408 1 -1 -9 23 -1.2239 3.34379 1 0 -9 23 24.2056 4.31244 1 1 -9 23 25.1183 6.28760 1 -4 -8 23 42.0216 5.29104 1 -3 -8 23 3.67561 3.55722 1 -2 -8 23 21.0445 4.32591 1 -1 -8 23 24.0143 4.50437 1 0 -8 23 5.88558 3.38708 1 1 -8 23 28.0842 6.66577 1 2 -8 23 16.1351 5.57861 1 -5 -7 23 2.57222 3.54563 1 -4 -7 23 0.39987 3.29935 1 -3 -7 23 -1.4584 3.41693 1 -2 -7 23 7.71143 3.75847 1 -1 -7 23 4.38113 3.61148 1 0 -7 23 7.12673 3.51715 1 1 -7 23 2.26846 4.98232 1 2 -7 23 1.48473 4.74531 1 -6 -6 23 13.2841 4.12882 1 -5 -6 23 13.5686 4.14824 1 -4 -6 23 34.9323 5.04266 1 -3 -6 23 -6.1348 3.24803 1 -2 -6 23 25.6089 4.49986 1 -1 -6 23 40.0111 5.00228 1 0 -6 23 5.20916 3.42351 1 1 -6 23 29.8229 6.69385 1 2 -6 23 5.81232 5.02834 1 -7 -5 23 -3.5396 3.38395 1 -6 -5 23 2.39843 3.74700 1 -5 -5 23 -6.6115 3.14536 1 -4 -5 23 -6.5570 3.22892 1 -3 -5 23 -1.6028 3.58961 1 -2 -5 23 1.28317 3.40624 1 -1 -5 23 -3.4218 3.00272 1 0 -5 23 6.45574 5.43742 1 1 -5 23 6.80718 5.55229 1 -7 -4 23 38.2003 5.28802 1 -6 -4 23 3.52246 3.81506 1 -5 -4 23 13.8568 4.21603 1 -4 -4 23 45.7372 5.34590 1 -3 -4 23 0.93477 5.43284 1 -2 -4 23 25.5405 6.70349 1 -1 -4 23 27.4235 6.99293 1 0 -4 23 8.67479 5.84796 1 1 -4 23 37.0661 6.97585 1 -7 -3 23 9.30662 3.89390 1 -6 -3 23 2.97992 5.04902 1 -5 -3 23 -3.4892 4.94238 1 -4 -3 23 3.61381 5.72414 1 -3 -3 23 -2.7346 5.16740 1 -2 -3 23 -5.1512 4.81519 1 -1 -3 23 -2.4589 5.05238 1 0 -3 23 2.35350 5.43448 1 -7 -2 23 30.8743 7.06645 1 -6 -2 23 9.23377 5.93627 1 -5 -2 23 13.6832 6.22895 1 -4 -2 23 15.3612 6.59581 1 -3 -2 23 -3.2813 5.06355 1 -2 -2 23 49.5466 8.03011 1 -1 -2 23 34.4785 7.22789 1 -6 -1 23 5.29973 6.01581 1 -5 -1 23 -0.2509 5.50704 1 -4 -1 23 2.60057 5.70478 1 -3 -1 23 -0.1295 5.47008 1 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 83910 data_mm297 _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C21 H36 Er Si3' _chemical_formula_weight 540.03 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Er' 'Er' -0.2586 4.9576 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system tetragonal _space_group_IT_number 82 _space_group_name_H-M_alt 'I -4' _space_group_name_Hall 'I -4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' _cell_length_a 16.8620(4) _cell_length_b 16.8620(4) _cell_length_c 20.2149(5) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 5747.6(3) _cell_formula_units_Z 8 _cell_measurement_temperature 200(2) _cell_measurement_reflns_used 9976 _cell_measurement_theta_min 2.42 _cell_measurement_theta_max 27.56 _exptl_crystal_description block _exptl_crystal_colour orange _exptl_crystal_density_meas n/a _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.248 _exptl_crystal_F_000 2176 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.170 _exptl_crystal_size_mid 0.130 _exptl_crystal_size_min 0.070 _exptl_absorpt_coefficient_mu 3.047 _shelx_estimated_absorpt_T_min 0.625 _shelx_estimated_absorpt_T_max 0.815 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6070 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_process_details 'SADABS, Bruker (2003)' _exptl_special_details ; Data collection is performed with three batch runs at phi = 0.00 deg (650 frames), at phi = 120.00 deg (650 frames), and at phi = 240.00 deg (650 frames). Frame width = 0.30 deg in omega. Data is merged, corrected for decay (if any), and treated with multi-scan absorption corrections (if required). All symmetry-equivalent reflections are merged for centrosymmetric data. Friedel pairs are not merged for noncentrosymmetric data. ; _diffrn_ambient_temperature 200(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 28967 _diffrn_reflns_av_unetI/netI 0.0354 _diffrn_reflns_av_R_equivalents 0.0309 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_theta_min 1.573 _diffrn_reflns_theta_max 28.279 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measured_fraction_theta_full 0.990 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_Laue_measured_fraction_full 0.990 _diffrn_reflns_point_group_measured_fraction_max 0.991 _diffrn_reflns_point_group_measured_fraction_full 0.990 _reflns_number_total 7058 _reflns_number_gt 6433 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.941 _reflns_Friedel_fraction_max 0.991 _reflns_Friedel_fraction_full 0.990 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX II, Bruker (2009)' _computing_cell_refinement 'APEX II, Bruker (2009)' _computing_data_reduction 'XPREP, Bruker (2009)' _computing_structure_solution 'SHELXS-03 (Sheldrick, 2003)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'SHELXTL, Bruker (2004)' _computing_publication_material 'SHELXTL, Bruker (2004)' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0384P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 2881 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons and Flack (2004), Acta Cryst. A60, s61). ; _refine_ls_abs_structure_Flack 0.051(5) _chemical_absolute_configuration ? _refine_ls_number_reflns 7058 _refine_ls_number_parameters 226 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0346 _refine_ls_R_factor_gt 0.0277 _refine_ls_wR_factor_ref 0.0658 _refine_ls_wR_factor_gt 0.0630 _refine_ls_goodness_of_fit_ref 1.012 _refine_ls_restrained_S_all 1.012 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Er1 Er 0.08251(2) 0.58973(2) 0.96576(2) 0.03533(8) Uani 1 1 d . . . . . Si1 Si 0.06380(12) 0.75657(11) 0.81508(9) 0.0508(4) Uani 1 1 d . . . . . Si2 Si 0.12502(12) 0.68772(11) 1.15123(9) 0.0532(4) Uani 1 1 d . . . . . Si3 Si 0.15879(9) 0.36157(9) 1.02881(10) 0.0431(3) Uani 1 1 d . . . . . C1 C 0.1086(4) 0.7079(3) 0.8899(3) 0.0423(13) Uani 1 1 d . . . . . C2 C 0.0783(4) 0.7378(3) 0.9504(3) 0.0398(14) Uani 1 1 d . . . . . H2A H 0.0389 0.7770 0.9429 0.048 Uiso 1 1 calc R U . . . C3 C 0.0906(4) 0.7253(4) 1.0192(3) 0.0405(13) Uani 1 1 d . . . . . H3A H 0.0579 0.7590 1.0451 0.049 Uiso 1 1 calc R U . . . C4 C 0.1378(4) 0.6769(4) 1.0588(3) 0.0443(13) Uani 1 1 d . . . . . C5 C 0.1975(4) 0.6206(4) 1.0423(4) 0.0491(14) Uani 1 1 d . . . . . H5A H 0.2201 0.5970 1.0806 0.059 Uiso 1 1 calc R U . . . C6 C 0.2315(4) 0.5910(4) 0.9836(4) 0.053(2) Uani 1 1 d . . . . . H6A H 0.2720 0.5532 0.9920 0.064 Uiso 1 1 calc R U . . . C7 C 0.2199(4) 0.6041(4) 0.9158(4) 0.0533(18) Uani 1 1 d . . . . . H7A H 0.2549 0.5734 0.8894 0.064 Uiso 1 1 calc R U . . . C8 C 0.1695(4) 0.6512(4) 0.8774(3) 0.0502(15) Uani 1 1 d . . . . . H8A H 0.1780 0.6435 0.8314 0.060 Uiso 1 1 calc R U . . . C9 C 0.1172(6) 0.8523(5) 0.8023(4) 0.080(3) Uani 1 1 d . . . . . H9A H 0.0953 0.8795 0.7635 0.120 Uiso 1 1 calc R U . . . H9B H 0.1737 0.8418 0.7951 0.120 Uiso 1 1 calc R U . . . H9C H 0.1106 0.8859 0.8415 0.120 Uiso 1 1 calc R U . . . C10 C -0.0448(5) 0.7734(6) 0.8262(4) 0.078(2) Uani 1 1 d . . . . . H10A H -0.0665 0.7987 0.7864 0.117 Uiso 1 1 calc R U . . . H10B H -0.0536 0.8079 0.8645 0.117 Uiso 1 1 calc R U . . . H10C H -0.0714 0.7225 0.8334 0.117 Uiso 1 1 calc R U . . . C11 C 0.0762(6) 0.6924(6) 0.7400(4) 0.082(3) Uani 1 1 d . . . . . H11A H 0.0525 0.7187 0.7016 0.123 Uiso 1 1 calc R U . . . H11B H 0.0499 0.6413 0.7474 0.123 Uiso 1 1 calc R U . . . H11C H 0.1328 0.6836 0.7318 0.123 Uiso 1 1 calc R U . . . C12 C 0.2189(6) 0.7263(6) 1.1855(5) 0.085(3) Uani 1 1 d . . . . . H12A H 0.2137 0.7327 1.2335 0.127 Uiso 1 1 calc R U . . . H12B H 0.2310 0.7778 1.1654 0.127 Uiso 1 1 calc R U . . . H12C H 0.2619 0.6889 1.1760 0.127 Uiso 1 1 calc R U . . . C13 C 0.0443(7) 0.7588(7) 1.1726(4) 0.097(3) Uani 1 1 d . . . . . H13A H 0.0396 0.7627 1.2208 0.145 Uiso 1 1 calc R U . . . H13B H -0.0059 0.7400 1.1539 0.145 Uiso 1 1 calc R U . . . H13C H 0.0569 0.8111 1.1542 0.145 Uiso 1 1 calc R U . . . C14 C 0.1023(7) 0.5921(5) 1.1920(4) 0.085(3) Uani 1 1 d . . . . . H14A H 0.0959 0.6006 1.2397 0.127 Uiso 1 1 calc R U . . . H14B H 0.1459 0.5548 1.1844 0.127 Uiso 1 1 calc R U . . . H14C H 0.0532 0.5702 1.1737 0.127 Uiso 1 1 calc R U . . . C15 C 0.0323(3) 0.4719(3) 1.0451(3) 0.0299(10) Uani 1 1 d . . . . . H15A H 0.0487 0.4592 1.0888 0.036 Uiso 1 1 calc R U . . . C16 C 0.0781(4) 0.4303(4) 0.9969(2) 0.0335(12) Uani 1 1 d . . . . . C17 C 0.0750(4) 0.4320(4) 0.9272(3) 0.0344(13) Uani 1 1 d . . . . . H17A H 0.1127 0.3969 0.9082 0.041 Uiso 1 1 calc R U . . . C18 C 0.0310(3) 0.4719(4) 0.8784(3) 0.0368(12) Uani 1 1 d . . . . . H18A H 0.0468 0.4576 0.8349 0.044 Uiso 1 1 calc R U . . . C19 C 0.2509(4) 0.3759(5) 0.9780(6) 0.087(3) Uani 1 1 d . . . . . H19A H 0.2927 0.3406 0.9943 0.130 Uiso 1 1 calc R U . . . H19B H 0.2685 0.4311 0.9816 0.130 Uiso 1 1 calc R U . . . H19C H 0.2395 0.3635 0.9316 0.130 Uiso 1 1 calc R U . . . C20 C 0.1812(7) 0.3824(7) 1.1174(5) 0.106(4) Uani 1 1 d . . . . . H20A H 0.2229 0.3463 1.1328 0.158 Uiso 1 1 calc R U . . . H20B H 0.1332 0.3744 1.1439 0.158 Uiso 1 1 calc R U . . . H20C H 0.1992 0.4373 1.1220 0.158 Uiso 1 1 calc R U . . . C21 C 0.1295(4) 0.2561(4) 1.0188(5) 0.068(2) Uani 1 1 d . . . . . H21A H 0.1719 0.2218 1.0355 0.102 Uiso 1 1 calc R U . . . H21B H 0.1205 0.2448 0.9718 0.102 Uiso 1 1 calc R U . . . H21C H 0.0807 0.2460 1.0437 0.102 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Er1 0.03014(12) 0.03473(13) 0.04114(12) -0.00026(11) -0.00002(11) -0.00797(9) Si1 0.0656(11) 0.0497(10) 0.0371(9) 0.0012(7) -0.0004(8) -0.0135(8) Si2 0.0640(11) 0.0526(10) 0.0430(9) -0.0038(8) -0.0145(8) -0.0072(9) Si3 0.0345(7) 0.0427(8) 0.0522(9) -0.0016(8) -0.0057(8) 0.0123(6) C1 0.048(3) 0.040(3) 0.039(3) -0.002(2) 0.007(3) -0.017(2) C2 0.047(3) 0.032(3) 0.041(4) 0.001(2) -0.001(3) -0.004(2) C3 0.045(3) 0.039(3) 0.038(3) -0.004(2) 0.001(2) -0.008(2) C4 0.042(3) 0.044(3) 0.046(3) 0.001(3) -0.009(3) -0.015(3) C5 0.039(3) 0.048(3) 0.060(4) 0.001(3) -0.015(3) -0.008(2) C6 0.029(3) 0.046(3) 0.085(6) -0.004(3) -0.006(3) -0.003(2) C7 0.030(3) 0.054(4) 0.075(5) -0.007(4) 0.018(3) -0.007(3) C8 0.046(3) 0.052(4) 0.053(4) -0.007(3) 0.015(3) -0.012(3) C9 0.115(8) 0.067(5) 0.058(5) 0.008(4) 0.004(5) -0.027(5) C10 0.075(5) 0.094(6) 0.064(5) 0.013(4) -0.014(4) 0.007(5) C11 0.116(8) 0.089(6) 0.041(4) -0.016(4) -0.006(4) -0.019(5) C12 0.086(6) 0.098(7) 0.069(5) -0.016(5) -0.029(5) -0.022(5) C13 0.106(7) 0.129(9) 0.054(5) -0.017(5) -0.001(5) 0.037(7) C14 0.146(9) 0.068(5) 0.041(3) -0.001(4) -0.003(4) -0.019(5) C15 0.027(2) 0.029(2) 0.034(3) 0.001(2) -0.001(2) 0.0014(18) C16 0.028(3) 0.034(3) 0.039(2) -0.001(3) -0.001(2) 0.002(2) C17 0.028(3) 0.033(3) 0.043(3) -0.008(3) 0.004(3) -0.002(2) C18 0.036(3) 0.047(3) 0.027(2) -0.006(2) 0.004(2) -0.008(2) C19 0.043(3) 0.066(5) 0.150(9) 0.020(6) 0.022(5) 0.018(3) C20 0.117(8) 0.124(8) 0.076(6) -0.028(6) -0.049(6) 0.079(7) C21 0.059(4) 0.042(3) 0.104(6) 0.009(4) -0.007(4) 0.016(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Er1 C2 2.518(6) . ? Er1 C3 2.532(6) . ? Er1 C5 2.535(6) . ? Er1 C8 2.533(6) . ? Er1 C7 2.539(6) . ? Er1 C6 2.539(6) . ? Er1 C1 2.553(6) . ? Er1 C4 2.562(6) . ? Er1 C15 2.690(5) . ? Er1 C15 2.720(5) 2_565 ? Er1 C16 2.762(7) . ? Er1 C17 2.775(6) . ? Si1 C10 1.867(9) . ? Si1 C11 1.876(8) . ? Si1 C9 1.866(8) . ? Si1 C1 1.880(7) . ? Si2 C12 1.847(8) . ? Si2 C14 1.851(8) . ? Si2 C13 1.864(10) . ? Si2 C4 1.890(6) . ? Si3 C21 1.857(7) . ? Si3 C20 1.863(9) . ? Si3 C19 1.877(8) . ? Si3 C16 1.901(6) . ? C1 C8 1.426(9) . ? C1 C2 1.417(8) . ? C2 C3 1.422(9) . ? C3 C4 1.393(9) . ? C4 C5 1.423(9) . ? C5 C6 1.409(10) . ? C6 C7 1.403(12) . ? C7 C8 1.397(11) . ? C15 C16 1.428(7) . ? C15 C15 1.444(9) 2_565 ? C15 Er1 2.720(5) 2_565 ? C16 C17 1.409(7) . ? C16 Er1 2.800(7) 2_565 ? C17 C18 1.408(8) . ? C17 Er1 2.793(6) 2_565 ? C18 C18 1.409(12) 2_565 ? C18 Er1 2.804(5) 2_565 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 Er1 C3 32.7(2) . . ? C2 Er1 C5 83.9(2) . . ? C3 Er1 C5 60.8(2) . . ? C2 Er1 C8 61.5(2) . . ? C3 Er1 C8 84.3(2) . . ? C5 Er1 C8 84.4(2) . . ? C2 Er1 C7 83.2(2) . . ? C3 Er1 C7 92.0(2) . . ? C5 Er1 C7 61.7(3) . . ? C8 Er1 C7 32.0(2) . . ? C2 Er1 C6 92.1(2) . . ? C3 Er1 C6 83.0(2) . . ? C5 Er1 C6 32.3(2) . . ? C8 Er1 C6 61.5(2) . . ? C7 Er1 C6 32.1(3) . . ? C2 Er1 C1 32.45(19) . . ? C3 Er1 C1 62.73(19) . . ? C5 Er1 C1 94.3(2) . . ? C8 Er1 C1 32.6(2) . . ? C7 Er1 C1 61.9(2) . . ? C6 Er1 C1 84.7(2) . . ? C2 Er1 C4 62.1(2) . . ? C3 Er1 C4 31.7(2) . . ? C5 Er1 C4 32.4(2) . . ? C8 Er1 C4 94.10(19) . . ? C7 Er1 C4 84.6(2) . . ? C6 Er1 C4 62.0(2) . . ? C1 Er1 C4 85.98(19) . . ? C2 Er1 C15 142.89(18) . . ? C3 Er1 C15 115.44(17) . . ? C5 Er1 C15 91.63(19) . . ? C8 Er1 C15 154.80(19) . . ? C7 Er1 C15 126.5(2) . . ? C6 Er1 C15 103.5(2) . . ? C1 Er1 C15 171.49(17) . . ? C4 Er1 C15 95.79(17) . . ? C2 Er1 C15 115.58(17) . 2_565 ? C3 Er1 C15 97.58(17) . 2_565 ? C5 Er1 C15 105.2(2) . 2_565 ? C8 Er1 C15 169.80(19) . 2_565 ? C7 Er1 C15 157.0(2) . 2_565 ? C6 Er1 C15 128.6(2) . 2_565 ? C1 Er1 C15 140.81(17) . 2_565 ? C4 Er1 C15 92.61(17) . 2_565 ? C15 Er1 C15 30.95(19) . 2_565 ? C2 Er1 C16 173.17(18) . . ? C3 Er1 C16 141.55(17) . . ? C5 Er1 C16 94.67(19) . . ? C8 Er1 C16 125.06(19) . . ? C7 Er1 C16 102.0(2) . . ? C6 Er1 C16 90.2(2) . . ? C1 Er1 C16 154.34(17) . . ? C4 Er1 C16 113.65(18) . . ? C15 Er1 C16 30.33(15) . . ? C15 Er1 C16 58.32(16) 2_565 . ? C2 Er1 C17 156.20(19) . . ? C3 Er1 C17 171.04(17) . . ? C5 Er1 C17 113.77(18) . . ? C8 Er1 C17 102.74(19) . . ? C7 Er1 C17 91.2(2) . . ? C6 Er1 C17 95.34(17) . . ? C1 Er1 C17 125.99(18) . . ? C4 Er1 C17 140.58(18) . . ? C15 Er1 C17 56.30(16) . . ? C15 Er1 C17 76.54(17) 2_565 . ? C16 Er1 C17 29.50(14) . . ? C10 Si1 C11 107.1(4) . . ? C10 Si1 C9 111.0(4) . . ? C11 Si1 C9 109.4(4) . . ? C10 Si1 C1 111.4(3) . . ? C11 Si1 C1 110.8(4) . . ? C9 Si1 C1 107.2(3) . . ? C12 Si2 C14 108.5(5) . . ? C12 Si2 C13 108.2(5) . . ? C14 Si2 C13 107.8(5) . . ? C12 Si2 C4 107.9(4) . . ? C14 Si2 C4 112.3(3) . . ? C13 Si2 C4 112.0(4) . . ? C21 Si3 C20 109.8(5) . . ? C21 Si3 C19 106.5(4) . . ? C20 Si3 C19 109.5(5) . . ? C21 Si3 C16 110.9(3) . . ? C20 Si3 C16 110.9(3) . . ? C19 Si3 C16 109.1(3) . . ? C8 C1 C2 130.6(6) . . ? C8 C1 Si1 116.1(5) . . ? C2 C1 Si1 113.2(5) . . ? C8 C1 Er1 73.0(3) . . ? C2 C1 Er1 72.4(3) . . ? Si1 C1 Er1 139.0(3) . . ? C3 C2 C1 137.5(6) . . ? C3 C2 Er1 74.2(4) . . ? C1 C2 Er1 75.1(3) . . ? C4 C3 C2 137.1(6) . . ? C4 C3 Er1 75.3(3) . . ? C2 C3 Er1 73.1(3) . . ? C3 C4 C5 131.4(6) . . ? C3 C4 Si2 116.5(5) . . ? C5 C4 Si2 112.1(5) . . ? C3 C4 Er1 72.9(3) . . ? C5 C4 Er1 72.8(3) . . ? Si2 C4 Er1 137.7(3) . . ? C6 C5 C4 136.1(6) . . ? C6 C5 Er1 74.0(4) . . ? C4 C5 Er1 74.8(3) . . ? C7 C6 C5 135.3(7) . . ? C7 C6 Er1 74.0(4) . . ? C5 C6 Er1 73.7(4) . . ? C6 C7 C8 135.8(7) . . ? C6 C7 Er1 73.9(4) . . ? C8 C7 Er1 73.8(4) . . ? C7 C8 C1 136.1(6) . . ? C7 C8 Er1 74.2(4) . . ? C1 C8 Er1 74.5(3) . . ? C16 C15 C15 136.9(3) . 2_565 ? C16 C15 Er1 77.6(4) . . ? C15 C15 Er1 75.7(3) 2_565 . ? C16 C15 Er1 78.2(3) . 2_565 ? C15 C15 Er1 73.4(3) 2_565 2_565 ? Er1 C15 Er1 98.90(16) . 2_565 ? C17 C16 C15 130.7(5) . . ? C17 C16 Si3 112.2(5) . . ? C15 C16 Si3 117.0(4) . . ? C17 C16 Er1 75.8(4) . . ? C15 C16 Er1 72.1(3) . . ? Si3 C16 Er1 130.7(3) . . ? C17 C16 Er1 75.1(4) . 2_565 ? C15 C16 Er1 71.9(3) . 2_565 ? Si3 C16 Er1 134.0(4) . 2_565 ? Er1 C16 Er1 95.30(17) . 2_565 ? C16 C17 C18 136.9(6) . . ? C16 C17 Er1 74.7(4) . . ? C18 C17 Er1 76.2(3) . . ? C16 C17 Er1 75.7(5) . 2_565 ? C18 C17 Er1 75.9(3) . 2_565 ? Er1 C17 Er1 95.19(17) . 2_565 ? C17 C18 C18 135.5(3) . 2_565 ? C17 C18 Er1 74.5(3) . . ? C18 C18 Er1 75.7(4) 2_565 . ? C17 C18 Er1 75.0(3) . 2_565 ? C18 C18 Er1 75.1(3) 2_565 2_565 ? Er1 C18 Er1 94.44(15) . 2_565 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C10 Si1 C1 C8 143.2(5) . . . . ? C11 Si1 C1 C8 24.1(6) . . . . ? C9 Si1 C1 C8 -95.2(5) . . . . ? C10 Si1 C1 C2 -40.1(5) . . . . ? C11 Si1 C1 C2 -159.2(5) . . . . ? C9 Si1 C1 C2 81.5(5) . . . . ? C10 Si1 C1 Er1 49.4(6) . . . . ? C11 Si1 C1 Er1 -69.7(6) . . . . ? C9 Si1 C1 Er1 171.0(5) . . . . ? C8 C1 C2 C3 -2.4(12) . . . . ? Si1 C1 C2 C3 -178.5(6) . . . . ? Er1 C1 C2 C3 45.0(7) . . . . ? C8 C1 C2 Er1 -47.4(6) . . . . ? Si1 C1 C2 Er1 136.5(3) . . . . ? C1 C2 C3 C4 -1.0(13) . . . . ? Er1 C2 C3 C4 44.3(7) . . . . ? C1 C2 C3 Er1 -45.3(7) . . . . ? C2 C3 C4 C5 3.2(12) . . . . ? Er1 C3 C4 C5 46.9(6) . . . . ? C2 C3 C4 Si2 -179.0(6) . . . . ? Er1 C3 C4 Si2 -135.3(4) . . . . ? C2 C3 C4 Er1 -43.7(7) . . . . ? C12 Si2 C4 C3 -115.1(5) . . . . ? C14 Si2 C4 C3 125.4(6) . . . . ? C13 Si2 C4 C3 3.8(7) . . . . ? C12 Si2 C4 C5 63.1(6) . . . . ? C14 Si2 C4 C5 -56.4(6) . . . . ? C13 Si2 C4 C5 -178.0(6) . . . . ? C12 Si2 C4 Er1 151.4(5) . . . . ? C14 Si2 C4 Er1 31.9(7) . . . . ? C13 Si2 C4 Er1 -89.6(6) . . . . ? C3 C4 C5 C6 -0.8(12) . . . . ? Si2 C4 C5 C6 -178.7(6) . . . . ? Er1 C4 C5 C6 46.1(7) . . . . ? C3 C4 C5 Er1 -46.9(6) . . . . ? Si2 C4 C5 Er1 135.2(3) . . . . ? C4 C5 C6 C7 -1.1(14) . . . . ? Er1 C5 C6 C7 45.3(8) . . . . ? C4 C5 C6 Er1 -46.4(7) . . . . ? C5 C6 C7 C8 -0.7(16) . . . . ? Er1 C6 C7 C8 44.6(9) . . . . ? C5 C6 C7 Er1 -45.2(8) . . . . ? C6 C7 C8 C1 1.4(15) . . . . ? Er1 C7 C8 C1 46.0(7) . . . . ? C6 C7 C8 Er1 -44.6(9) . . . . ? C2 C1 C8 C7 1.2(12) . . . . ? Si1 C1 C8 C7 177.3(6) . . . . ? Er1 C1 C8 C7 -46.0(7) . . . . ? C2 C1 C8 Er1 47.2(6) . . . . ? Si1 C1 C8 Er1 -136.8(3) . . . . ? C15 C15 C16 C17 1.0(16) 2_565 . . . ? Er1 C15 C16 C17 -51.7(9) . . . . ? Er1 C15 C16 C17 50.3(9) 2_565 . . . ? C15 C15 C16 Si3 179.8(7) 2_565 . . . ? Er1 C15 C16 Si3 127.1(5) . . . . ? Er1 C15 C16 Si3 -130.9(5) 2_565 . . . ? C15 C15 C16 Er1 52.7(8) 2_565 . . . ? Er1 C15 C16 Er1 102.00(12) 2_565 . . . ? C15 C15 C16 Er1 -49.3(8) 2_565 . . 2_565 ? Er1 C15 C16 Er1 -102.00(12) . . . 2_565 ? C15 C16 C17 C18 1.0(18) . . . . ? Si3 C16 C17 C18 -177.9(7) . . . . ? Er1 C16 C17 C18 -49.3(10) . . . . ? Er1 C16 C17 C18 50.2(10) 2_565 . . . ? C15 C16 C17 Er1 50.4(9) . . . . ? Si3 C16 C17 Er1 -128.5(5) . . . . ? Er1 C16 C17 Er1 99.57(11) 2_565 . . . ? C15 C16 C17 Er1 -49.2(9) . . . 2_565 ? Si3 C16 C17 Er1 131.9(5) . . . 2_565 ? Er1 C16 C17 Er1 -99.57(11) . . . 2_565 ? C16 C17 C18 C18 -0.8(18) . . . 2_565 ? Er1 C17 C18 C18 -49.7(9) . . . 2_565 ? Er1 C17 C18 C18 49.4(9) 2_565 . . 2_565 ? C16 C17 C18 Er1 48.9(10) . . . . ? Er1 C17 C18 Er1 99.06(12) 2_565 . . . ? C16 C17 C18 Er1 -50.2(11) . . . 2_565 ? Er1 C17 C18 Er1 -99.06(13) . . . 2_565 ? _refine_diff_density_max 0.867 _refine_diff_density_min -0.335 _refine_diff_density_rms 0.098 _shelxl_version_number 2013-4 _shelx_res_file ; TITL mm297 in I-4 CELL 0.71073 16.86200 16.86200 20.21490 90.0000 90.0000 90.0000 ZERR 8.00 0.00040 0.00040 0.00050 0.0000 0.0000 0.0000 LATT -2 SYMM -X, -Y, Z SYMM Y, -X, -Z SYMM -Y, X, -Z SFAC C H SI ER UNIT 168 288 24 8 TEMP -73.15C SIZE 0.07 0.13 0.17 L.S. 80 BOND FMAP 2 PLAN 5 LIST 0 ACTA CONF OMIT 2 2 0 OMIT 0 2 0 OMIT -2 4 0 OMIT 3 0 3 OMIT -2 1 3 OMIT 0 3 3 OMIT 1 2 3 OMIT 1 3 0 OMIT -1 3 0 OMIT 2 0 2 OMIT 1 1 0 OMIT -1 2 5 OMIT -3 6 3 OMIT 0 2 2 OMIT -1 2 3 OMIT 3 6 1 OMIT 2 2 2 OMIT -2 2 2 OMIT 2 4 2 OMIT -1 9 0 OMIT 2 1 3 OMIT -3 9 0 OMIT -1 1 4 OMIT -2 8 0 OMIT 2 7 7 OMIT 2 0 4 OMIT 11 5 20 OMIT -7 2 7 OMIT -3 7 0 OMIT -6 4 8 OMIT 4 6 8 OMIT -3 6 15 OMIT 3 1 2 OMIT 6 3 1 OMIT 0 0 4 OMIT 1 1 4 OMIT 2 4 0 OMIT 0 1 3 OMIT 4 1 3 OMIT -1 3 2 OMIT -1 9 2 OMIT 3 4 1 OMIT -1 4 3 OMIT -4 9 5 OMIT 3 9 0 OMIT 6 3 5 OMIT 1 3 2 OMIT -2 9 21 OMIT 0 4 0 OMIT 9 1 2 WGHT 0.038400 FVAR 0.04109 ER1 4 0.082505 0.589725 0.965762 11.00000 0.03014 0.03473 = 0.04114 -0.00026 -0.00002 -0.00797 SI1 3 0.063800 0.756573 0.815084 11.00000 0.06560 0.04967 = 0.03714 0.00123 -0.00043 -0.01346 SI2 3 0.125022 0.687721 1.151230 11.00000 0.06399 0.05264 = 0.04300 -0.00384 -0.01450 -0.00717 SI3 3 0.158786 0.361566 1.028812 11.00000 0.03453 0.04266 = 0.05225 -0.00164 -0.00567 0.01225 C1 1 0.108630 0.707942 0.889941 11.00000 0.04786 0.03974 = 0.03937 -0.00175 0.00735 -0.01696 C2 1 0.078312 0.737828 0.950375 11.00000 0.04690 0.03207 = 0.04056 0.00072 -0.00118 -0.00426 AFIX 43 H2A 2 0.038882 0.777048 0.942855 11.00000 -1.20000 AFIX 0 C3 1 0.090634 0.725302 1.019198 11.00000 0.04452 0.03949 = 0.03756 -0.00426 0.00095 -0.00774 AFIX 43 H3A 2 0.057886 0.759003 1.045124 11.00000 -1.20000 AFIX 0 C4 1 0.137827 0.676885 1.058770 11.00000 0.04235 0.04407 = 0.04640 0.00056 -0.00916 -0.01463 C5 1 0.197507 0.620596 1.042338 11.00000 0.03936 0.04820 = 0.05980 0.00147 -0.01469 -0.00763 AFIX 43 H5A 2 0.220145 0.596975 1.080598 11.00000 -1.20000 AFIX 0 C6 1 0.231518 0.591033 0.983619 11.00000 0.02890 0.04557 = 0.08518 -0.00422 -0.00605 -0.00257 AFIX 43 H6A 2 0.272024 0.553179 0.991983 11.00000 -1.20000 AFIX 0 C7 1 0.219872 0.604127 0.915757 11.00000 0.03026 0.05449 = 0.07519 -0.00736 0.01846 -0.00690 AFIX 43 H7A 2 0.254881 0.573362 0.889353 11.00000 -1.20000 AFIX 0 C8 1 0.169530 0.651215 0.877431 11.00000 0.04614 0.05182 = 0.05278 -0.00698 0.01526 -0.01223 AFIX 43 H8A 2 0.178004 0.643500 0.831418 11.00000 -1.20000 AFIX 0 C9 1 0.117184 0.852280 0.802279 11.00000 0.11491 0.06652 = 0.05847 0.00835 0.00429 -0.02702 AFIX 33 H9A 2 0.095264 0.879454 0.763522 11.00000 -1.50000 H9B 2 0.173700 0.841781 0.795131 11.00000 -1.50000 H9C 2 0.110625 0.885872 0.841460 11.00000 -1.50000 AFIX 0 C10 1 -0.044832 0.773407 0.826170 11.00000 0.07505 0.09419 = 0.06448 0.01313 -0.01444 0.00730 AFIX 33 H10A 2 -0.066482 0.798727 0.786446 11.00000 -1.50000 H10B 2 -0.053613 0.807877 0.864509 11.00000 -1.50000 H10C 2 -0.071418 0.722452 0.833375 11.00000 -1.50000 AFIX 0 C11 1 0.076246 0.692376 0.740030 11.00000 0.11610 0.08873 = 0.04060 -0.01577 -0.00566 -0.01896 AFIX 33 H11A 2 0.052461 0.718710 0.701636 11.00000 -1.50000 H11B 2 0.049936 0.641313 0.747406 11.00000 -1.50000 H11C 2 0.132845 0.683560 0.731830 11.00000 -1.50000 AFIX 0 C12 1 0.218942 0.726322 1.185549 11.00000 0.08621 0.09843 = 0.06931 -0.01590 -0.02948 -0.02235 AFIX 33 H12A 2 0.213711 0.732723 1.233535 11.00000 -1.50000 H12B 2 0.230998 0.777769 1.165363 11.00000 -1.50000 H12C 2 0.261940 0.688950 1.175953 11.00000 -1.50000 AFIX 0 C13 1 0.044332 0.758799 1.172562 11.00000 0.10630 0.12913 = 0.05445 -0.01682 -0.00093 0.03743 AFIX 33 H13A 2 0.039556 0.762711 1.220767 11.00000 -1.50000 H13B 2 -0.005895 0.739952 1.153912 11.00000 -1.50000 H13C 2 0.056906 0.811110 1.154224 11.00000 -1.50000 AFIX 0 C14 1 0.102337 0.592081 1.192044 11.00000 0.14650 0.06780 = 0.04054 -0.00114 -0.00291 -0.01860 AFIX 33 H14A 2 0.095869 0.600600 1.239695 11.00000 -1.50000 H14B 2 0.145949 0.554784 1.184362 11.00000 -1.50000 H14C 2 0.053187 0.570234 1.173679 11.00000 -1.50000 AFIX 0 C15 1 0.032296 0.471887 1.045089 11.00000 0.02701 0.02908 = 0.03355 0.00095 -0.00140 0.00140 AFIX 43 H15A 2 0.048671 0.459191 1.088790 11.00000 -1.20000 AFIX 0 C16 1 0.078090 0.430310 0.996862 11.00000 0.02767 0.03413 = 0.03863 -0.00068 -0.00122 0.00245 C17 1 0.075049 0.431987 0.927199 11.00000 0.02796 0.03269 = 0.04268 -0.00780 0.00371 -0.00179 AFIX 43 H17A 2 0.112726 0.396854 0.908172 11.00000 -1.20000 AFIX 0 C18 1 0.030961 0.471942 0.878359 11.00000 0.03582 0.04725 = 0.02730 -0.00581 0.00403 -0.00769 AFIX 43 H18A 2 0.046784 0.457609 0.834869 11.00000 -1.20000 AFIX 0 C19 1 0.250877 0.375918 0.978030 11.00000 0.04340 0.06620 = 0.15005 0.02018 0.02234 0.01846 AFIX 33 H19A 2 0.292721 0.340642 0.994342 11.00000 -1.50000 H19B 2 0.268517 0.431130 0.981596 11.00000 -1.50000 H19C 2 0.239470 0.363475 0.931641 11.00000 -1.50000 AFIX 0 C20 1 0.181162 0.382375 1.117379 11.00000 0.11693 0.12379 = 0.07623 -0.02812 -0.04925 0.07889 AFIX 33 H20A 2 0.222860 0.346330 1.132757 11.00000 -1.50000 H20B 2 0.133194 0.374401 1.143931 11.00000 -1.50000 H20C 2 0.199204 0.437340 1.122038 11.00000 -1.50000 AFIX 0 C21 1 0.129507 0.256069 1.018755 11.00000 0.05874 0.04200 = 0.10363 0.00928 -0.00718 0.01573 AFIX 33 H21A 2 0.171915 0.221777 1.035509 11.00000 -1.50000 H21B 2 0.120490 0.244779 0.971798 11.00000 -1.50000 H21C 2 0.080667 0.245986 1.043651 11.00000 -1.50000 AFIX 0 HKLF 4 REM mm297 in I-4 REM R1 = 0.0277 for 6433 Fo > 4sig(Fo) and 0.0346 for all 7058 data REM 226 parameters refined using 0 restraints END WGHT 0.0377 0.0000 REM Highest difference peak 0.867, deepest hole -0.335, 1-sigma level 0.098 Q1 1 0.1304 0.5730 0.9668 11.00000 0.05 0.87 Q2 1 0.0025 0.9322 0.6320 11.00000 0.05 0.69 Q3 1 0.0097 0.9361 1.0330 11.00000 0.05 0.67 Q4 1 -0.0365 0.9654 0.9595 11.00000 0.05 0.65 Q5 1 0.0597 0.5571 0.9644 11.00000 0.05 0.58 ; _shelx_res_checksum 70313 _shelx_hkl_file ; 1 1 0 526.73 18.46 -1 1 0 527.35 18.37 0 2 0 94.55 3.37 2 0 0 96.53 3.34 2 2 0 30.15 1.10 -2 2 0 29.62 1.07 -1 3 0 346.39 12.08 1 3 0 8.70 0.39 3 3 0 141.45 5.05 -3 3 0 142.72 5.00 -2 4 0 11.71 0.50 4 0 0 159.43 5.41 -4 0 0 152.90 5.41 0 4 0 152.43 5.47 2 4 0 170.84 6.04 4 -4 0 53.43 2.02 -4 4 0 53.72 1.93 4 4 0 52.22 1.99 -4 4 0 55.22 2.01 -3 5 0 1.77 0.18 5 3 0 1.95 0.23 5 3 0 1.58 0.19 5 1 0 257.36 8.92 -1 5 0 252.98 8.96 1 5 0 118.93 4.30 5 -1 0 121.82 4.39 -5 3 0 3.99 0.18 3 5 0 3.84 0.29 5 -3 0 4.18 0.30 5 -5 0 75.70 2.77 5 5 0 74.19 2.74 5 -5 0 74.27 2.78 5 5 0 73.76 2.76 -5 5 0 75.22 2.77 -5 5 0 72.53 2.66 -4 6 0 1.61 0.18 6 4 0 1.48 0.21 4 -6 0 1.56 0.28 6 4 0 1.65 0.20 -4 6 0 1.25 0.16 6 4 0 1.68 0.28 -2 6 0 50.53 1.90 6 2 0 51.52 1.97 6 2 0 50.62 1.87 2 -6 0 51.63 1.95 6 0 0 622.96 21.46 6 0 0 612.35 21.87 0 6 0 621.27 21.53 -6 0 0 608.23 21.48 2 6 0 76.47 2.78 6 -2 0 74.19 2.83 6 -4 0 58.72 2.13 4 6 0 52.78 2.08 4 6 0 57.42 2.12 -4 -6 0 55.14 2.10 6 -4 0 53.39 2.12 -6 4 0 54.02 1.96 6 -6 0 514.46 17.56 -6 6 0 507.36 17.93 6 6 0 514.03 17.55 6 -6 0 500.21 17.94 6 6 0 505.35 17.93 -6 -6 0 491.57 17.52 6 6 0 502.40 17.69 -6 6 0 497.59 17.59 5 -7 0 107.65 4.00 7 5 0 108.07 4.03 -5 7 0 110.55 3.99 -5 7 0 106.34 3.91 7 5 0 108.52 3.96 7 5 0 112.19 4.02 7 3 0 3.67 0.33 7 3 0 4.16 0.43 -3 7 0 3.58 0.28 3 -7 0 4.06 0.38 1 -7 0 125.70 4.50 7 1 0 123.93 4.60 -1 7 0 122.96 4.50 7 1 0 125.83 4.51 7 1 0 122.84 4.42 -1 7 0 126.45 4.70 -7 -1 0 122.67 4.42 -1 7 0 129.16 4.70 7 -1 0 196.43 6.99 7 -1 0 194.03 7.15 -1 -7 0 198.27 6.96 1 7 0 200.54 7.03 3 7 0 0.87 0.27 -3 -7 0 0.62 0.25 7 -3 0 0.87 0.18 7 -3 0 0.98 0.26 3 7 0 0.98 0.19 5 7 0 502.15 17.59 5 7 0 510.18 17.77 -7 5 0 500.85 17.44 7 -5 0 491.62 17.85 -7 5 0 502.26 17.84 7 -5 0 504.68 17.45 -5 -7 0 502.99 17.43 5 7 0 492.55 17.43 -7 7 0 129.89 4.58 7 -7 0 125.40 4.72 -7 -7 0 130.22 4.72 -7 7 0 125.94 4.74 7 -7 0 129.53 4.76 7 7 0 130.05 4.70 7 7 0 125.94 4.72 7 7 0 131.92 4.73 6 -8 0 26.12 1.22 -6 8 0 26.97 1.12 8 6 0 24.93 1.14 -6 8 0 26.17 1.06 8 6 0 25.57 1.23 8 6 0 26.25 1.13 -4 8 0 2.34 0.27 4 -8 0 2.39 0.36 8 4 0 2.09 0.38 -4 8 0 2.11 0.25 8 4 0 2.15 0.28 -8 -2 0 12.16 0.54 8 2 0 11.32 0.52 8 2 0 10.81 0.61 8 2 0 10.92 0.69 2 -8 0 12.86 0.69 -2 8 0 11.64 0.59 8 0 0 22.28 1.02 0 8 0 22.48 0.98 -8 0 0 22.50 0.86 8 0 0 22.56 1.05 0 -8 0 23.04 1.01 8 0 0 22.55 0.85 8 -2 0 5.28 0.49 8 -2 0 4.95 0.41 -2 -8 0 4.93 0.45 2 8 0 6.10 0.53 2 8 0 5.42 0.39 4 8 0 25.57 1.11 -4 -8 0 25.71 1.15 8 -4 0 25.87 1.18 8 -4 0 24.73 1.13 4 8 0 25.03 1.17 6 8 0 85.67 3.14 -8 6 0 85.26 3.22 8 -6 0 84.37 3.01 -6 -8 0 84.89 3.21 6 8 0 86.16 3.19 6 8 0 84.00 3.22 8 -6 0 84.51 3.23 8 -6 0 82.95 3.21 -8 6 0 83.14 3.01 -8 8 0 8.55 0.44 8 8 0 8.24 0.57 8 8 0 8.46 0.52 -8 -8 0 8.62 0.73 -8 8 0 8.43 0.55 8 8 0 7.98 0.71 8 -8 0 8.86 0.71 8 -8 0 7.66 0.43 -7 9 0 55.80 2.13 9 7 0 56.07 2.25 9 7 0 56.82 2.22 7 -9 0 58.81 2.33 -7 9 0 55.56 2.21 9 7 0 55.38 2.32 5 -9 0 5.82 0.57 -9 -5 0 5.59 0.41 -5 9 0 5.20 0.39 -5 9 0 5.64 0.40 9 5 0 5.13 0.43 9 5 0 5.28 0.57 -9 -3 0 0.11 0.13 9 3 0 0.28 0.29 9 3 0 0.27 0.14 9 3 0 0.13 0.17 -3 9 0 0.24 0.16 3 -9 0 0.47 0.26 9 1 0 1.06 0.24 -1 9 0 1.28 0.24 9 1 0 1.15 0.31 1 -9 0 1.08 0.30 -9 -1 0 1.30 0.16 9 1 0 1.50 0.18 1 9 0 1.78 0.28 -1 -9 0 1.81 0.32 9 -1 0 1.90 0.35 9 -1 0 1.67 0.27 3 9 0 0.00 0.15 9 -3 0 0.18 0.18 3 9 0 0.13 0.29 9 -3 0 0.29 0.26 -3 -9 0 0.21 0.27 5 9 0 1.31 0.28 5 9 0 1.10 0.18 -9 5 0 1.09 0.25 9 -5 0 1.07 0.34 5 9 0 0.95 0.35 9 -5 0 1.29 0.26 -5 -9 0 1.20 0.32 7 9 0 8.70 0.74 -7 -9 0 7.41 0.69 9 -7 0 7.98 0.58 9 -7 0 8.28 0.71 7 9 0 8.11 0.49 -9 7 0 7.64 0.56 7 9 0 7.57 0.57 9 9 0 2.38 0.38 -9 9 0 2.08 0.35 -9 -9 0 2.70 0.52 9 -9 0 1.76 0.49 9 9 0 2.52 0.53 9 9 0 2.29 0.33 -10 -8 0 26.99 1.28 10 8 0 27.42 1.27 8 -10 0 29.43 1.45 10 8 0 27.89 1.44 -8 10 0 26.96 1.24 -10 -6 0 76.62 2.87 10 6 0 75.31 2.85 6 -10 0 74.10 2.95 -6 10 0 75.79 2.85 10 6 0 73.46 2.97 -6 10 0 74.52 2.81 10 6 0 75.48 2.94 -10 -4 0 3.91 0.34 10 4 0 3.81 0.33 4 -10 0 2.82 0.42 -4 10 0 2.85 0.35 10 4 0 3.44 0.40 -4 10 0 4.03 0.35 10 4 0 4.08 0.51 -2 10 0 5.77 0.35 10 2 0 5.67 0.47 -2 10 0 5.56 0.44 10 2 0 6.34 0.59 10 2 0 5.06 0.34 2 -10 0 5.13 0.55 -10 -2 0 6.07 0.36 10 0 0 24.13 1.19 10 0 0 25.22 1.17 0 -10 0 24.81 1.16 -10 0 0 24.47 0.94 0 10 0 24.88 1.11 10 -2 0 19.23 0.98 10 -2 0 19.32 1.02 -2 -10 0 20.49 1.00 2 10 0 19.37 0.94 10 -4 0 27.59 1.30 10 -4 0 28.04 1.33 4 10 0 28.13 1.33 -4 -10 0 28.44 1.31 4 10 0 28.07 1.26 -6 -10 0 60.99 2.48 6 10 0 61.41 2.45 -10 6 0 61.35 2.48 6 10 0 62.20 2.52 10 -6 0 60.55 2.49 10 -6 0 63.57 2.53 10 -8 0 0.10 0.35 10 -8 0 0.29 0.24 -10 8 0 0.44 0.28 -8 -10 0 0.03 0.39 8 10 0 0.59 0.45 8 10 0 0.46 0.27 -10 10 0 26.23 1.29 10 10 0 27.44 1.31 -10 -10 0 27.74 1.33 -10 -10 0 25.63 1.43 10 -10 0 25.86 1.40 10 10 0 26.81 1.48 -11 -9 0 0.46 0.49 11 9 0 0.93 0.33 -9 11 0 1.34 0.34 9 -11 0 1.44 0.53 11 9 0 1.50 0.56 -11 -9 0 0.88 0.31 -11 -7 0 126.03 4.67 11 7 0 121.87 4.76 7 -11 0 129.47 4.78 11 7 0 129.07 4.66 -7 11 0 120.91 4.58 11 7 0 126.95 4.76 -5 11 0 66.37 2.61 11 5 0 69.13 2.61 11 5 0 65.66 2.76 11 5 0 69.31 2.74 5 -11 0 69.91 2.75 -11 -5 0 69.64 2.62 -11 -3 0 1.81 0.24 3 -11 0 1.14 0.40 -3 11 0 1.32 0.28 11 3 0 1.40 0.23 11 3 0 1.66 0.31 11 3 0 2.02 0.44 11 1 0 111.15 4.18 1 -11 0 111.80 4.09 11 1 0 107.82 4.12 -11 -1 0 107.53 3.91 -1 11 0 108.58 4.06 11 1 0 108.23 3.92 1 11 0 71.21 2.77 11 -1 0 68.66 2.82 11 -1 0 72.52 2.86 -1 -11 0 72.98 2.79 -3 -11 0 1.03 0.38 11 -3 0 1.13 0.31 3 11 0 1.29 0.31 11 -3 0 1.23 0.38 5 11 0 139.80 5.19 -11 5 0 141.83 5.26 5 11 0 132.73 5.16 11 -5 0 139.72 5.21 -5 -11 0 142.03 5.17 11 -5 0 142.38 5.28 -7 -11 0 24.71 1.30 -11 7 0 24.63 1.23 7 11 0 24.32 1.22 7 11 0 22.64 1.33 11 -7 0 24.99 1.33 11 -7 0 24.74 1.23 9 11 0 15.42 1.13 -9 -11 0 15.85 1.08 9 11 0 16.18 0.95 11 -9 0 14.94 1.09 -11 9 0 15.69 0.93 11 -11 0 19.29 1.28 -11 11 0 21.19 1.13 -11 -11 0 20.01 1.27 -11 -11 0 21.30 1.17 11 11 0 21.59 1.15 11 11 0 20.17 1.31 -12 -10 0 5.29 0.74 12 10 0 4.92 0.72 -12 -10 0 4.72 0.56 10 -12 0 5.04 0.72 12 10 0 5.49 0.58 -12 -8 0 13.97 0.85 12 8 0 15.14 0.88 12 8 0 16.37 0.92 12 8 0 14.59 1.11 8 -12 0 13.74 1.00 6 -12 0 124.03 4.74 -12 -6 0 124.92 4.64 12 6 0 126.59 4.79 12 6 0 126.80 4.79 -6 12 0 125.61 4.63 12 4 0 23.11 1.17 12 4 0 23.00 1.28 -12 -4 0 21.83 1.01 12 4 0 22.38 1.01 -4 12 0 22.84 1.09 4 -12 0 24.22 1.25 12 2 0 95.28 3.70 12 2 0 92.31 3.66 -2 12 0 93.84 3.59 2 -12 0 97.11 3.64 12 0 0 119.74 4.57 0 -12 0 117.51 4.45 0 12 0 120.07 4.46 12 0 0 118.93 4.51 12 -2 0 3.77 0.56 12 -2 0 2.36 0.38 -2 -12 0 3.02 0.49 2 12 0 3.01 0.41 12 -4 0 86.05 3.50 -12 4 0 91.79 3.54 12 -4 0 88.36 3.54 4 12 0 90.76 3.48 -4 -12 0 91.95 3.48 -6 -12 0 83.63 3.39 12 -6 0 92.15 3.49 12 -6 0 84.82 3.45 -12 6 0 86.10 3.44 6 12 0 88.07 3.41 6 12 0 87.13 3.45 -12 8 0 0.39 0.33 8 12 0 0.01 0.48 -8 -12 0 -0.09 0.45 12 -8 0 0.46 0.47 8 12 0 0.05 0.31 12 -8 0 0.02 0.27 10 12 0 27.29 1.55 -10 -12 0 28.44 1.42 10 12 0 28.45 1.41 -10 -12 0 27.96 1.54 -12 10 0 26.64 1.39 12 -10 0 27.30 1.54 12 -12 0 36.07 1.86 -12 -12 0 34.21 1.81 12 12 0 34.24 1.69 12 12 0 33.92 1.86 -12 -12 0 35.59 1.70 13 11 0 6.42 0.72 13 11 0 5.44 0.82 11 -13 0 6.94 0.84 -13 -11 0 6.20 0.80 -13 -11 0 5.59 0.67 13 9 0 -0.27 0.43 13 9 0 0.02 0.24 13 9 0 -0.15 0.28 -13 -9 0 -0.28 0.25 9 -13 0 -0.08 0.40 7 -13 0 22.11 1.30 -13 -7 0 21.16 1.08 13 7 0 19.74 1.13 13 7 0 23.12 1.34 5 -13 0 37.45 1.78 13 5 0 36.13 1.71 -5 13 0 37.91 1.62 13 5 0 36.90 1.82 -3 13 0 0.84 0.30 13 3 0 0.43 0.45 3 -13 0 0.61 0.43 13 3 0 0.39 0.27 -1 13 0 80.32 3.19 1 -13 0 81.42 3.24 13 1 0 83.08 3.29 13 1 0 84.35 3.31 1 13 0 7.16 0.63 -1 -13 0 6.46 0.75 13 -1 0 7.81 0.79 13 -1 0 6.99 0.66 13 -3 0 20.18 1.10 3 13 0 18.93 1.06 -3 -13 0 18.02 1.12 13 -3 0 18.63 1.12 5 13 0 66.00 2.70 -13 5 0 67.09 2.74 13 -5 0 67.98 2.78 13 -5 0 64.72 2.77 -5 -13 0 64.15 2.71 -7 -13 0 16.81 1.12 7 13 0 16.26 1.01 13 -7 0 18.50 1.16 7 13 0 15.42 1.13 13 -7 0 16.68 1.05 -13 7 0 15.11 1.00 -9 -13 0 5.67 0.72 13 -9 0 6.21 0.75 9 13 0 6.43 0.83 -13 9 0 5.34 0.65 -9 -13 0 6.72 0.68 9 13 0 6.28 0.67 -11 -13 0 47.70 2.14 11 13 0 44.46 2.24 13 -11 0 48.58 2.27 -13 11 0 49.90 2.15 -11 -13 0 43.60 2.19 11 13 0 48.04 2.14 13 -13 0 19.65 1.41 -13 -13 0 20.42 1.42 13 13 0 20.69 1.22 13 13 0 18.36 1.42 -13 -13 0 19.52 1.24 14 12 0 4.94 0.82 -14 -12 0 4.47 0.60 12 -14 0 3.80 0.71 14 12 0 3.93 0.58 -14 -12 0 3.81 0.74 -14 -10 0 -0.40 0.46 10 -14 0 -0.59 0.46 -14 -10 0 -0.02 0.28 14 10 0 0.17 0.54 14 10 0 -0.02 0.32 14 8 0 0.62 0.51 8 -14 0 0.47 0.49 14 8 0 0.58 0.30 14 6 0 2.93 0.46 -6 14 0 2.86 0.42 6 -14 0 3.07 0.55 14 6 0 3.07 0.61 14 4 0 5.98 0.63 14 4 0 5.10 0.72 -4 14 0 5.98 0.60 4 -14 0 4.35 0.66 -2 14 0 0.95 0.34 14 2 0 0.42 0.31 2 -14 0 0.41 0.41 14 2 0 0.78 0.50 14 0 0 6.12 0.68 0 14 0 6.54 0.64 0 -14 0 7.64 0.81 14 0 0 7.00 0.84 14 -2 0 0.79 0.36 -2 -14 0 1.02 0.48 2 14 0 1.12 0.38 14 -2 0 0.61 0.47 14 -4 0 3.69 0.63 4 14 0 3.26 0.50 -4 -14 0 4.36 0.64 -14 4 0 2.84 0.49 14 -4 0 3.43 0.52 6 14 0 9.89 0.95 14 -6 0 8.83 0.78 -6 -14 0 7.84 0.84 -14 6 0 7.62 0.76 6 14 0 8.03 0.74 14 -6 0 8.63 0.89 8 14 0 -0.22 0.46 -8 -14 0 0.06 0.48 14 -8 0 0.06 0.30 -14 8 0 -0.40 0.33 -8 -14 0 -0.23 0.32 14 -8 0 0.58 0.50 8 14 0 0.44 0.36 14 -10 0 11.85 1.10 10 14 0 11.75 1.15 10 14 0 12.91 0.97 -10 -14 0 11.20 1.08 -10 -14 0 13.23 0.96 -14 10 0 14.00 1.01 -12 -14 0 15.07 1.21 12 14 0 15.16 1.08 12 14 0 14.95 1.29 -12 -14 0 16.19 1.09 14 -12 0 16.88 1.30 -14 -14 0 2.33 0.53 14 14 0 1.38 0.50 -14 -14 0 1.92 0.70 14 -14 0 1.64 0.70 14 14 0 1.75 0.69 15 13 0 7.44 1.01 13 -15 0 6.03 0.95 -15 -13 0 6.75 0.92 15 11 0 1.76 0.66 -15 -11 0 1.16 0.57 11 -15 0 0.74 0.58 15 9 0 0.03 0.52 15 9 0 0.09 0.30 9 -15 0 0.03 0.46 15 7 0 7.73 0.74 7 -15 0 6.98 0.84 15 7 0 7.97 0.96 15 5 0 1.03 0.51 15 5 0 0.65 0.35 -5 15 0 0.34 0.29 5 -15 0 0.81 0.48 15 3 0 4.92 0.62 15 3 0 5.69 0.71 3 -15 0 5.22 0.72 -3 15 0 5.88 0.59 1 -15 0 6.16 0.74 15 1 0 5.76 0.67 -1 15 0 6.37 0.64 15 1 0 7.24 0.86 -1 -15 0 0.74 0.48 15 -1 0 0.97 0.51 1 15 0 0.71 0.37 15 -1 0 1.55 0.38 -3 -15 0 0.03 0.41 3 15 0 0.41 0.32 15 -3 0 0.51 0.34 15 -3 0 0.64 0.47 -15 3 0 0.42 0.32 15 -5 0 1.34 0.49 -15 5 0 1.23 0.43 15 -5 0 1.39 0.40 -5 -15 0 1.06 0.49 5 15 0 0.75 0.38 -7 -15 0 0.07 0.34 7 15 0 0.18 0.53 -7 -15 0 0.62 0.50 7 15 0 -0.23 0.32 15 -7 0 1.06 0.53 -15 7 0 0.56 0.38 15 -7 0 -0.36 0.31 -9 -15 0 0.12 0.51 9 15 0 0.09 0.36 -15 9 0 0.04 0.36 9 15 0 -0.02 0.54 -9 -15 0 0.16 0.34 15 -9 0 0.92 0.55 -15 11 0 0.67 0.43 15 -11 0 -0.10 0.54 11 15 0 0.73 0.42 -11 -15 0 0.74 0.40 -11 -15 0 0.02 0.53 11 15 0 0.58 0.60 -13 -15 0 0.70 0.46 15 -13 0 1.07 0.67 -13 -15 0 0.71 0.60 13 15 0 1.73 0.71 13 15 0 0.82 0.47 15 15 0 0.05 0.46 -15 -15 0 0.04 0.62 15 15 0 0.13 0.69 15 -15 0 0.37 0.71 16 14 0 9.44 1.19 14 -16 0 10.00 1.21 -16 -14 0 9.85 1.14 12 -16 0 12.66 1.25 16 12 0 9.89 1.17 -16 -12 0 11.83 1.24 -16 -10 0 1.82 0.63 10 -16 0 0.96 0.59 16 10 0 1.18 0.66 16 8 0 8.40 0.82 8 -16 0 7.94 0.90 16 8 0 9.49 1.05 16 6 0 24.58 1.50 6 -16 0 25.15 1.47 16 6 0 22.42 1.35 4 -16 0 1.88 0.41 16 4 0 2.47 0.62 16 4 0 2.11 0.47 4 -16 0 1.03 0.47 -4 16 0 1.83 0.42 16 2 0 28.26 1.50 2 -16 0 28.40 1.56 -2 16 0 30.03 1.45 16 2 0 26.91 1.57 16 0 0 17.37 1.13 0 16 0 17.80 1.08 16 0 0 18.33 1.23 0 -16 0 17.77 1.13 -16 2 0 0.09 0.37 16 -2 0 0.18 0.46 16 -2 0 0.38 0.35 -2 -16 0 0.67 0.48 2 16 0 1.29 0.41 -4 -16 0 6.73 0.82 4 16 0 6.50 0.74 -16 4 0 7.64 0.80 16 -4 0 7.44 0.86 16 -4 0 7.65 0.79 -6 -16 0 7.21 0.74 16 -6 0 8.46 0.86 -16 6 0 8.21 0.85 -6 -16 0 9.13 0.93 16 -6 0 8.09 0.87 6 16 0 7.94 0.81 8 16 0 0.37 0.41 16 -8 0 0.99 0.51 -8 -16 0 0.45 0.40 -16 8 0 0.43 0.41 -8 -16 0 0.34 0.53 -16 10 0 3.40 0.60 -10 -16 0 3.69 0.74 -10 -16 0 4.04 0.65 10 16 0 3.52 0.62 10 16 0 2.84 0.76 16 -10 0 3.94 0.82 12 16 0 5.11 0.75 -12 -16 0 4.05 0.83 -12 -16 0 4.15 0.69 16 -12 0 4.86 0.90 12 16 0 4.30 0.84 16 -14 0 -1.12 0.56 14 16 0 -0.38 0.45 -14 -16 0 -0.37 0.67 14 16 0 0.69 0.71 -14 -16 0 1.01 0.48 13 -17 0 18.46 1.57 -17 -13 0 18.34 1.48 17 13 0 19.50 1.65 -17 -11 0 3.55 0.81 11 -17 0 4.27 0.79 17 11 0 6.78 0.96 17 9 0 0.84 0.63 -17 -9 0 1.31 0.45 9 -17 0 0.21 0.59 17 9 0 0.63 0.35 7 -17 0 25.23 1.54 17 7 0 23.80 1.56 17 7 0 23.46 1.39 5 -17 0 16.99 1.08 17 5 0 19.15 1.20 17 5 0 18.05 1.33 -5 17 0 17.55 1.08 5 -17 0 17.70 1.27 3 -17 0 3.85 0.56 17 3 0 3.85 0.74 3 -17 0 4.32 0.71 17 3 0 3.23 0.56 -3 17 0 3.68 0.55 -1 17 0 59.72 2.60 17 1 0 59.66 2.71 17 1 0 60.95 2.70 1 -17 0 60.59 2.67 -17 -1 0 62.20 2.70 17 -1 0 12.50 1.14 1 17 0 13.60 1.00 -1 -17 0 14.67 1.13 17 -1 0 15.27 1.08 -17 1 0 14.49 1.06 17 -3 0 1.97 0.51 17 -3 0 1.75 0.58 -17 3 0 1.31 0.49 -3 -17 0 1.98 0.59 3 17 0 1.49 0.46 -5 -17 0 20.71 1.34 -17 5 0 20.82 1.31 -5 -17 0 20.44 1.27 17 -5 0 20.03 1.33 5 17 0 17.82 1.19 17 -5 0 20.62 1.39 -17 7 0 10.51 0.97 17 -7 0 8.34 1.02 7 17 0 8.07 0.88 -7 -17 0 8.93 1.01 -7 -17 0 7.77 0.83 9 17 0 2.39 0.57 -17 9 0 2.81 0.58 -9 -17 0 2.15 0.54 17 -9 0 1.96 0.70 -9 -17 0 2.24 0.64 11 17 0 11.91 1.31 -11 -17 0 12.64 1.08 -11 -17 0 14.98 1.28 17 -11 0 14.22 1.35 -17 11 0 13.52 1.14 11 17 0 13.79 1.13 17 -13 0 2.55 0.89 -13 -17 0 2.31 0.58 13 17 0 2.24 0.62 13 17 0 1.78 0.75 -13 -17 0 1.84 0.79 -18 -12 0 11.83 1.29 18 12 0 12.49 1.36 12 -18 0 11.27 1.35 10 -18 0 -0.20 0.63 18 10 0 1.56 0.74 8 -18 0 6.47 0.92 18 8 0 7.25 0.99 -18 -8 0 7.63 0.93 18 8 0 6.19 0.79 6 -18 0 20.00 1.40 18 6 0 17.80 1.23 -18 -6 0 18.20 1.26 18 6 0 19.03 1.40 -4 18 0 2.44 0.51 -18 -4 0 2.01 0.55 18 4 0 1.44 0.64 4 -18 0 2.38 0.63 4 -18 0 2.37 0.48 18 4 0 2.40 0.52 18 2 0 30.11 1.65 18 2 0 27.68 1.70 2 -18 0 30.77 1.71 -2 18 0 29.02 1.57 -18 -2 0 30.88 1.67 2 -18 0 29.27 1.56 0 18 0 38.12 1.91 18 0 0 37.97 1.98 0 -18 0 39.75 1.93 18 0 0 38.96 2.04 -18 0 0 40.75 2.00 0 -18 0 38.91 1.99 2 18 0 0.43 0.40 18 -2 0 0.09 0.55 18 -2 0 0.86 0.42 -2 -18 0 0.06 0.51 -18 2 0 0.72 0.47 -2 -18 0 0.57 0.41 -4 -18 0 21.11 1.33 18 -4 0 22.81 1.42 -4 -18 0 19.36 1.39 4 18 0 21.81 1.35 18 -4 0 21.69 1.47 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0.68 -3 -19 0 3.24 0.63 -3 -19 0 3.35 0.74 3 19 0 3.97 0.69 -19 3 0 3.97 0.71 19 -3 0 4.25 0.83 5 19 0 17.08 1.26 -19 5 0 18.98 1.33 19 -5 0 17.38 1.44 -5 -19 0 17.24 1.37 19 -5 0 17.10 1.30 -5 -19 0 16.99 1.23 -19 7 0 2.91 0.65 -7 -19 0 2.29 0.58 -7 -19 0 2.17 0.70 19 -7 0 2.19 0.74 7 19 0 2.02 0.59 19 -9 0 6.19 1.03 -19 9 0 7.21 0.91 -9 -19 0 4.71 0.91 -19 11 0 12.77 1.22 19 -11 0 11.54 1.42 -11 -19 0 12.12 1.43 10 -20 0 0.97 0.81 20 10 0 0.18 0.70 20 8 0 -0.45 0.43 -20 -8 0 0.35 0.46 8 -20 0 0.76 0.78 20 8 0 0.23 0.66 20 6 0 0.27 0.43 -20 -6 0 0.71 0.52 20 6 0 0.41 0.62 6 -20 0 1.01 0.70 20 4 0 -0.04 0.60 4 -20 0 -0.07 0.58 -20 -4 0 0.53 0.50 20 4 0 0.10 0.43 -20 -2 0 -0.28 0.47 20 2 0 -0.03 0.43 2 -20 0 0.10 0.39 20 2 0 0.77 0.66 2 -20 0 -0.23 0.57 -2 20 0 0.03 0.41 0 20 0 1.59 0.54 0 -20 0 2.53 0.72 20 0 0 2.60 0.78 20 0 0 3.47 0.66 0 -20 0 3.10 0.61 -20 0 0 2.01 0.59 20 -2 0 0.78 0.52 2 20 0 0.82 0.51 -2 -20 0 1.02 0.63 20 -2 0 0.78 0.70 -20 2 0 0.45 0.51 -2 -20 0 1.27 0.49 4 20 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